• Journal of the Korean Society of Propulsion Engineers
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• v.16 no.3
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• pp.9-15
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• 2012

This research simulates the ultrasonic wave propagation in multi-layered media using generalized formular of system response function. We made the artificial defect specimen of a rocket motor and compared with experimental wave forms. The simulation results are coincide with measured waves and we found that the pulse echo method is able to detect unbond defect at liner-propellant interface.

• Proceedings of the Korean Society of Propulsion Engineers Conference
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• 2011.11a
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• pp.912-918
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• 2011

This research simulates the ultrasonic wave propagation in multi-layered media using generalized formular of system response function. We made the artificial defect specimen of a rocket motor and compared with experimental wave forms. The simulation results are coinciede with mesuared waves and we found that the pulse echo method is able to detect disbond at liner-propellant interface.

• Journal of the Korean Society for Nondestructive Testing
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• v.32 no.4
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• pp.401-409
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• 2012

Ultrasonic testing are far superior to other nondestructive tests for detecting the disbond interface which occurred in adhesive interface. However, a solid rocket motor consisting of a steel case, rubber insulation, liner, and propellant poses many difficulties for analyzing ultrasonic waves because of the superposition of reflected waves and large differences in acoustic impedance of various materials. Therefore, ultrasonic tests for detecting the disbond interface in solid rocket motor have been applied in very limited areas between the steel case and rubber insulation using an automatic C-scan system. The existing ultrasonic test cannot detect the disbond interface between the liner and propellant of a solid rocket motor because most of the ultrasonic waves are absorbed in the rubber material which has low acoustic impedance. This problem could be overcome by analyzing the resonance frequency from the frequency spectrum using the ultrasonic resonance method. In this paper, a new technique to detect the disbond interface between the liner and propellant using ultrasonic resonance characteristics is discussed in detail.

• Journal of the Korean Society of Propulsion Engineers
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• v.12 no.2
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• pp.40-47
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• 2008

It is known that the adhesive interface testing of the rocket motor using the ultrasonic wave is superior to the other testing methods about the ability to economical detect the defects. But, the signal analysis of the ultrasonic wave takes a lot of time and efforts because the time interval of the transmitted pulse and the received pulse is too short to separate the reflected signals due to the multi-layers of the rocket motor. The ultrasonic testing of rocket motor have only applied to the automatic system about extremely limited areas like the debond in adhesive interface between the motor case and the insulator. In this study the new technique to detect the debond between the liner and the propellant using the property of the resonance and the lamb waves instead of the existing ultrasonic testing was described.

• Proceedings of the Korean Society of Propulsion Engineers Conference
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• 2007.11a
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• pp.55-59
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• 2007

It is known that the adhesive interface testing of the rocket motor which using the ultrasonic wave iS superior to the other testing methods about the economically detectable abiliη of the defects. But, the signal analysis of the ultrasonic wave takes too much time and effort that the time interval of the transmitted pulse and the received pulse is too short to be separated the reflected signals because the structure of the rocket motor is multi-layers. The ultrasonic testing of rocket motor have been only applied with automatic system about extremely limited area like the debond in adhesive interface between the motor case and insulator. In this study the new technique to detect the debond between the liner and the propellant using the property of the resonance and Lamb waves was described as comparing the existence ultrasonic testing.

• Journal of Adhesion and Interface
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• v.11 no.4
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• pp.174-180
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• 2010

The effect of carbon nanotube surface treatment on the interface and thermal conductivity of carbon nanotube-based poly(methylmethacrylate) (PMMA) composites was investigated. Coagulation and atomic-transfer radical polymerization (ATRP) was applied to modify the surface of multi-wall carbon nano-tube. The composite of ATRP method used carbon nanotube showed the higher transparency and thermal conductivities than that of the coagulation method used. In comparison to the thermal conductivity of pure PMMA, 0.21 W/mK, the ATRP carbon nanotube used PMMA/MWNT composite showed a thermal conductivity of 0.38 W/mK. The interface between carbon nanotube and PMMA was observed by scanning electron microscope and uniform dispersion of carbon nanotube was observed without any void in the PMMA matrix. It may be beneficial to transport the phonon without any scattering and it may result in a higher thermal conductivity.

• Journal of Adhesion and Interface
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• v.19 no.2
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• pp.68-73
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• 2018

In this study, conductive EVA foams including multi-wall carbon nanotubes (MWCNT), glass beads were prepared. The electrical conductivity and physical properties of the foams were confirmed with varying amount of MWCNT, mixing time, and amount of glass beads. The electrical conductivity increased with the amount of MWCNT. Dispersity of MWCNT in EVA foams were improved with glass beads. It can be suggested that conductive EVA foams can be successfully prepared with improved dispersity of MWCNT in ethylene-vinyl acetate by using glass beads.

• Journal of Adhesion and Interface
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• v.14 no.1
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• pp.1-12
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• 2013

Multi core-shell composite particles were prepared by the water-born emulsion polymerization of various core monomers such as methyl methacrylate (MMA), ethyl methacrylate (EMA) and shell monomers such as MMA, EMA, 2-hydroxyl ethyl methacrylate (2-HEMA), glycidyl methacrylate (GMA) and methacrylic acid (MAA) in the presence of different concentrations of sodium dodecyl benzene sulfonate (SDBS). The following conclusions are drawn from the conversion, particle size and distribution, average molecular weight, molecular structure, glass transition temperature with DSC, contact angle after plasma treatment, tensile strength and isothermal decomposition kinetics. In the case of the concentration of 0.02 wt% SDBS, the conversion of MMA core-(EMA/GMA) shell composite particles was excellent as 98.5%. In the case of the concentration of 0.03 wt% SDBS, the particle size of EMA core-(MMA/GMA) shell composite particles was high as $0.48{\mu}m$. We confirmed that 3 points of glass transition temperatures appear for multi core-shell composite particles compared to 1~2 points of glass transition temperatures appear for general copolymer particles. Overall, the adhesion strength of shell composite particles was in the order of EMA/MAA > EMA/2-HEMA > EMA/GMA.

• Journal of Adhesion and Interface
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• v.12 no.1
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• pp.16-25
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• 2011

Multi core-shell composite particles were prepared by the water-born emulsion polymerization of various core monomer such as methyl methacrylate (MMA), n-butyl methacrylate (BMA), and shell monomer such as MMA, BMA, stylene (St), 2-hydroxyl ethyl methacrylate (2-HEMA) and acrylic acid (AA) in the presence of different concentration of sodium dodecyl benzene sulfonate (SDBS). The following conclusions are drawn from the measured conversion, particle size and distribution, average molecular weight, molecular structure, glass transition temperature with DSC, morphology, tensile strength and elongation. In the case of the concentration of 0.02 wt% SDBS, the conversion of MMA core-(BMA/St/AA) shell composite particle was excellent as 98%. In the case of the concentration of 0.03 wt% SDBS, the particle size of BMA core-(MMA/St/AA) shell composite particle was high as $0.47{\mu}m$. We confirmed that 3 points of glass transition temperatures appear for multi core-shell composite particles compared to 2 points of glass transition temperatures appear for general core-shell composite particles. We showed that it is possible to adjust glass transition temperatures according to the kind and composition of the inner shell monomer that it is can be used as a adhesive binder material with improved adhesive power.

• Journal of Adhesion and Interface
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• v.13 no.3
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• pp.137-144
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• 2012

Chemical functionalization of carbon nanomaterials (CNMs) is generally carried out for increasing interfacial adhesion between filler and polymer matrix for CNM-polymer nanocomposites. The chemically functionalized CNTs can produce strong interfacial bonds with many polymers, allowing CNT based nanocomposites to possess high mechanical and functional properties. Hence, increased surface adhesion can be measured indirectly by observing increased mechanical properties. However, there is a more direct way to observe interfacial bonds between polymer and CNM by measuring piezoresistivity behavior so that we can imagine the behavior of CNM particles in polymer matrix under deflection. Fuctionalization of MWCNT and rGO was carried out by oxidization reaction of MWCNT and rGO with $H_2SO_4/HNO_3$ solution. Electrical resistivities of MWCNT-PMMA and rGO-PMMA composites were decreased after functionalization because of the destructive fuctionalization process. Meanwhile, piezoresistivities of functionalized CNM-PMMA composites showed more sensitive behavior under the same deflection as compared to pristine CNM-PMMA composites. Therefore, mobility of CNM in polymer matrix was found to be improved with chemical functionalization.