• Title/Summary/Keyword: $OCl^-$

Search Result 441, Processing Time 0.03 seconds

The Refactoring Specification for Dynamic Composition based on OCL (동적 조립을 위한 OCL 기반의 리팩토링 명세)

  • Jang, Pil-Jae;Kim, Kyung-Min;Kim, Tae-Woong;Kim, Un-Ji
    • Proceedings of the Korea Information Processing Society Conference
    • /
    • 2009.11a
    • /
    • pp.857-858
    • /
    • 2009
  • 최근의 소프트웨어 개발에서는 리팩토링이 일반적인 요소로서 활발하게 이용되고 있다. 리팩토링에 대한 관심이 높아지면서 리팩토링의 자동화와 리팩토링 재사용을 위한 조립에 대한 연구가 많이 진행되고 있다. 기존의 연구들에서는 리팩토링과 리팩토링 조립에 대해 선/후행조건을 각각 명세하고 있다. 하지만 리팩토링 조립의 경우에 대한 선/후행조건은 개별적인 리팩토링들의 선/후행조건들과 중복된 기능들이 대부분이며, 사용 가능한 리팩토링의 조립이 정적으로 고정되어 있음을 의미한다. 이에 본 연구에서는 리팩토링 조립의 경우가 고정되어 있지 않고 조립의 경우에 따른 선/후행조건의 추가적인 정의 없이 동적으로 다양하게 조립여부를 확인할 수 있도록 하고자 한다. 이를 위해 리팩토링의 동적 조립을 위한 전체 프레임워크를 제안하며 OCL 기반으로 리팩토링을 명세한다.

Passivation effect on large volume CdZnTe crystals

  • B. Park;Y. Kim;J. Seo;J. Byun;K. Kim
    • Nuclear Engineering and Technology
    • /
    • v.54 no.12
    • /
    • pp.4620-4624
    • /
    • 2022
  • Several cadmium zinc telluride (CZT) crystals were fabricated into radiation detectors using methods that included slicing, dicing, lapping, polishing, and chemical etching. A wet passivation with sodium hypochlorite (NaOCl) was then carried out on the Br-etched detectors. The Te-rich layer on the CZT surface was successfully compensated to the Te oxide layer, which was analyzed with X-ray photoelectron spectroscopy data of both a Br-etched crystal and a passivated CZT crystals. We confirmed that passivation with NaOCl improved the transport property by analyzing the mobility-lifetime product and surface recombination velocity. The electrical and spectroscopic properties of large volume detectors were compared before and after passivation, and then the detectors were observed for a month. Both bar and quasi-hemispherical detectors show an enhancement in performance after passivation. Thus, we could identify the effect of NaOCl passivation on large volume CZT detectors.

Antimicrobial Activities of Propolis against Oral Candidiasis by Candida Albicans -Effect of Microbial Inhibition Using Propolis- (구강 캔디다증 알비칸스에 대한 프로 폴리스의 항균 활동 -프로폴리스를 이용한 미생물 억제 효과-)

  • Kwun, Hyeon-Sook;Nam, Seoul-Hee;Park, Min-Kyoung;Cho, Mi SooK;Cheon, Sae-Hee
    • Journal of the Korea Academia-Industrial cooperation Society
    • /
    • v.15 no.9
    • /
    • pp.5644-5651
    • /
    • 2014
  • Propolis is an extremely safe natural antimicrobial substance that has been reported to have powerful antibacterial efficacy. The aim of this study was to evaluate the inhibitory effects of propolis against Candida albicans (C. albicans). Propolis was collected from the honey bee Apis mellifera. The strain of C. albicans was cultivated overnight in liquid media incubated at $37^{\circ}C$. The antimicrobial activity was investigated using phosphate buffered saline (PBS), 3% sodium hypochlorite (NaOCl), 0.1% chorhexidine (CHX), and propolis extracts ($5{\mu}l/ml$, $10{\mu}l/ml$). C. albicans were sensitive to 3% NaOCl, 0.1% CHX, and propolis ($5{\mu}l/ml$, $10{\mu}l/ml$) with zones of inhibition of 15, 14.5, 16, and 17 mm, respectively. The CFU of PBS, 3% NaOCl, 0.1% CHX, $5{\mu}l/ml$ and $10{\mu}l/ml$ of propolis led a 1, 7, 7, 5 and 7-log reduction. Among the groups tested, C. albicans was most sensitive to $10{\mu}l/ml$ of propolis, which showed the largest inhibition zones. Therefore, propolis can be a new antimicrobial therapy for oral mucosa disease in traditional medicine.

Preparation of Titanyl Chlorde (鹽化티타닐 製造에 關한 硏究)

  • Chyun, Byong-Doo;Shin, Yoon-Kyung
    • Journal of the Korean Chemical Society
    • /
    • v.4 no.1
    • /
    • pp.15-17
    • /
    • 1957
  • 1. Preparation of Titanium tetrachloride; The following precesses were strictly followed as the preliminary step to obtain pure $TiOCl_2$, titanyl chloride; First, pure Titanium Oxide mixed with carbon is rolled into pills. After drying up perfectly, these pills are heated at 900∼1000${\circ}C$. And then the pills are subjected to the flow of $Cl_2$ gas in a quartz tube heated to 900-1000${\circ}C$. Thus Titanium tetrachloride is obtained. 2. Preparation of $TiOCl_2$ ; Yellowish trobrown solution is made by pouring 80 g of conc. HCl (sp.gr. 1.19) to 45 gr of Titanium tetrachloride (approx. 2 times of theoretical amount). Then this solution is kept settled for 5-days in a desiccator filled with phosphorous pentoxide at room temperature. As the colorless amorphous solid thus obtained is washed with aceton, 36.5 g of the pure salt are obtained. 3. Determination of composition. The analysis of the sample taken from the deposit desiccated gives the following data; (A) Qualitative analysis; a) $Ti(OH)_4$ is precipitated by adding NaOH in water solution of the salt. b) Adding $AgNO_3$ solution, the water solution of the salt gives white precipitate of AgCl. c) When acid and $H_2O_2$ are added, the solution turns its color to redish brown (This proves that $TiO^{++}$ was converted into $TiO^{++}$ by oxidation of $H_2O_2$. (B) Quantitative analysis; a) $Ti(OH)_4$ precipitated by $10{\%}$ NaOH isalitatsubjected consecutively to the filtration and ignition in porcelain crucible at approx. 1000${\circ}C$. , then $TiO_2$ thus formed is weighed and calculated into Ti content. b) Chlorine involved in water solution of the salt is determined by Vorhardt method. Result: The values obtained from previous analysis, devied by their atomic weight gives the following composition: Ti : Cl = 1 : 2 Therefore $TiOCl_2$ should be given as its molecular formula. 4. Summary. When $TiCl_4$ is additated into conc. HCl, $TiO^{++}$ formed exists as a stable form, and forms $TiOCl_2$. However $TiOCl_2$ is unstable to heating. When the temperature is raised to $65{\circ}C$the decomposition of the solution is accelerated, and gives $TiO_2$ aq. $TiOCl_2$ in addition is highly hygroscopic.

  • PDF

Characteristic of Oxidation Reaction of Lanthanide Chlorides in Oxygen-Eutectic Salt Bubble Column (산소-공융염 기포탑에서 희토류염화물의 산화반응 특성)

  • Cho, Yung-Zun;Yang, Hee-Chul;Lee, Han-Soo;Kim, In-Tae
    • Korean Chemical Engineering Research
    • /
    • v.47 no.4
    • /
    • pp.465-469
    • /
    • 2009
  • Characteristics of oxidation reaction of four lanthanide chlorides(Ce, Nd, Pr and $EuCl_3$) in a oxygen-eutectic(LiCl-KCl) salt bubble column was investigated. From the results obtained from the thermochemical calculations by HSC chemistry software, the most stable lanthanide compounds in the oxygen-used rare earth chlorides system were oxychlorides(EuOCl, NdOCl, PrOCl) and oxides($CeO_2$, $PrO_2$), which coincide well with results of the Gibbs free energy of the reaction. In this study, similar to the thermochemical results, regardless of the sparging time and molten salt temperature, oxychlorides for Eu, Nd and Pr and oxides for Ce and Pr were formed as a precipitant by a reaction with oxygen. The structure of the rare earth precipitates was divided into two shapes : small cubic(oxide) and large tetragonal (oxychloride) structures. The conversion efficiencies of the lanthanide elements to their molten salt-insoluble precipitates(or compound) were increased with the sparging time and temperature, and Ce showed the best reactivity. In the conditions of $650^{\circ}C$ of the molten salt temperature and 420 min of the sparging time, the conversion efficiencies were over 99% for all the investigated lanthanide chlorides.

Asymbiotic germination and seedling growth of Calanthe striata f. sieboldii Decne. ex Regel (금새우난초(Calanthe striata f. sieboldii Decne. ex Regel)종자의 비공생 발아 및 신초증식)

  • Bae, Kee Hwa;Kim, Soo-Young
    • Journal of Plant Biotechnology
    • /
    • v.42 no.3
    • /
    • pp.239-244
    • /
    • 2015
  • Calanthe striata f. sieboldii Decne. ex Regel is a terrestrial orchid with beautiful flowers arranged in racemose inflorescences. This species is threatened due to over-collection and loss of suitable habitats. Asymbiotic germination is useful in the conservation efforts to re-establish plants in the wild, and for commercial propagation. In this study, we investigate the effects of sodium hypochlorite (NaOCl), three types of culture media (Phytomax Orchid Maintenance - POM, Seed Germination Maintenance - SGM, and Murashige and Skoog 1962 - MS), and plant growth regulators on embryo swelling, protocorm formation, and embryo diameter of C. striata f. sieboldii. Treatment with 1% NaOCl for 30 min greatly enhanced embryo swelling (28.3%), embryo diameter ($205.8{\mu}m$), and embryo protocorm formation (54.8%) compared to seeds without NaOCl treatment (embryo swelling 8.5%, embryo diameter $14.6{\mu}m$, and protocorm formation 13.4%) on POM medium. Protocorm formation on POM medium supplemented with 1.0 mg/L N6-benzyladenine (BA) (95.6%) was better than the control (54.5%). Additionally, the effects of activated charcoal (AC) and sucrose on seedling growth in in vitro culture were examined. The protocorm converted into healthy plants with well-developed shoot primordia on the POM medium with AC and sucrose. The most suitable conditions for seedling growth after 10 weeks of culture were the POM medium with AC or sucrose. These results show effective asymbiotic seed germination and in vitro seedling growth of C. striata f. sieboldii.

Seed Treatment and Plug Production of Ornamental Grasses (Gramineae spp.) (화본과 관상용 그래스의 종자처리와 플러그 묘 생산)

  • Kim, Ki Dong;Kim, Yoon Joong;Lee, Jong Min;Lee, Jeong Ho;Joo, Young Kyoo
    • Weed & Turfgrass Science
    • /
    • v.2 no.4
    • /
    • pp.376-380
    • /
    • 2013
  • This research was carried out to establish a mass-production method and to develop ornamental Gramineae species as cash crops for famers as three species of ornamental grasses were used for seed treatment and plug production. Germination rates of Arundinella hirta were improved to 52.6% by soaking in 4% NaOCl for 60 min and 49.4% with 4% NaOH for 30 min. Germination rates of Panicum virgatum were 20.3% and 22.4% when treated with 4% NaOCl for 10 min and 2% NaOH for 60min treatment, respectively. Pennisetum alopecuroides showed germination rates higher than 98% with both 4% of NaOCl and NaOH for 60 min. When the same size of trays were used, Pennisetum showed faster plug formation in 21 and 30 days with 162 and 40 cell trays, respectively. Arundinella showed a similar trend with Pannicum in completing plug formation, those took 32, 41, and 44 days with the 162, 72, and 40 cell tray, respectively. Plug production was faster with smaller cells; however, total growing period was longer with larger cells in general.

Synthesis and Characterization of Molybdenum(V)-Oxo Complexes with ONO-Donors

  • Kim, Jeong Suk;Kim, Hui Jeong;Gu, Bon Gwon
    • Bulletin of the Korean Chemical Society
    • /
    • v.16 no.1
    • /
    • pp.26-29
    • /
    • 1995
  • Six-coordinate molybdenum(Ⅴ)-oxo complexes (PyH)[MoOCl2L] and (R4N)-[MoOCl2L] (R=CH3 and C2H5) with N-salicylidene-2-aminophenol(L1) and its derivatives(L2=5-CH3, L3=3-CH3O, L4=5,6-C4H4 and L5=5-NO2) as ONO-donor ligands have been synthesized and the spectral and electrochemical properties of the complexes by elemental analysis, molar conductivity, UV-vis, IR, 1H NMR and CV have been studied.

Pull-out bond strength of a self-adhesive resin cement to NaOCl-treated root dentin: effect of antioxidizing agents

  • Khoroushi, Maryam;Kachuei, Marzieh
    • Restorative Dentistry and Endodontics
    • /
    • v.39 no.2
    • /
    • pp.95-103
    • /
    • 2014
  • Objectives: This study evaluated the effect of three antioxidizing agents on pullout bond strengths of dentin treated with sodium hypochlorite. Materials and Methods: Root canals of 75 single-rooted human teeth were prepared. Fifteen teeth were irrigated with normal saline for a negative control group, and the remaining 60 teeth (groups 2 - 5) with 2.5% NaOCl. The teeth in group 2 served as a positive control. Prior to post cementation, the root canals in groups 3 - 5 were irrigated with three antioxidizing agents including 10% rosmarinic acid (RA, Baridge essence), 10% hesperidin (HPN, Sigma), and 10% sodium ascorbate hydrogel (SA, AppliChem). Seventy-five spreaders (#55, taper .02, Produits Dentaires S.A) were coated with silica and silanized with the Rocatec system and ceramic bond. All the prepared spreaders were cemented with a self-adhesive resin cement (Bifix SE, Voco Gmbh) in the prepared canals. After storage in distilled water (24 h/$37^{\circ}C$), the spreaders were pulled out in a universal testing machine at a crosshead speed of 1.0 mm/min. Pull-out strength values were analyzed by one-way ANOVA and Tukey's HSD test (${\alpha}$ = 0.05). Results: There were significant differences between study groups (p = 0.016). The highest pullout strength was related to the SA group. The lowest strength was obtained in the positive control group. Conclusions: Irrigation with NaOCl during canal preparation decreased bond strength of resin cement to root dentin. Amongst the antioxidants tested, SA had superior results in reversing the diminishing effect of NaOCl irrigation on the bond strength to root dentin.