• Nuclear Engineering and Technology
• /
• 제54권3호
• /
• pp.1062-1070
• /
• 2022

In the present communication, pure and stable α-Bismuth Oxide (Bi₂O₃) nanoparticles (NPs) were synthesized by low temperature solution combustion method using urea as a fuel and calcined at 500℃. The synthesized sample was characterized by using powder X-ray Diffraction (PXRD), Scanning Electron Microscopy (SEM), Energy dispersive X-ray analysis (EDAX), Transmission Electron Microscopy (TEM), Fourier Transform Infrared Spectroscopy (FTIR) and UV-Visible absorption spectroscopy. The PXRD pattern confirms the formation of mono-clinic, stable and low temperature phase α-Bi₂O₃. The direct optical energy band gap was estimated by using Wood and Tauc's relation which was found to be 2.81 eV. The characterized sample was studied for X-ray/gamma ray shielding properties in the energy range 0.081-1.332 MeV using NaI (Tl) detector and multi channel analyzer (MCA). The measured shielding parameters agrees well with the theory, whereas, slight deviation up to 20% is observed below 356 keV. This deviation is mainly due to the influence of atomic size of the target medium. Furthermore an accurate theory is necessary to explain the interaction of X-ray/gamma ray with the NPs.The present work opens new window to use this facile, economical, efficient, low temperature method to synthesize nanomaterials for X-ray/gamma ray shielding purpose.

• 자원리싸이클링
• /
• 제1권1호
• /
• pp.44-50
• /
• 1992

소규모공장 규모의 알카리 및 산공정법에 의해 철강의 산세 폐액으로부터 $\alpha$-FeOOH를 제조하였으며, 이 때 합성된 분체를 TEM, SEM, TG-DTA, XRD, VSM 및 화학분석으로 물성을 조사하였다. 실험결과에 의하면, $\alpha$-FeOOH의 제조에 있어서 알카리 공정의 반응 시간이 짧으며, 제조된 분체는 약 $0.5\mu\textrm{m}$의 크기로 침상을 나타내었다. 또한 제조 방법에 따라 $\alpha$-FeOOH 와 $\alpha-Fe_2O_3$가 생성되며 이들은 미려한 황색 및 적색을 띠고 있었고 $\alpha-Fe_2O_3$를 $370^{\circ}C$의 수소 분위기에서 1시간 환원하면 367(Oe) 및 86.7 (emu/g)의 자성을 갖는 $Fe_3O_4$ 가 얻어질 수 있었다.

• 한국멀티미디어학회논문지
• /
• 제18권6호
• /
• pp.701-709
• /
• 2015

Image stitching method is a technique for obtaining an high-resolution image by combining two or more images. In X-ray image for clinical diagnosis, the size of the imaging region taken by one shot is limited due to the field-of-view of the equipment. Therefore, in order to obtain a high-resolution image including large regions such as a whole body, the synthesis of multiple X-ray images is required. In this paper, we propose a rapid stitching method of digital X-ray images using template-based registration. The proposed algorithm use principal component analysis(PCA) and k-nearest neighborhood(k-NN) to determine the location of input images before performing a template-based matching. After detecting the overlapping position using template-based matching, we synthesize input images by alpha blending. To improve the computational efficiency, reduced images are used for PCA and k-NN analysis. Experimental results showed that our method was more accurate comparing with the previous method with the improvement of the registration speed. Our stitching method could be usefully applied into the stitching of 2D or 3D multiple images.

• Bulletin of the Korean Chemical Society
• /
• 제34권10호
• /
• pp.3093-3097
• /
• 2013

The synthesis, X-ray crystallography, spectroscopic (IR, UV-vis), and electrochemical properties of the title compound, $[H_3O][Cr(dipic)_2][H_3O^+.Cl^-]$ (1), ($H_2dipic$ = 2,6-pyridinedicarboxylic acid), are reported. This complex crystallizes in the monoclinic space group Cc with a = 14.9006(10) ${\AA}$, b = 12.2114(8) ${\AA}$, c = 8.6337(6) ${\AA}$, ${\alpha}=90.00^{\circ}$, ${\beta}=92.7460(10)^{\circ}$, ${\gamma}=90.00^{\circ}$, and V = 1569.16(18) ${\AA}^3$ with Z = 4. The hydrogen bonding and noncovalent interactions play roles in the stabilization of the structure. In order to gain a better understanding of the most important geometrical parameters in the structure of the complex, atoms in molecules (AIM) method at B3LYP/6-31G level of theory has been employed.

• 한국방사선학회논문지
• /
• 제13권7호
• /
• pp.979-986
• /
• 2019

본 연구는 Rib Rando Phantom을 이용하여 겨드랑 첫 번째, 두 번째 갈비뼈 골절이 선예하게 나타나는 영상의 검사방법을 연구하였다. 팬톰의 자세와 엑스선관 각도를 수직, 머리쪽 5°, 다리쪽 5°로 변경하여 검사하였다. 획득한 영상을 방사선사가 주관적으로 영상평가 하였으며, 평가 데이터를 SPSS ver. 3.0으로 분석하였다. ImageJ Program을 이용하여 신호대잡음비(SNR)를 계산하였다. 그 결과 Cronbach Alpha 값이 0.789로 유의하게 높았다. 신호대잡음비(SNR)의 결과는 갈비뼈 앞쪽의 경우 엑스선관을 머리쪽으로 5° 기울여 검사 시 6.038, 갈비뼈 뒤쪽의 경우 엑스선관을 다리쪽으로 5° 기울여 검사 시 7.860으로 가장 높았다. 겨드랑 갈비뼈의 촬영기법으로 앞쪽 검사는 골절된 부위를 거상하고 엑스선관 각도를 머리쪽으로 5° 주며, 뒤쪽 검사는 골절된 부위를 밀착하여 엑스선관 각도를 발쪽으로 5° 기울여 검사한다면 선예한 영상을 얻을 수 있을 것으로 사료된다.

• 한국입자에어로졸학회지
• /
• 제9권4호
• /
• pp.209-219
• /
• 2013

We have used the modified diffusion flame burner to synthesize silica coated iron oxide nanoparticles having enhanced superparamagnetic property. Silica-encapsulated iron oxide particles were directly observed using a high resolution transmission electron microscope. From the energy dispersive X-ray spectroscopy (EDS) and zeta potential measurements, the iron oxide particles were found to be completely covered by a silica coating layer. X-ray photoelectron spectroscopy (XPS) and X-ray diffraction (XRD) measurements revealed that the iron oxide core consists of ${\gamma}-Fe_2O_3$ rather than ${\alpha}-Fe_2O_3$. Our magnetization measurements support this conclusion. Biocompatibility test of the silica-coated iron oxide nanoparticles is also conducted using the protein adsorption onto the coated particle.

• 한국전기전자재료학회:학술대회논문집
• /
• 한국전기전자재료학회 1998년도 추계학술대회 논문집
• /
• pp.93-96
• /
• 1998

The X-ray spectra dependence for intensifying screens of medical radiography was investigated through analysis of the absorbed coefficiency(${\mu}$), absorbed efficiency(η$\sub$${\alpha}$/) and absorbed ratio(R). It was found that the absorbed coefficiency was increased in the order of CaWO$_4$$_4$ screen showed the highest value.

• 대한전기학회:학술대회논문집
• /
• 대한전기학회 1998년도 추계학술대회 논문집 학회본부 C
• /
• pp.825-828
• /
• 1998

The X-ray spectra dependence for intensifying screens of medical radiography was investigated through analysis of the absorbed coefficiency($\mu$), absorbed efficiency(${\eta}_{\alpha}$) and absorbed ratio(R). It was found that the absorbed coefficiency was increased in the order of $CaWO_4$$CaWO_4$ screen showed the highest value.

• 천문학회보
• /
• 제41권1호
• /
• pp.38.1-38.1
• /
• 2016

Gamma ray burst, the most brightest explosion phenomena in the current universe is well suited for study of high redshift universe. We report the afterglow multi-wavelength observation and GTC spectroscopy follow up of GRB 140304A which was exploded at z=5.283. The spectrum was shown damped Lyman alpha features and a series of absorption lines S, Si, SiII*, Oi, CII, CII*, SiIV are clearly detected at common redshift. Clear optical flares are detected when X-ray flare happened and a possible gamma-ray excess also. At this conference, we report on implications for the GRB host and environments using its absorption features which place the results in context to other well studied high redshift GRBs and studies about the ejecta using its observed flaring activities.

• 한국분말야금학회:학술대회논문집
• /
• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
• /
• pp.472-473
• /
• 2006

Maghemite and hematite nanospheres were synthesized by using the Sol-gel technique. The structural properties of these nanosphere powders were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), field emission scanning electron microscopy (FESEM), and pore size distribution. Hematite phase shows crystalline structures. The mean particle size that resulted from BET and XRD analyses were 4.9 nm and 2 nm. It can be seen from transmission electron microscopy that the size of the particles are very small which is in good agreement with the FESEM and the X-ray diffraction. The BET and pore size method were employed for specific surface area determination.