• Nuclear Engineering and Technology
• /
• v.46 no.3
• /
• pp.413-422
• /
• 2014

Presented in this study are the variations of microstructures and mechanical properties with tempering and Post-Weld Heat Treatment (PWHT) conditions for SA508 Gr.4N steel used as Reactor Pressure Vessel (RPV) material. The blocks of model alloy were austenitized at the conventional temperature of $880^{\circ}C$ then tempered and post-weld heat treated at four different conditions. The hardness and yield strength decrease with increased tempering and PWHT temperatures, but impact toughness is significantly improved, especially in the specimens tempered at $630^{\circ}C$. The sample tempered at $630^{\circ}C$ with PWHT at $610^{\circ}C$ shows optimum mechanical properties in hardness, strength, and toughness, excluding only the transition property in the low temperature region. The microstructural observation and quantitative analysis of carbide size distribution show that the variations of mechanical properties are caused by the under-tempering and carbide coarsening which occurred during the heat treatment process. The introduction of PWHT results in the deterioration of the ductile-brittle transition property by an increase of coarse carbides controlling cleavage initiation, especially in the tempered state at $630^{\circ}C$.

• Proceedings of the Korean Society for Technology of Plasticity Conference
• /
• 2006.05a
• /
• pp.63-66
• /
• 2006

The effect of warm rolling under various conditions on the microstructure and mechanical property was investigated using an AZ31 Mg alloy sheet. Several processing parameters such as initial thickness, thickness reduction by a single pass rolling, rolling temperature, roll speed, and roll temperature were varied to elicit an optimum condition for the warm rolling process of AZ31 Mg alloy. Microstructure and mechanical properties were measured for specimens subjected to rolling experiments of various conditions. Warm rolling of 30% thickness reduction per pass was possible without any side-crack at temperatures as low as $200^{\circ}C$ under the roll speed of 30 m/min. The initial microstructure before rolling was the mixed one consisting of partially recrystallized and cast structures. Grain refinement was found to occur actively during the warm rolling, producing a very fine grain size of 7 mm after 50% reduction in single pass rolling at $200^{\circ}C$. Yield strength of 204MPa, tensile strength of 330MPa and uniform elongation of 32% have been obtained in warm rolled sheets.

• Culinary science and hospitality research
• /
• v.23 no.8
• /
• pp.90-97
• /
• 2017

This study investigated optimal extraction conditions for application of Hippophae rhamnoides leaves as a natural antioxidant. Hippophae rhamnoides leaves were extracted using ethanol at various concentrations (0, 30, 50, and 70%) and extraction times (4, 8, and 12 hrs) at $70^{\circ}C$ and then evaluated for extraction yield (22.51%), total phenolic contents (84.21~149.25 mg/g), total flavonoid contents (63.10~124.14 mg/g), as well as antioxidant activities DPPH, ABTS radical scavenging activity, reducing power, and FRAP. Antioxidant activities (DPPH, ABTS radical scavenging activity, reducing power) were correlated with total phenolic and flavonoid contents. 70% EtOH extracts for 12 h at $70^{\circ}C$ showed the highest total phenolic and flavonoid contents with strong antioxidant activities, and that the leaves of Hippophae rhamnoides could be considerd as a candidate of new functional antioxidant agents. This extract could be a good source for natural antioxidants and good health food. This work offers would be useful for chemical and biological studies of natural plants and its products.

• Proceedings of the Korea Concrete Institute Conference
• /
• 2000.10a
• /
• pp.617-622
• /
• 2000

In this study, effective compressive strength and nodal zone of Strut-and-Tie Model are studied to propose a new design method for RC T-type pier coping for prevention of sudden brittle failure. The coping which transmits loads of bridge to pier should be properly designed to retain ductile behavior. In order to carry out this proper design using STM, tie must yield before concrete fails, and a stress at strut should not exceed a certain effective stress. Therefore, reasonable determination of the effective compressive strength of strut by considering stress states at the nodal zone exactly is very important. Since conventional STM is applied under assumption that all nodes are under hydrostatic stress state, actual non-hydrostatic stress state in nodal zone caused by geometrical characteristics, loading conditions, support conditions of structures can not be considered properly. In order to apply STM for design of RC T-type pier coping, the non-hydrostatic stress state of nodal zone is considered and effective compressive strength is proposed. Then, a new design method of RC T-type pier coping which applies the principle of superposition to obtain optimum ductile behavior is rationally designed.

• Journal of the Korean Ceramic Society
• /
• v.33 no.12
• /
• pp.1387-1393
• /
• 1996

A study on mesophase pitch as a matrix precursor of carbon fiber reinforced carbon (C/C) composite has been recently presented. This study is concerned with the production of mesophase pitch as matrix precursors for C/C composite from coal tar pitch. A commercial coal tar pitch was heat-treated at 25$0^{\circ}C$ for 2 hours to remove low molecular weight fraction from the pitch then increasing the temperature of the pitch to between 350~45$0^{\circ}C$ to produce mesophase pitch. The pitch was continuously stirred during this time and nitrogen gas was continuously bubbled through the pitch. Spherical and bulk mesophases were formed in the pitch after heat-treatment,. Parent and mesophae pitches were characterized by elemental analysis coke yield solubi-lity in tetrahydrofuran and hexane and an optical microscopy to measure the mesiophase content. It was neces-sary to produce C/C composite that a mesophase pitch with about 30-40 vol% mesophase spherulites can be infiltrated into a fiber preform without a filter effect as a matrix precursor conditions. This condition was satisfied with mesophase pitch heat treated at 40$0^{\circ}C$ for 2 hours. The other heat treatment conditions showed the nuclei of mesophase or bulk mesophae which were not satisfied with the matix precursor condition.

• Journal of the Korean Society of Food Science and Nutrition
• /
• v.30 no.3
• /
• pp.455-459
• /
• 2001

Tofu (soybean curd) was made with whole soybean flour (WSF, 420 mesh) by various processing conditions of water addition ratio, heating time, coagulation temperature, molding pressure and 0.3% of mixed coagulant (CaSO₄:GDL=50:50(w/w)). Yield content of WSF-tofu was the highest in processing condition of 85℃ coagulation temperature, 10 times water addition, 5min. heating time and 25.00 g/㎠ molding pressure. As the increase of the water addition ratio from 8 to 14 times (water:WSF, v/w), Hunter's L and a values were increased. Raising of heating time (100℃, 1, 5, 10 and 15 min), a and b value were increased. Textural properties of WSF-tofu were significantly affected by coagulation temperature (75, 80, 85 and 90℃). Hardness was increased, but adhesiveness and cohesiveness were decreased. heating time was influenced on harness of WSF-tofu, but water addition ratio was not affected on hardness of WSF-tofu. Increasing of molding pressure (16.83, 25.00, 33.22 and 41.67 g/㎠, 1 hr) was resulted from a increased hardness, gumminess and chewingss of tofu, but adhesiveness was addition ratio, 5 min heating time and 25.00 g/㎠ molding pressure recorded the highest score in sensory evaluation test.

• KSBB Journal
• /
• v.9 no.1
• /
• pp.35-39
• /
• 1994

Separation of pure fructo-oligosaccharides from the mixed solution of glucose, sucrose and fructo-oligosaccharides was studied using a cationic ion-exchange resin column. Optimum separation conditions, i.e., temperature, feeding rate and the ratio of column vs. diameter were evaluated, which were found to be $85^{\circ}C$, $0.25h^{-1}$ and 30, respectively. At the optimized separation conditions, high-purity fructo-oligosaccharides up to 96% were obtained and the total recovery yield was about 66% after four cycles. After the chromatographic separation, purification to remove the salts and color in pure fructo-oligosaccharides solution was successfully conducted using the mixed-bed of cationic and anionic ionexchange resin columns.

• KSBB Journal
• /
• v.10 no.2
• /
• pp.159-165
• /
• 1995

Methyl fructoside was continuously produced in suspended bed enzyme reactor using alginate-enclosed microspheres biocatalyst which was developed for enzymatic synthesis of methyl fructoside. And the continuous operating conditions were optimized with reactor simulation in order to demonstrate a feasibility of commercialization of the continuous enzymatic production process development. The yield and productivity of methyl fructoside were as high as 47.1%o and $2g/\ell$-hr, respectively. The optimum operating conditions were pH 4.8, 30%(v/v) of methanol content and $2U/m\ell$ of enzyme activity when the initial concentration of sucrose is $0.291mo1/\ell$ at the reaction temperature of $25^{\circ}C$.

• Biotechnology and Bioprocess Engineering:BBE
• /
• v.6 no.5
• /
• pp.341-346
• /
• 2001

For the purpose of mass producing Monascus red pigments optimum medium composition and environmental conditions were investigated in submerged flask cultures. The optimum carbon and nitrogen sources were determined to be 30g/L of glucose and 1.5 g/L of monosodium glutamate (MSG). Of the three metals examined, Fe$\^$2+/ showed the strongest stimulatory effect on pigment production and some stimulatory effect was also found in Mn$\^$2+/. Optimum pH and agitation speed were determined to be 6.5 and 700 rpm, respectively. Under the optimum culture conditions batch fermentation showed that the maximum biomass yield and specific productivity of red pigments were 0.20 g DCW/g glucose and, 32.5 OD$\sub$500/g DCW$\^$-1/h$\^$-1/, respectively.

• Transactions of the Korean Society of Mechanical Engineers A
• /
• v.30 no.5 s.248
• /
• pp.543-549
• /
• 2006

The bursting properties under various conditions were investigated to ascertain the optimum conditions to yield the best properties. Fiber aspect ratio (AR: length of fiber/diameter of fiber), interphase condition and fiber content were considered as variables which impact the bursting pressure, bulge constant, torsional rigidity ratio. The bursting pressure of reinforced rubber increases up to 8.73 times compared to the virgin material. The better interphase condition shows the higher bursting pressure at given AR and fiber content. The bulge constant and torsional rigidity highly decrease with increasing AR and better interphase condition at same fiber content. The bulge constant and torsional rigidity reveal the minimum of 11% and 0.6% of the matrix, respectively. The bursted shape after test shows the different patterns between unfilled and reinforced rubbers. The case of virgin rubber shows a radiating shape while that of reinforced rubber shows a fluctuating straight line. Overall, it was found that the fiber AR and interphase condition have an important effect on bursting properties.