• Korean Journal of Metals and Materials
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• v.48 no.1
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• pp.39-48
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• 2010

In order to investigate the effects of tempering temperature and heat-treatment path on the microstructural and mechanical properties of ASTM Gr.92 steels, four samples with different tempering temperatures and heat-treatment paths wer prepared. THeree experimental steels showed tempered martensitic microstructures, but the sample tempered at $810^{\circ}C$ was presumed to retain partially untempered martensitic microstructures due to a lower ${\alpha}$+${\gamma}$ phase regime. $M_{23}C_6$, V(C,N), and Nb(C,N) precipitates were observed in all samples. In addition $Cr_2N$ was observed to be precipitated finely and uniformly by isothermal heat-treatment. The lath width and precipitate size in the isothermal heat-treated samples were much smaller than those of the tempered-only specimens. Because of a fine and uniform precipitate, a reduction of lath width would enhance precipitation hardeing, and it was shown that mechanical propertiesincluding the hardness and tensile properties of the steels were improved by isothermal heat-treatment.

• Korean Journal of Metals and Materials
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• v.49 no.6
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• pp.505-513
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• 2011

A magnetic device which enables the application of a strong and uniform magnetic field to thin film during sputtering was designed for controlling the magnetic anisotropy using a three dimensional finite element method, and the effects of the external magnetic field on the magnetic properties of sputtered thin films were investigated. Both the intensity and the uniformity of the magnetic flux density in the sputter zone (50 mm ${\times}$50 mm) was dependent on not only the shape and size of the magnet device but also the magnitude of stray fields from the magnet. For the magnet device in which the distance between two magnets or two pure iron bars was 80-90 mm, the magnetic flux density along the direction normal to the external magnetic field direction was minimum. The two row magnets increased the magnetic flux density and uniformity along the external magnetic field direction. An Fe thin film sputtered using the optimized magnet device showed a higher remanence ratio than that fabricated under no external magnetic field.

• Journal of Powder Materials
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• v.28 no.2
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• pp.110-119
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• 2021

In this study, the high-temperature oxidation properties of austenitic 316L stainless steel manufactured by laser powder bed fusion (LPBF) is investigated and compared with conventional 316L manufactured by hot rolling (HR). The initial microstructure of LPBF-SS316L exhibits a molten pool ~100 ㎛ in size and grains grown along the building direction. Isotropic grains (~35 ㎛) are detected in the HR-SS316L. In high-temperature oxidation tests performed at 700℃ and 900℃, LPBF-SS316L demonstrates slightly superior high-temperature oxidation resistance compared to HR-SS316L. After the initial oxidation at 700℃, shown as an increase in weight, almost no further oxidation is observed for both materials. At 900℃, the oxidation weight displays a parabolic trend and both materials exhibit similar behavior. However, at 1100℃, LPBF-SS316L oxidizes in a parabolic manner, but HR-SS316L shows a breakaway oxidation behavior. The oxide layers of LPBF-SS316L and HR-SS316L are mainly composed of Cr₂O₃, Fe-based oxides, and spinel phases. In LPBF-SS316L, a uniform Cr depletion region is observed, whereas a Cr depletion region appears at the grain boundary in HR-SS316L. It is evident from the results that the microstructure and the high-temperature oxidation characteristics and behavior are related.

• Korean Chemical Engineering Research
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• v.60 no.1
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• pp.139-144
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• 2022

This study reports a microfluidic approach to produce monodisperse hydrogel microparticles in a simple and highly efficient manner. Specifically, we produce double emulsion drops with a thin oil shell surrounding an aqueous prepolymer solution, which is solidified via UV-induced free radical polymerization. When they are dispersed in an aqueous solution, the oil shell is dewetted due to the absence of surfactants, resulting in production of highly uniform hydrogel microparticles (C.V.=1%). Results show that production of monodisperse hydrogel microparticles with controllable size and composition can be achieved with minimal use of oil unlike water-in-oil (w/o) single emulsion-based approach. Furthermore, in-depth study of flow patterns in microfluidic device using a phase diagram exhibits a crucial relationship among relative flow rates while providing windows of readily controllable parameters for reliable manufacturing of hydrogel microparticles.

• Journal of the Korean Society of Safety
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• v.37 no.1
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• pp.1-11
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• 2022

This numerical study investigates the effects of the size of the natural smoke vent area (10% and 1% of the floor area) and the location of the fire source (i.e., at the side and center of the stage) on the temperature distribution in the compartment and velocity distribution and mass flow rate of flow through a natural smoke vent for a reduced-scale model of a theater stage. Then, the mass flow rate of outflow through the natural smoke vent in the event of a fire for a real-scale theater stage was examined. The case with the larger natural smoke vent area and central fire source location showed lower temperature distributions and higher mass flow rates of outflow and inflow than the case with the smaller natural smoke vent area and side fire source location. The trends of the temperature distributions were closely related to those of the mass flow rates for the outflow and inflow. Additionally, the case with the larger natural smoke vent area and central fire source location exhibited the most non-uniform flow velocity distribution in all cases tested. A bidirectional flow, in which the outflow and inflow occur simultaneously, was observed through the natural smoke vent. In the event of a fire situation in a real-scale theater stage, it was predicted that the case with the larger natural smoke vent area and central fire source location would have a mass flow rate of outflow that is 43.53 times higher than that of the case with the smaller natural smoke vent area and side fire source location. The present results indicate that the natural smoke vent location should be determined by considering the location in a theater stage where a fire can occur.

• Journal of Electrochemical Science and Technology
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• v.12 no.4
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• pp.458-464
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• 2021

Lithium ion batteries (LIBs) is a kind of rechargeable secondary battery, developed from lithium battery, lithium ions move between the positive and negative electrodes to realize the charging and discharging of external circuits. Zeolitic imidazolate frameworks (ZIFs) are porous crystalline materials in which organic imidazole esters are cross-linked to transition metals to form a framework structure. In this article, ZIF-67 is used as a sacrificial template to prepare nano porous carbon (NPC) coated cobalt nanoparticles. The final product Co/NPC composites with complete structure, regular morphology and uniform size were obtained by this method. The conductive network of cobalt and nitrogen doped carbon can shorten the lithium ion transport path and present high conductivity. In addition, amorphous carbon has more pores that can be fully in contact with the electrolyte during charging and discharging. At the same time, it also reduces the volume expansion during the cycle and slows down the rate of capacity attenuation caused by structure collapse. Co/NPC composites first discharge specific capacity up to 3115 mA h/g, under the current density of 200 mA/g, circular 200 reversible capacity as high as 751.1 mA h/g, and the excellent rate and resistance performance. The experimental results show that the Co/NPC composite material improves the electrical conductivity and electrochemical properties of the electrode. The cobalt based ZIF-67 as the precursor has opened the way for the design of highly performance electrodes for energy storage and electrochemical catalysis.

• Tribology and Lubricants
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• v.38 no.3
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• pp.93-100
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• 2022

Micro-light emitting diode (micro-LED) displays offer numerous advantages such as high brightness, fast response, and low power consumption. Hence, they are spotlighted as the next-generation display. However, defective LEDs may be created due to non-uniform contact loads or LED alignment errors. Therefore, a repair process involving the replacement of defective LEDs with favorable ones is necessitated. The general repair process involves the removal of defective micro-LEDs, interconnection material transfer, as well as new micro-LED transfer and bonding. However, micro-LEDs are difficult to repair since their size decreases to a few tens of micron in width and less than 10 ㎛ in thickness. The conventional nozzle-type dispenser for fluxes and the conventional vacuum chuck for LEDs are not applicable to the micro-LED repair process. In this study, transfer conditions are determined using a micro stamp for repairing micro-LEDs. Results show that the aging time should be set to within 60 min, based on measuring the aging time of the flux. Additionally, the micro-LEDs are subjected to a compression test, and the result shows that they should be transferred under 18.4 MPa. Finally, the I-V curves of micro-LEDs processed by the laser and hot plate reflows are measured to compare the electrical properties of the micro-LEDs based on the reflow methods. It was confirmed that the micro-LEDs processed by the laser reflow show similar electrical performance with that processed by the hot plate reflow. The results can provide guidance for the repair of micro-LEDs using micro stamps.

• Textile Coloration and Finishing
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• v.34 no.1
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• pp.20-26
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• 2022

Centrifugal spinning is an emerging technique for fabricating micro-to-nano-fibers in recent years. To obtain fibers with the desired size and morphology, it is necessary to configure and optimize the parameters used in centrifugal spinning. In this study, it was controlled by changing the solution's concentration (7.5, 10, and 12.5 wt.%) and disk's rotational velocity (6,000, 8,000, and 10,000 rpm) to prepare centrifugal spun nano-filter. The morphological property, air permeability, and dust collection efficiency of the PVA/PP bi-layer nanoweb prepared by centrifugal spun PVA on the PP micron nonwoven substrate are studied using a field emission scanning electron microscope, an air permeability tester, and a filter tester equipment, and the analysis results indicate that it is suitable as a nano-filter when the concentration of PVA solution is 10 wt.% and the rotational velocity of the disk is 8,000 rpm. The resultant reduced diameter and uniform fibers also proved that an excellent dust collection efficiency filter could be made.

• Industry Promotion Research
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• v.7 no.1
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• pp.9-15
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• 2022

This study tried to analyze the growth background of Starbucks, a competitive company in the Korean coffee industry. Therefore, by using the STEEP analysis technique, each company's competitiveness was analyzed and the results were used to derive competitive factors. And the research results are as follows. Looking at the social aspect, economic activity has been a catalyst for women as the standard of living has increased due to economic growth. In addition, in the case of coffee culture in the past, Starbucks' response strategy, which has seen the transformation from vending machine mixed coffee culture to a consumer market that emphasizes cultural and spatial aspects, was effective. Looking at the technical aspect, the deviation has been reduced by securing uniform standardization of the taste of coffee beans at franchise stores, and the operation of a standardized operating system was possible by operating the store directly. And looking at the economic aspect, as the coffee consumption market continues to expand, the overall size of the market has also grown proportionally, creating a stable growth environment. Lastly, looking at the environmental and policy aspects, it is that the marketing strategy direction based on the policy activities as an eco-friendly company as a market leader has been the main focus of the recent policy direction emphasizing eco-friendliness.

• Corrosion Science and Technology
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• v.21 no.2
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• pp.130-137
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• 2022

In this work, the degradation of high-pressure superheater tubes exposed to the flame of a duct burner in a heat recovery steam generator of a district heating system was evaluated. To assess the deterioration of the used superheater tube, the microstructure, microhardness, and tensile properties were investigated by comparison to an unused tube. The study found that a fin bound at the outer surface of the used tube became fragile only in the location facing the flame. This indicates that the tube was directly exposed to the flame from the duct burner or underwent abnormal overheating. While the unused tube showed a uniform value in hardness and equiaxial grain structure, the used tube revealed a decrease in hardness up to 105 HV and an increase in grain size with a plate-like morphology in the location facing the flame. The coarsening of the grain structure by the flame weakened the mechanical properties of yield strength, tensile strength, and elongation.