dos Santos, Victor Hugo;Griza, Sandro;de Moraes, Rafael Ratto;Faria-e-Silva, Andre Luis
Restorative Dentistry and Endodontics
/
v.39
no.1
/
pp.12-16
/
2014
Objectives: Extensively destroyed teeth are commonly restored with composite resin before cavity preparation for indirect restorations. The longevity of the restoration can be related to the proper bonding of the resin cement to the composite. This study aimed to evaluate the microshear bond strength of two self-adhesive resin cements to composite resin. Material and Methods: Composite discs were subject to one of six different surface pretreatments: none (control), 35% phosphoric acid etching for 30 seconds (PA), application of silane (silane), PA + silane, PA + adhesive, or PA + silane + adhesive (n = 6). A silicone mold containing a cylindrical orifice ($1mm^2$ diameter) was placed over the composite resin. RelyX Unicem (3M ESPE) or BisCem (Bisco Inc.) self-adhesive resin cement was inserted into the orifices and light-cured. Self-adhesive cement cylinders were submitted to shear loading. Data were analyzed by two-way ANOVA and Tukey's test (p < 0.05). Results: Independent of the cement used, the PA + Silane + Adhesive group showed higher microshear bond strength than those of the PA and PA + Silane groups. There was no difference among the other treatments. Unicem presented higher bond strength than BisCem for all experimental conditions. Conclusions: Pretreatments of the composite resin surface might have an effect on the bond strength of self-adhesive resin cements to this substrate.
This study aimed to illuminate the correlatives between the surface processing of Zirconia core and the shear bond strength. The specimens were made by precipitating for two minutes in color liquid and drying to produce a colored Zirconia core following the manufacturer's instructions. The specimens were divided into 4 subgroups according to the surface treatment-sandblasted+liner treatment, SLT group; sandblasted treatment, ST group; liner treatment, LT group; non treatment (control), NT group. The specimens were put on the device with regard to ISO/TS 11405, then tested the shear bond strength with 1 mm shearing speed per minute using the Instron multi-purpose tester. The collected data was analysed by one way ANOVA and t-test. After applying the liner and sandblast to the Zirconia core, shear bond strength value were SLT (23.19 MPa), ST (21.17 MPa), LT (20.53 MPa) and NT (16.46 MPa) in the order. There was a significant difference in the surface roughness between NT and ST group (p<0.001), and in the compressive shear bond strength between NT and SLT group (p<0.05). Therefore, sandblasted plus liner treatment on pre-sintered substructure increased the bond strength of veneering ceramic, compared with other surface treatments.
The problem of reducing the self-weight of reinforced concrete structures is very important issue. There are two approaches which may be used to reduced member weight. The first is tackled through reducing the cross sectional area by using voids and the second through using light weight materials. Reducing the weight of slabs is very important as it constitutes the effective portion of dead loads in the structural building. Eleven slab specimens was casted in this research. The slabs are made one way though using two simple supports. The tested specimens comprised three reference solid slabs and eight styropor block slabs having (23% and 29%) reduction in weight. The voids in slabs were made using styropor at the ineffective concrete zones in resisting the tensile stresses. All slab specimens have the dimensions ($1100{\times}600{\times}120mm$) except one solid specimens has depth 85 mm (to give reduction in weight of 29% which is equal to the styropor block slab reduction). Two loading positions or cases (A and B) (as two-line monotonic loads) with shear span to effective depth ratio of (a/d=3, 2) respectively, were used to trace the structural behavior of styropor block slab. The best results are obtained for styropor block slab strengthened by minimum shear reinforcement with weight reduction of (29%). The increase in the strength capacity was (8.6% and 5.7%) compared to the solid slabs under loading cases A and B respectively. Despite the appearance of cracks in styropor block slab with loads lesser than those in the solid slab, the development and width of cracks in styropor block slab is significantly restricted as a result of presence a mesh of reinforcement in upper concrete portion.
PURPOSE. The purpose of this study was to investigate the impact of different surface treatment methods and thermal ageing on the bond strength of autopolymerizing acrylic resin to Co-Cr. MATERIALS AND METHODS. Co-Cr alloy specimens were divided into five groups according to the surface conditioning methods. C: No treatment; SP: flamed with the Silano-Pen device; K: airborne particle abrasion with $Al_2O_3$; Co: airborne particle abrasion with silica-coated $Al_2O_3$; KSP: flamed with the Silano-Pen device after the group K experimental protocol. Then, autopolymerized acrylic resin was applied to the treated specimen surfaces. All the groups were divided into two subgroups with the thermal cycle and water storage to determine the durability of the bond. The bond strength test was applied in an universal test machine and treated Co-Cr alloys were analyzed by scanning electron microscope (SEM). Two-way analysis of variance (ANOVA) was used to determine the significant differences among surface treatments and thermocycling. Their interactons were followed by a multiple comparison' test performed uing a post hoc Tukey HSD test (${\alpha}=.05$). RESULTS. Surface treatments significantly increased repair strengths of repair resin to Co-Cr alloy. The repair strengths of Group K, and Co significantly decreased after 6,000 cycles (P<.001). CONCLUSION. Thermocycling lead to a significant decrease in shear bond strength for air abrasion with silica-coated aluminum oxide particles. On the contrary, flaming with Silano-Pen did not cause a significant reduction in adhesion after thermocycling.
Kim, Lyang-Woon;Chung, Chang-Yong;Lee, Soo-Kueon;Kim, Sang-Sik;Choi, Kwang-Ho;Lee, Jung-Yoon
Proceedings of the Korea Concrete Institute Conference
/
2008.04a
/
pp.209-212
/
2008
DBS method of underground works can reduce the term of works for manufacturing the underground members in factory and producing members in modularization, apart from that, the horizontal member could be used as permanent members, which are the advantages of this method. As the component element of DBS method, in order th transfer the vertical load on horizontal member to the column during the construction or in service, developed ${\sharp}$ shaped double beam-column connection is dominated by shear failure in the complicated state of multi-axial stresses. In this study, in order to check the shear-failure mechanism of ${\sharp}$ shaped connection of double beam-column and an increase of shear internal force with the thickness of the steel plate. 7 specimens were made and one-way static tests. All of the specimens were subjected to brittle failure. Constraint of slab will increase its shear strength by 1.06${\sim}$1.48 times. Shear strength of slabs with different constraints steel plate in two-way increase more than which are same. So the slab with different constraints steel plate will be more effective.
Yang, Jun Mo;Shin, Hyun Oh;Lee, Joo Ha;Yoon, Young Soo
Journal of the Korea institute for structural maintenance and inspection
/
v.15
no.2
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pp.161-169
/
2011
Two-way slabs reinforced with high-performance steels, which have several practical advantages of a reduction of congestion in heavily reinforced members, savings in the cost of labor and repair, the higher corrosion resistance, and a reduction of construction time, were constructed and tested. The influences of the flexural reinforcement ratio, concentrating the reinforcement in the immediate column region, and using steel fiber-reinforced concrete (SFRC) in the slab on the punching shear resistance and post-cracking stiffness were investigated, and compared with the punching shear test results of the slabs reinforced with conventional steels and GFRP bars. In addition, the strain distribution of flexural reinforcements and crack control were investigated, and the effective width calculating method for the average flexural reinforcement ratio was estimated. The use of high-performance steel reinforcement increased the punching shear strength of slabs, and decreased the amount of flexural reinforcements. The concentrating the top mat of flexural reinforcement increased the post-cracking stiffness, and showed better strain distribution and crack control. In addition, the use of SFRC showed beneficial effects on the punching shear strength and crack control. It was suggest that the effective width should be changed to larger than 2 times the slab thickness from the column faces.
Kim, Dong-Hwan;Bae, Ji-Hyun;Cho, Byeong-Hoon;Lee, In-Bog;Baek, Seung-Ho;Ryu, Hyun-Mi;Son, Ho-Hyun;Um, Chung-Moon;Kwon, Hyuck-Choon
Restorative Dentistry and Endodontics
/
v.29
no.2
/
pp.170-176
/
2004
Objectives : In the unique metal iris method. the developing interfacial gap at the cavity floor resulting from the cavity wall property during polymerizing composite resin might affect the nominal shear bond strength values. The aim of this study is to evaluate that the iris method reduces the cohesive failure in the substrates and the cavity wall property effects on the shear bond strength tests using iris method. Materials and Methods : The occlusal dentin of 64 extracted human molars were randomly divided into 4 groups to simulate two different levels of cavity wall property (metal and dentin iris) and two different materials ($ONE-STEP^{\circledR}$ and $ALL-BOND^{\circledR}$ 2) for each wall property. After positioning the iris on the dentin surface. composite resin was packed and light-cured. After 24 hours the shear bond strength was measured at a crosshead speed of 0.5 mm/min. Fracture analysis was performed using a microscope and SEM. The data was analyzed statistically by a two-way ANOV A and t-test. Results : The shear bond strength with metal iris was significant higher than those with dentin iris (p=0.034). Using $ONE-STEP^{\circledR}$, the shear bond strength with metal iris was significant higher than those with dentin iris (p=0.005), but not in $ALL-BOND^{\circledR}$ 2 (p=0.774). The incidence of cohesive failure was very lower than other shear bond strength tests that did not use iris method. Conclusions:The iris method may significantly reduce the cohesive failures in the substrates. According to the bonding agent systems. the shear bond strength was affected by the cavity wall property.
Park, Sang-Hoon;Suk, Chang-Mok;Jung, Hwan-Mok;Kwon, Young-Hwan
Journal of Korean Association for Spatial Structures
/
v.2
no.1
s.3
/
pp.85-92
/
2002
Two way grid single-layer domes are of great advantage in fabrication and construction because of the simple fact that they have only four members at each junction. But, from a point of view of mechanics, the rectangular latticed pattern gives rise to a nonuniform rigidity-distribution in the circumferential direction. If the equivalent rigidity is considered in the axial direction of members, the in-plane equivalent shearing rigidity depends only on the in-plane bending rigidity of members and its value is very small in comparison to that of the in-plane equivalent stretching rigidity. It has a tendency to decrease buckling -strength of dome considerably by external force. But it is possible to increase buckling strength by the use of roofing covering materials connected to framework. In a case like this, shearing rigidity of roofing material increases buckling strength of the overall structure and can be designed economically from the viewpoint of practice. Therefore, the purpose of this paper, in Lamella dome and rectangular latticed dome that are a set of 2-way grid dome, is to clarify the effects of roofing covering materials for increasing of buckling strength of overall dome. Analysis method is based on FEM dealing with the geometrically nonlinear deflection problems. The conclusion were given as follows: 1. In case of Lamella domes which have nearly equal rigidity in the direction of circumference, the rigidity of roofing covering materials does not have a great influence on buckling-strength, but in rectangular latticed domes that has a clear periodicity of rigidity, the value of its buckling strength has a tendency to increase considerably with increasing rigidity of roofing covering materials 2. In case of rectangular latticed domes, as rise-span-ratio increases, models which is subjected to pressure -type-uniform loading than vertical-type-uniform loading are higher in the aspects of the increasing rate of buckling- strength according to the rate of shear reinforcement rigidity, but in case of Lamella dome, the condition of loading and rise-span-ratio do not have a great influence on the increasing rate of buckling strength according to the rate of shear reinforcement rigidity.
Statement of problem. The aims of the study were to evaluate the effect of current surface conditioning methods on the bond strength of a resin composite luting cement bonded to ceramic surfaces and to identify the optimum cement type. Material and methods. The sixty zirconia ceramic specimens(10 per group) with EVEREST milling machine and 60 tooth block were made. The zirconia ceramic surface was divided into two groups according to surface treatment: (1) airborne abrasion with $110{\mu}m$ aluminum oxide particles; (2) Rocatec system, tribochemical silica coating. The zirconia ceramic specimens were cemented to tooth block using resin cements. The tested resin cements were Rely X ARC, Panavia F and Superbond C&B. Each specimen was mount in a jig of the universal testing machine for shear strength. The results were subjected to 2-way ANOVA and Post hoc tests was performed using Tukey, Scheffe, and Bonferroni test. Results. The mean value of shear bond strength(MPa) were as follows: $$RelyXARC(+Al_2O_3),5.35{\pm}1.69$$; $$RelyXARC(+Rocatec),8.50{\pm}2.13$$; $$PanaviaF(+Al_2O_3),9.58{\pm}1.13$$; $$PanaviaF(+Rocatec),12.98{\pm}1.71$$; $$SuperbondC&B(+Al_2O_3)8.27{\pm}2.04$$; $$SuperbondC&B(+Rocatec),14.46{\pm}2.39$$. There was a significant increase in the shear bond strength when the ceramic surface was subjected to the tribochemical treatment(Rocatec 3M) in all cement groups(P<0.05). Bonding strengths of cements applied to samples treated with $Al_2O_3$ were compared; Rely X ARC showed the lowest values, whereas Panavia F cement showed higher value than that of Superbond C&B group with no statistical significance. When the bond strength of cements with of Rocatec treatment was compared, Rely X ARC showed lowest values. Overall, it was apparent that tribochemical treated Super-Bond possessed higher mean bond strength (14.46MPa; P<0.05) than that of Panavia F cement group with no significance. Conclusions. Silica coating followed silanization(Rocatec treatment) increase the bond strength between resin cement and zirconia ceramic. Panavia F containing phosphate monomer and Superbond C&B comprised of 4-META tend to bond chemically with zirconia ceramic, thus demonstrating higher bond strength compared to BisGMA resin cement. Superbond C&B has shown to have highest value of bonding strength to zirconia ceramic after Rocatec treatment compared to other cement.
Seul-Gi, Yi;Jin-Woo, Kim;Se-Hee, Park;Yoon, Lee;Eung-Hyun, Kim;Kyung-Mo, Cho
Journal of Dental Rehabilitation and Applied Science
/
v.38
no.4
/
pp.189-195
/
2022
Purpose: For orthodontic bracket bonding, light curing resin cement is widely used because the process is convenient, and it can be polymerized at the desired time. This study compared the difference of bonding strength of orthodontic resin cement according to storage condition. Materials and Methods: After acid etching the bovine enamel surface with 37% phosphoric acid, 15 orthodontic brackets for mandible incisors were bonded with Ortho Connect and Orthomite LC according to following three conditions; 1) Immediate after 4℃ refrigeration for 3 months (IR), 2) One day room temperature after 4℃ refrigeration for 3 months (OR), 3) Room temperature for 3 months (RT). The shear bond strength was measured with a universal material tester and failure pattern of the specimen was observed. Two-way ANOVA and One-way ANOVA were used at the 95% significance level. Results: Ortho Connect that was applied immediately after refrigeration showed the maximum shear bond strength. Orthomite that was applied immediately after refrigeration showed the lowest shear bond strength, and the group stored at room temperature for three months showed the highest shear bond strength, and the difference between the two groups was significant. Conclusion: Ortho Connect can be used without worrying about bond strength even if it is used immediately after refrigeration, but Orthomite should be kept at room temperature sufficiently after refrigeration.
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