• 한국안광학회지
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• 제7권2호
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• pp.175-180
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• 2002

렌즈의 thin film 균일성을 평가하기 위하여 spctrophotometer를 이용한다. 렌즈의 중심 중간, edge 등의 지점에서 파장의존상의 반사율을 측정하여 반사율 spectrum의 두 peak를 선택하여 비교하여, 박막 균일성 여부를 분석한다. 반사율의 두 peak의 파장 영역(${\lambda}_1,{\lambda}_2$)으로부터 thin film의 thickness(t)를 구한다. $$t=\frac{1}{2(n^2-\sin^2{\theta})^{1/2}}{\times}\frac{{\lambda}_1{\lambda}_2}{{\lambda}_2-{\lambda}_1}$$ 렌즈의 중심 중간, edge 등의 지점에서 반사율 pattern이 동일 값이면 coating 렌즈의 박막은 균일성 갖는다. coating 렌즈의 박막 균일성 평가 방법을 단층막 $MgF_2$(n=1.38) coating 렌즈에 적용하였다. 박막의 thickness 차이는 360nm 정도였다. 파장의존성에 대한 광반사율의 측정으로부터 coating 렌즈의 박막 균일성을 쉽게 분석할 수 있다.

• 한국항행학회논문지
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• 제17권5호
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• pp.574-580
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• 2013

본 논문에서는 박막코팅기술의 공정은 고경도 박막과 질화층의 접합력을 높이기 위하여 적용하였다. 이 박막코팅기술은 프레스 금형에 사용되는 경도와 인성을 얻을 수 있는 복합 박막을 형성했다. 이러한 박막 코팅 생산 기술은 물리증착방법을 이용하여 진공 챔버의 진공도를 증가하고, 건파워의 투사율을 향상시켰다. 티타늄합금 타겟은 각종 정밀가공 부품에 복합박막코팅기술 개발을 통하여 성능과 표면재질을 개선하였다.

• Bulletin of the Korean Chemical Society
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• 제32권5호
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• pp.1483-1490
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• 2011

The protection effect of a $ZrO_2$ coating layer on a $LiCoO_2$ thin film was characterized. A wide and smooth $LiCoO_2$ thin film offers sufficient opportunity for careful observation of the reaction at the interface between cathode (coated and uncoated) and electrolyte. The formation of a $ZrO_2$ coating on a $LiCoO_2$ thin film was confirmed by secondary ion mass spectrometry. Scanning electron and atomic force microscopy were used to characterize the surface morphologies of coated and uncoated films before and after cycling. A $ZrO_2$-coated $LiCoO_2$ film showed a higher discharge capacity and rate capability than an uncoated film. This may be associated with a surface protection effect of the coating. The surface of a pristine film was damaged during cycling, whereas the coated film maintained a relatively clear surface under the same measurement conditions. This result clearly demonstrates the protection effect of a $ZrO_2$ coating on a $LiCoO_2$ thin film.

• 한국전기전자재료학회논문지
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• 제24권3호
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• pp.219-223
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• 2011

Rhenium-Iridium(Re-Ir) thin films were deposited onto the tungsten carbide(WC) molding core by sputtering system. The Re-Ir films were prepared by multi-target sputtering with iridium, rhenium and chromium as the sources. Argon and nitrogen were inlet into the chamber to be the plasma and reactive gases. The Re-Ir thin films were prepared with targets having atomic percent of 3:7 and the Re-Ir thin films were formed with 240 nm thickness. The Re-Ir thin films on tungsten carbide molding core were analyzed by scanning electron microscope(SEM) and surface roughness. Also, adhesion strength and coefficient friction of Re-Ir thin film were examined. The Re-Ir coating technique has been intensive efforts in the field of coating process because the coating technique and process have been their feature, like hardness, high elasticity, abrasion resistance and mechanical stability and also have been applied widely the industrial and biomedical areas. In this report, tungsten carbide(WC) molding core was manufactures using high performance precision machining and the efforts of Re-Ir coating on the surface roughness.

• 한국한의학연구원논문집
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• 제13권3호
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• pp.119-124
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• 2007

Introduction: In Oriental medicine, the status of tongue is the important indicator to diagnose one's health, because it represents physiological and clinicopathological changes of inner parts of the body. The method of tongue diagnosis is not only convenient but also non-invasive, so tongue diagnosis is most widely used in Oriental medicine. By the way, since tongue diagnosis is affected by examination circumstances a lot, its performance depends on a light source, degrees of an angle, a medical doctor's condition etc. Therefore, it is not easy to make an objective and standardized tongue diagnosis. In order to solve this problem, in this study, we tried to design a discriminant function for thick and thin coating with color vectors of preprocessed image. Method: 52 subjects, who were diagnosed as white-coated tongue, were involved. Among them, 45 subjects diagnosed as thin coating and 7 subjects diagnosed as thick coating by oriental medical doctors, and then their tongue images were obtained from a digital tongue diagnosis system. Using those acquired tongue images, we implemented two steps: Preprocessing and image analyzing. The preprocessing part of this method includes histogram equalization and histogram stretching at each color component, especially, intensity and saturation. It makes the difference between tongue substance and tongue coating was more visible, so that we can separate tongue coating easily. Next part, we analyzed the characteristic of color values and found the threshold to divide tongue area into coating area. Then, from tongue coating image, it is possible to extract the variables that were important to classify thick and thin coating. Result : By statistical analysis, two significant vectors, associated with G, were found, which were able to describe the difference between thick and thin coating very well. Using these two variables, we designed the discriminant function for coating classification and examined its performance. As a result, the overall accuracy of thick and thin coating classification was 92.3%. Discussion : From the result, we can expect that the discriminant function is applicable to other coatings in a similar way. Also, it can be used to make an objective and standardized diagnosis.

• 한국전기전자재료학회논문지
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• 제34권5호
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• pp.321-326
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• 2021

We fabricated BiAlO thin film by a solution process with a brush coating to be used as liquid crystal (LC) alignment layer. Solution-processed BiAlO was coated on the glass substrate by brush process. Prepared thin films were annealed at different temperatures of 80℃, 180℃, and 280℃. To verify whether the BiAlO film was formed properly, X-ray photoelectron spectroscopy analysis was performed on Bi and Al. Using a crystal rotation method by polarized optical microscopy, LC alignment state was evaluated. At the annealing temperature of 280℃, the uniform homogenous LC alignment was achieved. To reveal the mechanism of LC alignment by brush coating, field emission scanning electron microscope was used. Through this analysis, spin-coated and brush coated film surface were compared. It was revealed that physical anisotropy was induced by brush coating at a high annealing temperature. Particles were aligned in one direction along which brush coating was made, resulting in a physical anisotropy that affects a uniform LC alignment. Therefore, it was confirmed that brush coating combined with BiAlO thin film annealed at high temperature has a significant potential for LC alignment.

• 한국결정성장학회지
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• 제12권1호
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• pp.7-10
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• 2002

$TiO_2$ 박막을 금속유기화합물인 Titanium-naphthenate의 코팅-열분해법으로 제조하였다. 출발물질은 Ti-naphthenate를 toluene에 희석한 용액을 사용하였으며 기판은 slide glass를 사용하였다 Titanium-naphthenate 용액을 spin-coating법으로 기판에 코팅하고 $450^{\circ}C$에서 열터리하여 $TiO_2$ 박막을 제조하였다 제조한 박막의 특성을 UV/Vis, XRD 및 SEM 등으로 박막의 투과율, 굴절률, 결정상 및 표면 형상을 분석하였다. Slide glass 위에 제조한 TiO$_2$ 박막은 투과율은 70~90%이며 420nm에서의 굴절율은 2.7이었다. $TiO_2$박막은 anatase상을 나타내었고 실타래 형상의 주름을 가진 표면을 나타내었다

• 한국정밀공학회지
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• 제30권6호
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• pp.596-600
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• 2013

We report here on the processing and manufacturing of thin film for printed electronics by micro-gravure coating system. The micro-gravure coating systems are consisted of various modules such as web and system tension controller, micro-gravure coating units, dispenser and hybrid dry units (UV, NIR, Hot air). Especially, for the optimization of system, the number of idle roller was minimized and tension isolating infeeder was included. Also, we applied four patterns circle, 45 degree, square and 35 degree for the optimizing coating thickness. The micro-gravure coating system which applied various patterns to enable continuous coating process and fast coating time compare with conventional batch coating system. In this paper, introduce of micro-gravure coating system and testing results of coating thickness (20~700nm), coating time (1~2sec) and surface roughness (3~12nm) by using micro-gravure coating system.

• 한국전기전자재료학회논문지
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• 제24권10호
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• pp.812-816
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• 2011

An optical lens is usually produced in the manner of high temperature compression molding with tungsten carbide alloy molding cores, it is necessary to develop and study technology for super-precision processing of molding cores and coating the core surface. As main methods used in surface improvement technologies using thin film, DLC present high hardness, chemical stability, and outstanding durability of abrasion to be extensively applied in various industrial fields. In this study, the effect of DLC coating of a thin film by means of the FVAS (filtered vacuum arc source) analyzed the characteristics of thin film. Surface roughness before and after DLC coating was measured and the result showed that the surface roughness was improved after coating as compared to before coating. In conclusion, it was observed that DLC coating of the ultra hard alloy core surface for molding had an effect on improving the surface roughness and shape of the core surface. It is considered that this will have an effect on improving abrasion resistance and the service life of the core surface.

• Corrosion Science and Technology
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• 제22권5호
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• pp.341-350
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• 2023

In the present study, effects of a thin Zn-flash coating on hydrogen evolution, infusion, and embrittlement of advanced high strength steel during electro-galvanizing were examined. The electrochemical permeation technique in conjunction with impedance spectroscopy was employed under applied cathodic polarization. Moreover, a slow-strain rate test was conducted to evaluate loss of elongation (i.e., indicative of hydrogen embrittlement (HE)) and examine fracture surfaces. Results showed that the presence of a thin Zn-flash coating, even when it was not distributed uniformly, reduced hydrogen evolution rate and substantially impeded infusion of hydrogen into the steel substrate. This was primarily due to a hydrogen overvoltage on Zn coating and trapping of hydrogen at the interface of Zn coating/flash coating/steel substrate. Consequently, the sample with flash coating had a smaller HE index than the sample without flash coating. These results suggest that a thin Zn-flash coating could be an effective technical strategy for mitigating HE in advanced high-strength steels.