• Journal of the Korean Society for Aeronautical & Space Sciences
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• v.39 no.2
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• pp.97-105
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• 2011

This paper was conducted on analytical solution using superposition and FEM analysis in the free vibration analysis of rectangular plates under uniform thermal loadings. Materials of three rectangular plates were aluminum, steel and stainless-steel respectively. Applied temperature conditions were from room temperature to $300^{\circ}C$ and boundary condition was free-free condition. Fully symmetric mode(FSM), fully antisymmetric mode(FASM) and symmetric-antisymmetric mode(SAM) were analyzed.

• Macromolecular Research
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• v.8 no.2
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• pp.80-88
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• 2000

Biodegradable microspheres were prepared with poly(L-lactide-co-glycolide) (PLGA, 75 : 25 by mole ratio) by an oil/oil solvent evaporation method for the sustained release of anti-AIDS virus agent, AZT The microspheres of relatively narrow size distribution (7.6$\pm$ 3.8 ㎛) were obtained by controlling the fabrication conditions. The shape of microspheres prepared was smooth and spherical. The efficiency of AZT loading into the PLGA microsphere was over 93% compared to that below 15% for microspheres by a conventional water/oil/water method. The effects of Preparation conditions on the morphology and in vitro AZT release pattern were investigated. in vitro release studies showed that different release pattern and release rates could be achieved by simply modifying factors in the fabrication conditions such as the type and amount of surfactant, initial amount of loaded drug, the temperature of solvent evaporation, and so on. PLCA microspheres prepared by 5% of initial drug loading, 1.0% (w/w) of surfactant concentration, and 25$\^{C}$ of solvent evaporation temperature were free from initial burst effect and a near-zero order sustained release was observed. Possible mechanisms of the near-zero order sustained release for our system have been proposed.

• Structural Engineering and Mechanics
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• v.67 no.2
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• pp.165-173
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• 2018

A simple predicted model using a modified Shear-lag method was used to represent the moisture absorption effect on the stiffness degradation for $[0/90]_{2s}$ composite laminates with transverse cracks and under flexural loading. Good agreement is obtained by comparing the prediction model and experimental data published by Smith and Ogin (2000). The material properties of the composite are affected by the variation of temperature and moisture absorption. The transient and non-uniform moisture concentration distribution give rise to the transient elastic moduli of cracked composite laminates. The hygrothermal effect is taken into account to assess the changes in the normalised axial and flexural modulus due to transverse crack. The obtained results represent well the dependence of the stiffness properties degradation on the cracks density, moisture absorption and operational temperature. The composite laminate with transverse crack loaded in axial tension is more affected by the hygrothermal condition than the one under flexural loading. Through this theoretical study, we hope to contribute to the understanding of the moisture absorption on the composite materials with matrix cracking.

• Nano
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• v.13 no.10
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• pp.1850117.1-1850117.11
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• 2018

Sulfated $TiO_2$ nanoparticles were successfully immobilized on zeolite through improving hydrolysis-deposition method. Microstructure, crystallization, surface state and surface area of composite catalysts were characterized by SEM, XRD, FTIR spectra, XPS and BET and the photocatalytic activity was evaluated by degradation of methyl orange under UV irradiation. We optimized these factors ($SO^{2-}_4$ ions, calcination temperature and loading amount of sulfated $TiO_2$) on photocatalytic activity and crystallization of composite photocatalysts. The results indicated that the $SO^{2-}_4$ ions are successfully immobilized on the surface of $TiO_2$, and sulfated $TiO_2$/zeolite show the highest photocatalytic activity for methyl orange at the $[SO^{2-}_4 ]/[Ti^{4+}]$ molar rate of 1:1, calcination temperature of $600^{\circ}C$ for 2 h, and sulfated $TiO_2$ loading amount of 40%, respectively.

• Advances in nano research
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• v.6 no.4
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• pp.377-397
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• 2018

In the present investigation, thermal buckling and free vibration characteristics of functionally graded (FG) Timoshenko nanobeams subjected to nonlinear thermal loading are carried out by presenting a Navier type solution. The thermal load is assumed to be nonlinear distribution through the thickness of FG nanobeam. Thermo-mechanical properties of FG nanobeam are supposed to vary smoothly and continuously throughout the thickness based on power-law model and the material properties are assumed to be temperature-dependent. Eringen's nonlocal elasticity theory is exploited to describe the size dependency of nanobeam. Using Hamilton's principle, the nonlocal equations of motion together with corresponding boundary conditions based on Timoshenko beam theory are obtained for the thermal buckling and vibration analysis of graded nanobeams including size effect. Moreover, in following a parametric study is accompanied to examine the effects of the several parameters such as nonlocal parameter, thermal effect, power law index and aspect ratio on the critical buckling temperatures and natural frequencies of the size-dependent FG nanobeams in detail. According to the numerical results, it is revealed that the proposed modeling can provide accurate frequency results of the FG nanobeams as compared some cases in the literature. Also, it is found that the small scale effects and nonlinear thermal loading have a significant effect on thermal stability and vibration characteristics of FG nanobeams.

• Korean Journal of Metals and Materials
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• v.49 no.10
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• pp.774-779
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• 2011

S-N fatigue behavior of cast 304 stainless steel was studied at 25, -50 and $-196^{\circ}C$ and at a stress ratio of -1 in uniaxial and bending loading condition. It was found that the resistance to S-N fatigue was greatly improved with decreasing testing temperature. The normalized S-N fatigue curves by tensile strength at three different testing temperatures matched each other, suggesting that tensile strength determines the S-N fatigue resistance of cast 304 stainless steel at low temperatures. The effects of different loading on the resistance to S-N fatigue of cast 304 stainless steel were quantified. The S-N fatigue curves at 25, -50 and $-196^{\circ}C$ were described by using Basquin's law the relationship between the S-N fatigue curve and the testing temperature was obtained by using a simple regression method.

• Journal of Powder Materials
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• v.29 no.6
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• pp.499-504
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• 2022

The objective of this study is to assess the impact of spray drying conditions on medium-chain triglyceride (MCT) loading, solubility, and release of an MCT-loaded solid self-emulsifying system in a water-insoluble oily substance. MCT-loaded solid self-emulsifying systems are prepared by spray drying with SDS and calcium silicate. The effects of inlet temperature (60, 80, or 100℃) and feed solution composition (0, 10, 50, 90, or 100% ethanol) on physicochemical properties of MCT-loaded solid self-emulsifying systems are studied. The inlet temperature significantly affects the water solubility of MCT. Moreover, the feed solution composition significantly affects water solubility, release rate, and MCT loading. The MCT-loaded solid self-emulsifying system obtained at 60℃ using 90% ethanol feed solution shows the best physicochemical properties among the synthesized products and exhibits better water solubility (4.43 ± 0.44 vs. 0 ㎍/mL) and release (94.4 ± 1.6 vs. 32.8 ± 7.4%, 60 min) than a commercial product. Furthermore, the MCT-loaded solid self-emulsifying system shows an excellent emulsion droplet size (approximately 230 nm).

• Coupled systems mechanics
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• v.12 no.5
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• pp.409-418
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• 2023

A coupled algorithm is proposed which first considers the creation of porous structure of the material and then the simulations of response of mechanical components with porous structure to a variable load history. The simulations are carried out by the Prandtl operator approach in the finite element method (FEM) which enables structural simulations of mechanical components subjected to variable thermomechanical loads. Temperature-dependent material properties and multilinear kinematic hardening of the material can be taken into account by this approach. Several simulations are then performed for a tensile-compressive specimen made of a generic porous structure and mechanical properties of Aluminium alloy AlSi9Cu3. Variable mechanical load history has been applied to the specimens under constant temperature conditions. Comparison of the simulation results shows a considerable elastoplastic stress-strain response in the vicinity of pores whilst the surface of the gauge-length of the specimen remains in the elastic region of the material. Moreover, the distribution of the pore sizes seems more influential to the stress-strain field during the loading than their radial position in the gauge-length.

• Korean Journal of Materials Research
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• v.23 no.8
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• pp.423-429
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• 2013

Recently, steel structures have increasingly been required to have sufficient deformability because they are subjected to progressive or abrupt displacement arising from structure loading itself, earthquake, and ground movement in their service environment. In this study, high-strength low-carbon bainitic steel specimens with enhanced deformability were fabricated by varying thermo-mechanical control process conditions consisting of controlled rolling and accelerated cooling, and then tensile and Charpy V-notch impact tests were conducted to investigate the correlation between microstructure and mechanical properties such as strength, deformability, and low-temperature toughness. Low-temperature transformation phases, i.e. granular bainite (GB), degenerate upper bainite(DUB), lower bainite(LB) and lath martensite(LM), together with fine polygonal ferrite(PF) were well developed, and the microstructural evolution was more critically affected by start and finish cooling temperatures than by finish rolling temperature. The steel specimens start-cooled at higher temperature had the best combination of strength and deformability because of the appropriate mixture of fine PF and low-temperature transformation phases such as GB, DUB, and LB/LM. On the other hand, the steel specimens start-cooled at lower temperature and finish-cooled at higher temperature exhibited a good low-temperature toughness because the interphase boundaries between the low-temperature transformation phases and/or PF act as beneficial barriers to cleavage crack propagation.

• Structural Engineering and Mechanics
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• v.47 no.6
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• pp.839-856
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• 2013

Metallic annular discs with their outer boundary fully constrained are studied with newly derived semi-analytical solutions for the effects of thickness variations under thermal loading and unloading. The plane stress and axisymmetric assumptions were adopted, and the thickness of the disk depends on the radius hyperbolically with an exponent n. Furthermore, it is assumed that the stress state is two dimensional and temperature is uniform in the domain. The solutions include the elastic, elastic-plastic and plastic-collapse behavior, depending on the values of temperature. The von Mises type yield criterion is adopted in this work. The material properties, Young's modulus, yield stress and thermal expansion coefficient, are assumed temperature dependent, while the Poisson's ratio is assumed to be temperature independent. It is found that for any n values, if the normalized hole radius a greater than 0.6, the normalized temperature difference between the elastically reversible temperature and plastic collapse temperature is a monotonically decreasing function of inner radius. For small holes, the n values have strong effects on the normalized temperature difference. Furthermore, it is shown that thickness variations may have stronger effects on the strain distributions when temperature-dependent material properties are considered.