• Analytical Science and Technology
• /
• v.32 no.5
• /
• pp.163-172
• /
• 2019

Methamphetamine (MA) is currently the most abused illicit drug in Korea and its major metabolite is amphetamine (AP). As MA exist as two enantiomers with the different pharmacological properties, it is necessary to determine their respective amounts in a sample. Thus a chiral stationary phase liquid chromatography-tandem mass spectrometric (LC-MS/MS) method was developed for identification and quantification of d-MA, l-MA, d-AP, and l-AP in human urine. Urine sample ($200{\mu}L$) was diluted with pure water and purified using solid-phase extraction (SPE) cartridge. A $5-{\mu}L$ aliquot of SPE treated sample solution was injected into LC-MS/MS system. Chiral separation was carried out on the Astec Chirobiotic V2 column with an isocratic elution for each enantiomer. Identification and quantification of enantiomeric MA and AP was performed using multiple reaction monitoring (MRM) detection mode. Linear regression with a $1/x^2$ as the weighting factor was applied to generate a calibration curve. The linear ranges were 25-1000 ng/mL for all compounds. The intra- and inter-day precisions were within 3.6 %, while the intra- and inter-day accuracies ranged from -5.4 % to 11.8 %. The limits of detection were 2.5 ng/mL (d-MA), 3.5 ng/mL (l-MA), 7.5 ng/mL (d-AP), and 7.5 ng/mL (l-AP). Method validation parameters such as selectivity, matrix effect, and stability were evaluated and met acceptance criteria. The applicability of the method was tested by the analysis of genuine forensic urine samples from drug abusers. d-MA is the most common compound found in urine and mainly used by abusers.

• Journal of the Korean Society for Aeronautical & Space Sciences
• /
• v.41 no.9
• /
• pp.720-725
• /
• 2013

Nylon wire cutting method by nichrome wire is generally applicable for cube satellite applications due to its advantages of simplicity. However, the system complexity is not avoidable to apply it on the cube satellite with multi-deployable structures. A lower constraint force of the mechanism is also one of the disadvantages of the mechanism. In this study, we proposed a preliminary structure design of cube satellite with the separation mechanism which is applicable for holding and release of the multi-deployable structures. The effectiveness of the mechanism design was verified through function test of EM mechanism. The structure analysis results showed that the structure design proposed in this study is feasible.

• Journal of the Korea Academia-Industrial cooperation Society
• /
• v.19 no.2
• /
• pp.21-27
• /
• 2018

FRN (Full range Naphtha) is distilled from crude oil in a Naphtha Splitter Unit and is separated into the Light Straight Naphtha, Heavy Naphtha, and kerosene according to the boiling point in sequence. This separation is conducted using a series of binary-like columns. In this separation method, the energy consumed in the reboiler is used to separate the heaviest components and most of this energy is discarded as vapor condensation in the overhead cooler. In this study, the first two columns of the separation process are replaced with the Petlyuk column. A structural design was exercised by a stage to stage computation with an ideal tray efficiency in the equilibrium condition. Compared to the performance of a conventional system of 3-column model, the design outcome indicates that the procedure is simple and efficient because the composition of the liquid component in the column tray was designed to be similar to the equilibrium distillation curve. An analysis of the performance of the new process indicated an energy saving of 12.3% under same total number of trays and with a saving of the initial investment cost.

• Proceedings of the Korean Radioactive Waste Society Conference
• /
• 2017.05a
• /
• pp.83-83
• /
• 2017

Electrorefining is a key step in pyroprocessing. The electrorefining process is generally composed of two recovery steps - the deposit of uranium onto a solid cathode and the recovery of the remaining uranium and TRU elements simultaneously by a liquid cadmium cathode. The solid cathode processing is necessary to separate the salt from the cathode since the uranium deposit in a solid cathode contains electrolyte salt. Distillation process was employed for the cathode processing. It is very important to increase the throughput of the salt separation system due to the high uranium content of spent nuclear fuel and high salt fraction of uranium dendrites. In this study, a mesh-covered crucible was investigated for the sat distillation of electrorefiner uranium deposits. A liquid salt separation step and a vacuum distillation step were combined for salt separation. The adhered salt in uranium deposits was efficiently removed in the mesh-covered crucible. The salt distiller was operated simply since repeated cooling - heating step was not necessary for the change of the crucible. The operation time could be reduced by the use of the mesh-covered crucible and the combined operation of the two steps. A method to preserve a vacuum level was proposed by double O-rings during the operation of the distiller with the mesh-covered crucible. After the salt distillation, the salt content was measured and was below 0.1wt% after the salt distillation. The residual salt after the salt distillation can be removed further during melting of uranium metal.

• Journal of Intelligence and Information Systems
• /
• v.10 no.2
• /
• pp.15-37
• /
• 2004

With the growth in the size of datasets, data mining has recently become an important research topic. Especially, interests about spatio-temporal data mining has been increased which is a method for analyzing massive spatio-temporal data collected from a wide variety of applications like GPS data, trajectory data of surveillance system and earth geographic data. In the former approaches, conventional clustering algorithms are applied as spatio-temporal data mining techniques without any modification. In this paper, we focused to SOM that is the most common clustering algorithm applied to clustering analysis in data mining wet and develop the spatio-temporal data mining module based on it. In addition, we analyzed the clustering results of developed SOM module and compare them with those of K-means and Agglomerative Hierarchical algorithm in the aspects of homogeneity, separation, separation, silhouette width and accuracy. We also developed specialized visualization module fur more accurate interpretation of mining result.

• Transactions of the Korean Society for Noise and Vibration Engineering
• /
• v.18 no.8
• /
• pp.879-885
• /
• 2008

A rotordynamic analysis was performed with a decant-type centrifuge, which is a kind of industrial centrifuge. The system is composed of screw rotor, bowl rotor, driving motors, gear box, and support rolling element bearings. These rotors have a rated speed of 4300 rpm, and were modeled utilizing a rotordynamic FE method for analysis, which was verified through 3-D FE analysis. Design goals are to achieve wide separation margins of lateral critical speeds, and favorable unbalance responses of the rotor in the operating range. Then, a complex analysis rotordynamic analysis of the system was carried out to evaluate its forward synchronous critical speeds and mode shapes, whirl natural frequencies, and unbalance responses under various balance grade. As a result of analysis, the rotordynamic analysis performed by separating a screw rotor and bowl rotor may cause an error in predicting critical speed of entire system. Therefore, the rotordynamic analysis of a coupled rotor combining a screw and bowl rotor must be performed in order to more accurately estimate dynamic characteristics of the decanter-type centrifuge as presented in this paper. Also, rolling element bearings with suitable stiffness should be selected to keep enough separation margin. In addition, in establishing balance grade of a screw and bowl rotor, ISO G2.5 balance grade is more recommended than ISO G6.3, in particular balancing correction of a screw rotor based on ISO G2.5 grade is strongly recommended.

• Polymer(Korea)
• /
• v.25 no.2
• /
• pp.177-185
• /
• 2001

In this work, the cure kinetics and rheological properties of difunctional epoxy(diglycidylether of bisphenol A, DGEBA)/polysulfone (PSF) blends were investigated using differential scanning calorimeter and rheometer. From the DSC results of the blends, the temperature of the exothermic peak and cure activation energy (E) using a half-width method were increased with increasing the PSF content to neat epoxy resin up to 30 wt%. However, a marginal decrease in the blend system was shown in E. The conversion ($\alpha$) and conversion rate (d$\alpha$/dt) were decreased as the content of PSF increases. Rheological properties of the blend system were investigated under isothermal condition using a rheometer. Cross-linking activation energy (E$_{c}$) was determined from the Arrhenius equation based on gel time and curing temperature. As a result, the E$_{c}$ showed a similar behavior with E which could be resulted from high viscosity of PSF and the phase separation between DGEBA and PSF.PSF.f PSF and the phase separation between DGEBA and PSF.PSF.

• Journal of the Society of Naval Architects of Korea
• /
• v.28 no.2
• /
• pp.146-158
• /
• 1991

The flow around a two-dimensional foil section Is measured by a LDV(Laser Doppler Velocimetry) system which is capable of measuring the datailed flow field without interfering the original flow field. A 2-color 3-beam LDV system, which is capable of mea,;tiring 2 velocity components simultaneously and uses 2W Ar-Ion laser source, is used to measure the flow field around an NACA0012 foil section. The measured flow velocities are analysed iii order to study the boundary layer characteristics, flow separation and the detail structure of the flow near the trailing edge of the foil. The boundary layer characteristics are compared with the results by the head's momentum integral method. For the case of small angle of attack at relatively higher Reynolds number, both results show good agreements. The measured data of the velocity field around an NACA0012 foil section would be valuable data to validate the CFD(Computational Fluid Dynamic) calculation results. The developed experimental technique to evaluate the characteristics of two-dimensional foil sections is essential tool to develope new blade sections which have good lift characteristics and better cavitation performances.

• Journal of the Korean Society for Aeronautical & Space Sciences
• /
• v.37 no.10
• /
• pp.984-991
• /
• 2009

In this study, transonic aeroelastic response analyses have been conducted for the DLR-F4(wing-body) aircraft configuration considering shockwave and flow separation effects. The developed fluid-structure coupled analysis system is applied for aeroelastic computations combining computational structural dynamics(CSD), finite element method(FEM) and computational fluid dynamics(CFD) in the time domain. It can give very accurate and useful engineering data on the structural dynamic design of advanced flight vehicles. For the nonlinear unsteady aerodynamics in high transonic flow region, Navier-Stokes equations using the structured grid system have been applied to wing-body configurations. In transonic flight region, the characteristics of static and dynamic aeroelastic responses have been investigated for a typical wing-body configuration model. Also, it is typically shown that the current computation approach can yield realistic and practical results for aircraft design and test engineers.

• The Journal of Korea Institute of Information, Electronics, and Communication Technology
• /
• v.10 no.6
• /
• pp.512-521
• /
• 2017

Telemetry ground station use very high gain directional antenna systems that are sensitive to interference from other RF communication systems, Without appropriate interference protection, these systems could be severely impacted or even rendered useless for mission support. In ECC, we suggested ans interference analysis method between LTE-TDD system and telemetry ground station using 2.3GHz. In this paper, based on the interference analysis scenario considered in Electronic Communication Committee, We have derived mutual coexistence separation distance between telemetry ground station and LTE-TDD system(Base station, User equipment) in Spatial domain.