• Title/Summary/Keyword: stripping

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Determination of Germanium(IV) by Differential Pulse Anodic Stripping Voltammetry(I) (Differential Pulse Anodic Stripping Voltammetry법에 의한 게르마늄 분석에 관한 연구(제1보))

  • 문동철
    • YAKHAK HOEJI
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    • v.27 no.1
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    • pp.1-10
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    • 1983
  • Voltammetric deposition and differential pulse anodic stripping (DPASV) of Ge(IV)at a gold electrode was investigated. Germanium (IV) exhibits two stripping peaks by DPASV in sodium borate solution, the first peak at about -1.1v. vs SCE and the second one, in the range of -0.6 to -0.2v. vs SCE. Factors affecting the sensitivity and precision included the nature of working electrode, supporting electrolytes, deposition potential, deposition time, pH, pulse height, voltage scan rate. The relative standard deviation of the measurements of the peak currents, for 100ng/ml Ge(IV), was less than ${\pm}3%$. The detection limit of Ge(IV) was 0.01ng/ml. Percent recovery in the extraction procedure of Ge(IV) from matrices by benzene in c-HCl, followed by back extraction with saturated borax solution, ranged from 96 to 104%.

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Characteristics of the Oxygen Plasma and Its Application to Photoresist Stripping (산소 플라즈마의 특성과 포토레지스트 제거에의 응용)

  • Whang, Ki Woong;Lee, Jong Duk;Kim, Joung Ho
    • Journal of the Korean Institute of Telematics and Electronics
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    • v.24 no.1
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    • pp.73-78
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    • 1987
  • The physical mechanism of a RF discharge used in photoresist stripping and etching process are not well understood and, plasma reactor design and the determination of optimum operating coditions are done largely on empirical basis. We analyzed the discharge process through the measurement of plasma characteristics and applied out results tothe analysis of the photoresist stripping. We investigated the effects of plasma electron density, neutral oxygen gas pressure and electrode temperature on the stripping rates and related their effects with the characteristics of plasma.

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Methane Recovery and Carbon Dioxide Stripping by MEA Solution the Autocirculation Bubble Lift Column Reactor (내부순환식 기포탑 반응기 상에서 MEA (monoethanolamine) 용액에 의한 이산화탄소 분리 및 메탄회수)

  • Lee, In-Hwa;Kim, Sun-Yil;Park, Ju-Young
    • Applied Chemistry for Engineering
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    • v.18 no.3
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    • pp.239-244
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    • 2007
  • For the simultaneous methane recovery and $CO_2$-stripping, we have been developed dual vent auto circulation bubble lift column reactor, and evaluate optimum conditions for monoethanolamine (MEA) solutions as a $CO_2$ absorbent. At the 5 wt% MEA solution, we investigated the pH change during $CO_2$-stripping and absorption reaction, $CO_2$-stripping rate with reaction time, methane recovery efficiency for various inflow rates of air, $CO_2$-stripping rate for flow liquid over flow height, and $CO_2$-stripping dependency on the temperature of absolvent solutions. The suggested optimum conditions for $CO_2$ recovery with MEA in the dual vent auto circulation bubble lift column reactor were 40 mm over flow liquid height, 1.5 L/min of air inflow rate, and $25^{\circ}C$ of absorbent solution temperature.

A SCANNING ELECTRON MICROSCOPIC STUDY ON CHANGES OF ENAMEL SURFACE BY INTERPROXIMAL STRIPPING AND POLISHING (치아인접면 삭제 및 연마에 따른 법랑질 표면의 변화에 관한 주사전자현미경적 연구)

  • Kim, Young-Sun;Kim, Kwang-Won
    • The korean journal of orthodontics
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    • v.22 no.1
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    • pp.123-131
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    • 1992
  • This study was done to evaluate the changes of enamel surface by interproximal stripping and recovery of it by polishing. The number of 34 1st premolars which had extracted for orthodontic treatment were selected as samples. Interproximal stripping was performed by hand with metal strip and strip placer (Dentaurum Co., Germany) and low speed handpiece with diamond disk (Superdiaflex, Germany). Polishing was performed by hand with plastic strip (3M Col) and low speed handpiece with whip-mix, DCPA (Dicalcium Phosphate, Anhydrous, $CaHPO_4$) powder and Sof-lex (3M Co. U.S.A.) polishing kit. Each groups were examined under the scanning electron microscope (JEOL Co., JSM-840A, Japan) and the following results were obtained: 1. The stripped group performed by metal strip and diamond disk altogether showed deep furrow on the enamel surface as wide as about $10{{\mu}m}$. 2. There could be seen more irregular scratched line in the group stripped by metal strip than that by diamond disk. 3. The polished group performed by plastic strip and DCPA powder showed slight smoothening of the edge of stripped furrow on the enamel surface without relation to the stripping method. 4. The polished group performed by Sof-lex progressive polishing kit could not avoid the formation of the furrows on the enamel surface according to the particle size without relation to the stripping method. 5. The polished group performed by the superfine polishing wheel, the final stage of Sof-lex polishing method showed shallow scratched line as wide as within about $2{{\mu}m}$ on the enamel surface without relation to the stripping method. 6. The interproximal stripped enamel surface could not recover its original surface texture by any kind of polishing methods.

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Evaluation of Anti-Stripping Performance in Asphalt Concrete using Byproduct Ash produced from Circulating Fluidized Bed Boiler (보일러 부산 애쉬를 이용한 아스팔트 콘크리트의 박리저항성 평가)

  • Kim, Yooseok;Kim, Nakseok
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.38 no.2
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    • pp.319-325
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    • 2018
  • Pot-holes are steadily increasing due to abnormal climate such as heavy rainfall and frequent snowfall. Pot-hole related to traffic accidents cause injuries, car damage and distress of road facilities. To reduce pot-holes, the use of an anti-stripping agent is mandatorily recommended to asphalt concrete mixture. Hydrated lime is commonly used as anti-stripping agent due to the convenience and economics. Byproduct ash from circulating fluidized bed boiler was reviewed as an anti stripping agent. According to the test results, the byproduct ash is satisfied with TSR specification using 1% to 3% by weight of the asphalt mixture. The byproduct ash was examined under various condition changes of aggregate and asphalt concrete mixture considering quality movement. According to the results, using the byproduct ash was measured average 0.87 of TSR and coverage rates of 60% after rolling bottle test. Test results also revealed that the byproduct ash showed stable performance. Using the byproduct ash to decrease pot-hole in asphalt concrete pavement is suitable for demonstrating stable performance as anti-stripping agent.

Study on the Ethanol Recovery Process using Dircet Contact Heat Exchange (고온의 기포접촉에 의한 에탄올 회수공정에 관한 연구)

  • Lee, Won-Young;Yeo, Sang-Do;Choi, Yong-Hee
    • Korean Journal of Food Science and Technology
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    • v.27 no.2
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    • pp.176-180
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    • 1995
  • Direct contact heat exchange (DCHE) method has been employed to investigate the separation of ethanol from dilute aqueous solutions. Bubbles at high temperature were dispersed into a continuous liquid phase, generating temperature gradient in air-liquid interface, which causes heat and mass transfer accordingly. The experiments were performed in the ranges of jet regime air flow. The air-water stripping coefficient increased $5{\sim}10,\;and\;1{\sim}1.5$ times as temperature and air flow rate increased, respectively. The recovery ratio based on the initial ethanol concentration reached into 80% at the air flow rate of 84.88 m/min. The initial ethanol concentration showed little effect on the stripping coefficient and the recovery ratio.

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Analysis on Stripping Time of Form of High-Early-Strength Concrete Incorporating Binder and Admixture (결합재 및 혼화제를 사용한 조강 콘크리트의 거푸집 탈형 시기 분석)

  • Jun, Myoung-Hoon;Bang, Jong-Dae;Lee, Bum-Sik;Park, Seong-Sik;Park, Ji-Young;Cho, Gun-Hee
    • Land and Housing Review
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    • v.4 no.2
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    • pp.193-200
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    • 2013
  • Construction duration in construction project is an important factor which affects project cost. Advanced countries have reduced project cost by time shortening. Even though domestic construction companies have tried to time shortening, they yet failed to find systematic method for time shortening. Typically, duration of structural framework is affected by stripping time of form. Therefore, it need to shorten the stripping time of form for time shortening of structural framework. In this study, specimens of high-early-strength concrete were manufactured with variety conditions and compressive strength was tested. This study proposed stripping time of side and slab forms using test results. The stripping time of form was shortened when using high-early-strength concrete in structural framework by the test results. The result of this study will be useful for time shortening of structural framework.

Estimation of Ammonia Stripping Condition for Adequate Aerobic Liquid-Composting of Swine Manure (돈분뇨의 적합한 호기성 액비화를 위한 암모니아 탈기조건 설정)

  • Son, Bo-Kyoon;Gang, Seong-Gu;Jo, Eun-Ju;Kim, Shin-Do;Lee, Chang-Ju;Kim, Jeong-Ho
    • Korean Journal of Soil Science and Fertilizer
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    • v.39 no.2
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    • pp.73-79
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    • 2006
  • Aeration is the most important and indispensable operation unit for the treatment of swine manure using aerobic liquid-composting process. The composting of swine manure depends on biological treatment process, but the highly concentrated ammonia nitrogen is required a pretreatment to expect the appropriate efficiency of the biological treatment process. In this study, pilot experiments have been carried out to estimate of the fit condition about ammonia stripping process as a pretreatment to aerobic liquid- composting. pH adjustment with $Ca(OH)_2$ was economically superior to use of NaOH and optimum pH of ammonia stripping was 12.3, ammonia nitorgen was rapidly removed as pH were increased at $$35^{\circ}C$$. When air stripping is performed before aerobic liquid-stripping, a high initial pH is required for complete ammonia removal and is additional effects such as organic substances, phosphorus, turbidity, and color removal. Stripping process was very efficient in the pretreatment of highly concentrated ammonia nitrogen for composting of swine manure. Emission rate of gaseous ammonia was $0.5355mole\;s^{-1}$ at initial time and $0.0253mole\;s^{-1}$ at finitial time. The fit condition of ammonia stripping in this study were at the temperature of $$35^{\circ}C$$, and the pH of 12.3 during 48 hours.

A Comparative study of roughness of enamel surface to various interdental enamel stripping methods in vitro (치간 법랑질 삭제방법에 따른 치아표면 거칠기에 관한 비교연구)

  • Row, Joon;Chun, Youn-Sic
    • The korean journal of orthodontics
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    • v.29 no.4 s.75
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    • pp.483-490
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    • 1999
  • Interdental enamel stripping is an usual method for correction of abnormal tooth shape and tooth size discrepancy which is one of the etiologic factors of malocclusion. Clinically it Is useful to correct the minor crowding in anterior teeth and posterior occlusion during finishing stage of orthodontic treatment. But this procedure has risks such as irreversible tooth reduction and remaining roughness of enamel surface can accumulate plaque which can evoke periodontal problem. Even if various methods were introduced to minimize the enamel surface roughness, their evaluation was limited in morphologic differences by scanning electronic microscope(SEM). The purpose of this study was to compare the various interdental enamel stripping method by SEM and to quantify the difference of surface roughness by use of Surfcorder SEF-30D(Kosaka Lab. Ltd.) which can measure the roughness of surface. The stripping methods were divided into mechanical and mechanical-chemical method. Air-rotor stripping and separating strip were used for mechanical stripping and $37\%$ phosphoric acid was used for chemical stripping. The enamel surface roughness after mechanical or mechanical-chemical stripping of interproximal surfaces of premolars which were extracted for orthodontic purpose were measured and compared by means of SEM and $Surfcorder^{\circledR}$, the results were as follows. 1. Enamel surface of primary treated by coarse diamond bur and separating strip groups showed highest value of roughness. 2. To compare the primary treated groups between mechanical and mechanical-chemical method, the latter group showed lower value of roughness remarkably. 3. Mechanical stripping groups which were treated both coarse and fine instrument showed lower value of roughness as much as non treated group. 4. The use of Pumice for final polishing did not show significantly smoothening the stripped enamel surface any more.

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