• Title/Summary/Keyword: size-dependent

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Crystal Growth of $LiTaO_3$ and the Effect pf Crucible Type and Atmosphere ($LiTaO_3$ 단결정 성장과 용기 및 분위기의 영향)

  • 박승익;채승욱;김정돈;주기태;정수진
    • Journal of the Korean Ceramic Society
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    • v.31 no.1
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    • pp.39-46
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    • 1994
  • LiTaO3 single crystals were growth without cracking using Pt-Rh crucible and Ir crucible. The starting composition to get the melt of congruent melting composition, which has been dependent upon the experimental procedure, was taken after fixing the total growing process by the result of preliminary experiments. The Rh contamination from the Pt-Rh crucible was to be neglected if the crystal had been grown under inert atmosphere, which resulted in the crystal color being slightly yellow. This color was decolored after 24 hour's annealing at 1200℃ under air atmosphere. The optimum conditions for the crystal growing and the diameter control were so dependent upon the crucible material in spite of using the crucible of the same size. The liquid-solid interface of LiTaO3 crystal of 1" diameter has been flat if the rotation speed was 45rpm.

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Dynamic buckling response of temperature-dependent functionally graded-carbon nanotubes-reinforced sandwich microplates considering structural damping

  • Shokravi, Maryam;Jalili, Nader
    • Smart Structures and Systems
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    • v.20 no.5
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    • pp.583-593
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    • 2017
  • This research deals with the nonlocal temperature-dependent dynamic buckling analysis of embedded sandwich micro plates reinforced by functionally graded carbon nanotubes (FG-CNTs). The material properties of structure are assumed viscoelastic based on Kelvin-Voigt model. The effective material properties of structure are considered based on mixture rule. The elastic medium is simulated by orthotropic visco-Pasternak medium. The motion equations are derived applying Sinusoidal shear deformation theory (SSDT) in which the size effects are considered using Eringen's nonlocal theory. The differential quadrature (DQ) method in conjunction with the Bolotin's methods is applied for calculating resonance frequency and dynamic instability region (DIR) of structure. The effects of different parameters such as volume percent of CNTs, distribution type of CNTs, temperature, nonlocal parameter and structural damping on the dynamic instability of visco-system are shown. The results are compared with other published works in the literature. Results indicate that the CNTs have an important role in dynamic stability of structure and FGX distribution type is the better choice.

Functional Analysis of RAD4 Gene Required for Nucleotide Excision Repair of UV-induced DNA Damage in Saccharomyces cerevisiae

  • Park, Sang Dai;Park, In Soon
    • Animal cells and systems
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    • v.6 no.4
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    • pp.311-315
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    • 2002
  • The RAD4 gene is essential for nucleotide excision repair in Saccharomyces cerevisiae. It has been known that the deduced amino acid sequence of Rad4 protein contains three DNA-dependent ATPase/helicase motifs. To determine the biochemical activities and functional role of RAD4 the Rad4 protein was expressed and purified. Immunoblot analysis showed a specific band of 21 kDa, which was well-matched with the size of open reading frame of the RAD4 gene. The purified Rad4 protein had no detectable helicase activity. However, the protein could interact with double stranded oligonucleotides, as judged by mobility shift assay. This result suggests that the Rad4 protein is a DNA binding protein.

Etching and Polishing Behavior of Cu thin film according to the additive chemicals

  • Ryu, Ju-Suk;Eom, Dae-Hong;Hong, Yi-Koan;Park, Jum-Yong;Park, Jin-Goo
    • Proceedings of the International Microelectronics And Packaging Society Conference
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    • 2002.05a
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    • pp.274-278
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    • 2002
  • The purpose of this study was to characterize the reaction of Cu surface with Cu slurry and CMP performance as a function of additives in CMP slurry. The polish rate of Cu was dependent on the kind of organic acids added in slurry. It was considered that polish rate of Cu was dependent on the concentration of carboxylates and mean particle size. When the etchant and oxidant were added in slurry, the highest removal rate and lower etch rate were measured at neutral pH. The addition of etchant, oxidant and pH adjustor played key roles of CMP ability in slurry. As the pH increased, polish rate of Cu was increased by the enhanced the mechanical effects due to effective dispersion of slurry particles. Alumina abrasives was more desirable for 1st step slurry because of high removal rate of Cu and high selectivity ratio among TaN and Cu.

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Local nanofiller volume concentration effect on elastic properties of polymer nanocomposites

  • Shin, Hyunseong;Han, Jin-Gyu;Chang, Seongmin;Cho, Maenghyo
    • Multiscale and Multiphysics Mechanics
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    • v.1 no.1
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    • pp.65-76
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    • 2016
  • In this study, an influence of local variation of nanoparticulate volume fraction on the homogenized elastic properties is investigated. It is well known that interface effect is dependent on the radius and volume fraction of reinforced nanofillers. However, there is no study on the multiscale modeling and analysis of polymer nanocomposites including polydispersed nanoparticles with consideration of interphase zone, which is dependent on the volume fraction of corresponding nanoparticles. As results of numerical examples, it is confirmed that an influence of local variation of nanoparticulate volume fraction should be considered for non-dilute system such as cluster of nanoparticles. Therefore representative volume element analysis is conducted by considering local variation of nanoparticle volume fraction in order to analyze the practical size of cell including hundreds of nanoparticles. It is expected that this study could be extended to the multiparticulate nanocomposite systems including polydispersed nanoparticles.

Temperature-Dependent Thermal and Chemical Stabilities as well as Mechanical Properties of Electrodeposited Nanocrystalline Ni

  • Zheng, Liangfu;Peng, Xiao
    • Metals and materials international
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    • v.24 no.6
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    • pp.1293-1302
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    • 2018
  • Nanocrystalline (NC) Ni electrodeposits (EDs) with a mean grain size of $34{\pm}12nm$ has been investigated, from room temperature to $800^{\circ}C$ under a purge gas of argon, by both non-isothermal and isothermal differential scanning calorimetry measurements, in combination with characterization of temperature-dependent microstructural evolution. A significant exothermic peak resulting from superimposition of recrystallization and surface oxidation occurs between 340 and $745^{\circ}C$ at a heating rate of $10^{\circ}C/min$ for the NC Ni EDs. The temperatures for recrystallization and oxidation increase with increasing the heating rate. In addition, recrystallization leads to a profound brittle-ductile transition of the Ni EDs in a narrow range around the peak temperature for the recrystallization.

Restricted maximum likelihood estimation of a censored random effects panel regression model

  • Lee, Minah;Lee, Seung-Chun
    • Communications for Statistical Applications and Methods
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    • v.26 no.4
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    • pp.371-383
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    • 2019
  • Panel data sets have been developed in various areas, and many recent studies have analyzed panel, or longitudinal data sets. Maximum likelihood (ML) may be the most common statistical method for analyzing panel data models; however, the inference based on the ML estimate will have an inflated Type I error because the ML method tends to give a downwardly biased estimate of variance components when the sample size is small. The under estimation could be severe when data is incomplete. This paper proposes the restricted maximum likelihood (REML) method for a random effects panel data model with a censored dependent variable. Note that the likelihood function of the model is complex in that it includes a multidimensional integral. Many authors proposed to use integral approximation methods for the computation of likelihood function; however, it is well known that integral approximation methods are inadequate for high dimensional integrals in practice. This paper introduces to use the moments of truncated multivariate normal random vector for the calculation of multidimensional integral. In addition, a proper asymptotic standard error of REML estimate is given.

Surface effects on scale-dependent vibration behavior of flexoelectric sandwich nanobeams

  • Ebrahimi, Farzad;Karimiasl, Mahsa;Civalek, Omer;Vinyas, Mahesh
    • Advances in nano research
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    • v.7 no.2
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    • pp.77-88
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    • 2019
  • This paper infer the transient vibration of piezoelectric sandwich nanobeams, In present work, the flexoelectric effect on the mechanical properties of vibration piezoelectric sandwich nanobeam with different boundary conditions is investigated. According to the Nonlocal elasticity theory in nanostructures, the flexoelectricity is believed to be authentic for such size-dependent properties. The governing equations are derived by Hamilton's principle and boundary condition solved by Galerkin-based solution. This research develops a nonlocal flexoelectric sandwich nanobeam supported by Winkler-Pasternak foundation. The results of this work indicate that natural frequencies of a sandwich nanobeam increase by increasing the Winkler and Pasternak elastic constant. Also, increasing the nonlocal parameter at a constant length decreases the natural frequencies. By increasing the length to thickness ratio (L/h) of nanobeam, the nonlocal frequencies reduce.

Improvement of thermal buckling response of FG-CNT reinforced composite beams with temperature-dependent material properties resting on elastic foundations

  • Bensaid, Ismail;Kerboua, Bachir
    • Advances in aircraft and spacecraft science
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    • v.6 no.3
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    • pp.207-223
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    • 2019
  • Current investigation deals with the thermal stability characteristics of carbon nanotube reinforced composite beams (CNTRC) on elastic foundation and subjected to external uniform temperature rise loading. The single-walled carbon nanotubes (SWCNTs) are supposed to have a distribution as being uniform or functionally graded form. The material properties of the matrix as well as reinforcements are presumed to be temperature dependent and evaluated through the extended rule of mixture which incorporates efficiency parameters to capture the size dependency of the nanocomposite properties. The governing differential equations are achieved based on the minimum total potential energy principle and Euler-Bernoulli beam model. The obtained results are checked with the available data in the literature. Numerical results are supplied to examine the effects of numerous parameters including length to thickness ratio, elastic foundations, temperature change, and nanotube volume fraction on the thermal stability behaviors of FG-CNT beams.

Effect of pH in 3.5% NaCl aqueous solution and ferrite grain size on corrosion fatigue fracture of dual phase steel (複合組織鋼의 부식피로파괴에 미치는 3.5% NaCl水溶液의 pH와 母相粒徑의 效果)

  • 오세욱;강호민
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.11 no.6
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    • pp.867-876
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    • 1987
  • Corrosion fatigue fracture with change in the grain size of M.E.F. dual phase steel is investigated in 3.5% NaCI aqueous solution at pH 2, 4, 6, 9, and 11. Generally speaking, decrease in corrosion fatigue life is strongly dependent on decrease in pH and slightly on the grain size. For the B material with the big grain size, the fatigue life is small due to its large reduction ratio of corrosion fatigue life. The influence of grain size on the reduction ratio of corrosion fatigue life is large at pH 11-6. Whi9le at pH 4-2 the reduction ratio of corrosion fatigue life only depends on the corrosion effect. The larger grain size and the lass pH result in the greater influence on corrosion fatigue crack propagation rate. As pH decreases, the plateau portion in the crack propagation rate curves of the B material are distinct. Crack propagation rate curves become slow down at high .DELTA.K range because crack closure effect by minute corrosion products inside crack causes the oxidation corrosion action less effective for a certain period of time. In A material with small grain size, fatigue life is increased in proportion with increase of martensite intergranular which brings forth restraining the crack propagation decreases crack propagation rate. Corrosion pit which is created in the surface of specimen is found at pH 6,4 and 2 which is noticeable and the unevenness of the surface of the specimen becomes severe as pH decreases. The unevenness of corrosion fatigue fracture surface is severe as the effect of pH increases i.e. as pH decreases. In proportion with increase in the grain size and decrease in pH, the aspect of brittle fracture becomes evident.