• Title/Summary/Keyword: size analysis

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Analysis of Manufacturing Conditions Affecting the DropletSize of Ethyl Cellulose Nanoparticles (에틸 셀룰로오스 나노 파티클 입자 사이즈에 영향을 주는제조 조건의 분석)

  • Jong Hwan Bae;Byung Suk Jin
    • Journal of Integrative Natural Science
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    • v.17 no.3
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    • pp.87-92
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    • 2024
  • Using the design of experiments (DOE), factors affecting the droplet size of ethyl cellulose (EC) nanoparticles in the manufacturing process were analyzed to optimize process conditions. The concentration of EC dissolved in solvent (acetone or ethanol), the mixing ratio of the EC solution to distilled water, and sonication power were selected as the main variables affecting the droplet size of the nanoparticles. The effect of these variables on droplet size was examined through the signal-to-noise (S/N) ratios of the Taguchi method and ANOVA analysis. Sonication power in the acetone solvent and EC solution concentration in the ethanol solvent were identified as the most influential factors on nanoparticle size.

Prediction for the Dynamically Recrystallized Grain Size of AISI 304 (AISI 304 스테인리스강의 동적 재결정립 예측)

  • Kim S. I.;Yoo Y. C.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2001.05a
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    • pp.143-146
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    • 2001
  • The evolution of dynamic recrystallization (DRX) was studied with torsion test for AISI 304 stainless steel in the temperature range of $900-1000^{\circ}C$ and strain rate range of 0.05-5/sec. The evolution of DRX was investigated with microstructural analysis and change of flow stress curve slope. The investigation of serrated grain boundaries using electron back scattered diffraction (EBSD) analysis indicated that the nucleated new DRX grain size was similar to the size of bulging part. Before the steady state, the dynamically recrystallizing grains do not remain a constant size and gradually grow to the size of fully DRX grain at steady state. The calculation of grain size was based on $X_{DRX}$ and the assumption, which the nucleated DRX grains are growing to the steady state, continuously. It was found that the calculated results agreed with the microstructure of the alloy.

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Analysis of Sodium Spray Fire Using Gaussian Droplet Size Distribution (Gaussian 액적 크기 분포 함수를 이용한 분무형 화재 현상 해석)

  • Kim, B.H.;Hahn, D.H.;Suh, S.H.
    • Journal of Hydrogen and New Energy
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    • v.15 no.1
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    • pp.72-81
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    • 2004
  • Study on the analysis of sodium spray fire using Gaussian drop size distribution, which redistributes a droplet spectrum with given mean diameter if its size classes with critical diameter(D>8mm) occur, was carried out. In this case, the oversized droplets were reduced to a stable diameter. Results calculated by the code using Gaussian drop size distribution were in better agreement with AI experimental results than those of NACOM and SPRAY code. The effect of variance on pressure in the test cell appeared greatly by introducing Gaussian function, which could represent various sodium droplet size distribution. The increase of the variance with mean droplet size resulted had an important effect upon the pressure in the test cell.

Particle Size Characteristics with the Specification of Yeongdong Illite Powder Products (영동 일라이트 분말 제품의 규격에 따른 입도 특성)

  • EunJi Baek;Yu Na Lee;Eun Jeong Kim;Youngseuk Keehm;Hyun Na Kim
    • Korean Journal of Mineralogy and Petrology
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    • v.36 no.4
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    • pp.345-353
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    • 2023
  • This study aimed to investigate the differences in the commercial powder products of the Yeongdong illite based on sales specifications, specifically examining the mineralogical composition, particle size, and chemical composition according to mesh size. The goal was to understand the characteristics of illite powder products and utilize them as a mineralogical database for exploring various applications. Commercial illite powder samples obtained from two mines were subjected to various experiments, including X-ray diffraction (XRD) analysis, laser diffraction particle size analysis, and scanning electron microscopy analysis, X-ray fluorescence analysis. The XRD analysis revealed that the illite powder products from the two mines mainly consisted of illite/muscovite, quartz, and feldspar, indicating similar constituent minerals matching with those of ores for each mine. Laser diffraction particle size analysis indicated the difference in particle size distribution depending on the product specifications, with particle size uniformity tending to increase with increasing mesh sizes. Scanning electron microscopy analysis showed variations in particle shape and size based on specifications. The size of illite particles did not vary significantly with product specifications, with noticeable changes observed mainly in the particle sizes of quartz and feldspar. Furthermore, although there were some differences in chemical composition among the samples from different mines, no significant variations were observed according to specifications. Based on these results, when considering the application of commercial illite powder, it is essential to carefully select it with the consideration of its specifications to account for characteristic variations. The findings of this study present support the great potential of various application fields of commercial illite powder, contributing to industrial utilization and the development of new technologies.

WSR Study of Particle Size, Concentration and Chemistry Near Soot Inception (WSR 초기매연 조건에서의 입자 크기, 농도 및 화학적 특성)

  • Lee, Eui-Ju;Mulholland, George W.
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.28 no.9
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    • pp.1117-1123
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    • 2004
  • The characteristics of soot near the soot inception point for an ethene-air flame was carried out in a WSR (well-stirred reactor). The new sampling tool like the temperature controlled filter system was introduced to minimize the condensation during sampling. The new analysis tools applied include the real time size distribution analysis with the Nano-DMA, particle size by transmission electron microscopy, C/H analysis, g filter analysis, and thermogravimetric analysis using both non-oxidative and oxidative pyrolysis. The WSR can generate young soot particles that can be collected and examined to gain insight into inception. For the current conditions, soot does not form for ${\Phi}$=1.9, inception occurs at or before ${\Phi}$=2.0, and inception combined with soot surface growth and/or coagulation occurs for ${\Phi}$=2.1. The filter samples for ${\Phi}$=1.9 are composed of volatile compounds that evolve at relatively low temperatures when heated in the presence or absence of O$_2$. The samples collected from the WSR at ${\Phi}$=2.0 and ${\Phi}$=2.1 are precursor-like in morphology and size. They have higher C/H ratios and lower organic percentages than precursor particles, but they are clearly not fully carbonized soot. The WSR PAH distribution is similar to that in young soot from inverse flames.

WSR Study of Particle Size, Concentration, and Chemistry near Soot Inception (WSR 초기수트 조건에서의 입자 크기, 농도 및 화학적 특성)

  • Lee, Eui-Ju;Mulholland, George. W.
    • Proceedings of the KSME Conference
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    • 2004.04a
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    • pp.1298-1303
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    • 2004
  • The characteristics of soot near the soot inception point for an ethene-air flame was carried out in a WSR (well-stirred reactor). The new sampling tool like the temperature controlled filter system was introduced to minimize the condensation during sampling. The new analysis tools applied include the real time size distribution analysis with the Nano-DMA, particle size by transmission electron microscopy, C/H analysis, g filter analysis, and thermogravimetric analysis using both non-oxidative and oxidative pyrolysis. The WSR can generate young soot particles that can be collected and examined to gain insight into inception. For the current conditions, soot does not form for ${\Phi}=1.9$, inception occurs at or before ${\Phi}=2.0$, and inception combined with soot surface growth and/or coagulation occurs for ${\Phi=2.1}$. The filter samples for ${\Phi}$=1.9 are composed of volatile compounds that evolve at relatively low temperatures when heated in the presence or absence of $O_2$. The samples collected from the WSR at ${\Phi}=2.0$ and ${\Phi}=2.1$ are precursor-like in morphology and size. They have higher C/H ratios and lower organic percentages than precursor particles, but they are clearly not fully carbonized soot. The WSR PAH distribution is similar to that in young soot from inverse flames.

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Measurement of the Single and Size-Classified Raindrops

  • Ma, Chang-Jin;Mikio Kasahara;Hwang, Kyung-Chul;Park, Kum-Chan;Kim, Hui-Kang
    • Journal of Korean Society for Atmospheric Environment
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    • v.15 no.E
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    • pp.73-79
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    • 1999
  • To Characterize the single raindrops as a function of their size we designed the sampling and handling apparatuses. Samplings of single and size- classified raindrops were performed at a height of 20m above the ground level of a Kyoto University building located in Uji, Japan in rain events from middle of July to the end of August, 1999. And PIXE method was applied to the analysis of single raindrops sampled as a function of their size. Diameter change of frozen raindrops by liquid nitrogen did nto affect the size segregation ability of our sampling apparatus. The number of raindrops increases with decreasing drop size. And it is found that the size distribution of raindrops verified depends on the rain events. Application of PIXE analysis to the measurement of single raindrops was very successful. Every element showed a continuous increase in concentration with decreasing raindrop diameter. It seems reasonable to say that our work should be helpful to obtain more detailed information on single raindrops and especially to study on the rainout and washout mechanisms.

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A meta-analysis on the effects of the differentiated instruction in mathematics (수학과 수준별 수업의 효과에 대한 메타분석)

  • Kim, Sun Hee
    • The Mathematical Education
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    • v.54 no.4
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    • pp.335-350
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    • 2015
  • The purpose of this study was to investigate the effectiveness of the differentiated instruction in mathematics by a meta-analysis. Among the studies conducted for last twenty three years, the relevant 49 research articles were selected, 80 effect sizes were calculated for the cognitive domain and 70 effect sizes for the affective domain. Effect sizes were analyzed with school levels, student level, group organization method such as homogeneous vs. heterogeneous, class transfer and adjusting class sizes for each cognitive domain and affective domain. The results are as the followings: In the cognitive domain, the overall effect size of the differentiated instruction produced a medium effect(effect size=0.68, U3=75.17%). The differentiated instruction showed the highest effect size on elementary school and middle school, mid level students, heterogeneous group, class transfer and not adjusted class size. And in the affective domain, the overall effect size of the differentiated instruction produced a low effect(effect size=0.36, U3=65.36%). The differentiated instruction showed the highest effect size on elementary school, mid level students, and heterogeneous group. Thus the differentiated instruction was proved to be effective in mathematics classes.

Analysis of Size Effect of Nano Scale Machining Based on Normal Stress and Indentation Theories (수직응력과 압입이론에 기반한 나노스케일 기계가공에서의 크기효과 분석)

  • Jeon, Eun-chae;Lee, Yun-Hee;Je, Tae-Jin
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.17 no.6
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    • pp.1-6
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    • 2018
  • Recently nano meter size pattern (sub-micro scale) can be machined mechanically using a diamond tool. Many studies have found a 'size effect' which referred to a specific cutting energy increase with the decrease in the uncut chip thickness at micro scale machining. A new analysis method was suggested in order to observe 'size effect' in nano scale machining and to verify the cause of the 'size effect' in this study. The diamond tool was indented to a vertical depth of 1,000nm depth in order to simplify the stress state and the normal force was measured continuously. The tip rounding was measured quantitatively by AFM. Based on the measurements and theoretical analysis, it was verified that the main cause of the 'size effect' in nano scale machining is geometrically necessary dislocations, one of the intrinsic material characteristics. st before tool failure.

Evaluation of characteristics of drainage layer according to particle size, particle size, and compositional location of aggregate using fluid analysis program (유체해석 프로그램을 이용한 골재의 입자크기 및 입도, 구성위치에 따른 배수층의 특성 평가)

  • Lim, Chang-Min;Kwon, Hyun-Woo;Kim, Young-Min;Cho, Do-Young;Lee, Gun-Cheol
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2022.11a
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    • pp.147-148
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    • 2022
  • Due to recent climate abnormalities, the form of rainfall is changing to localized torrential rains. Localized torrential rains cause flooding in urban areas. In addition, in various industrial fields, there are cases where materials necessary for the process are kept outdoors, and damage from material loss and flooding of stockyards occurs during heavy rain. Accordingly, it is necessary to introduce a drainage layer where flooding is expected. This drainage layer places the aggregate inside and allows rainwater to penetrate and drain into the voids between the aggregates. However, the amount of voids differs according to the particle size distribution and particle size of the aggregate, and the drainage performance varies according to the compositional location of the aggregate. Therefore, in this study, the drainage characteristics according to the particle size, particle size, and compositional location of aggregates are analyzed using a fluid analysis program.

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