• Journal of Welding and Joining
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• v.28 no.2
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• pp.79-83
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• 2010

In this study, newly developed welding consumables for EGW were welded in EH 36 TM steel plates and their welded joints were evaluated in point of mechanical properties and microstructures compared with imported consumables. Newly developed welding consumables were evaluated as good arc stability and slag fluidity, substantially the same with imported products. The tensile strength of all welded joints were sufficient to meet the requirements specified in a ship’s classification(490~640MPa) and all areas of fracture were heat affected zone(HAZ). Charpy absorbed energy values of all EG welded metals were sufficient to meet the requirements of classification(min. 34J) and those of newly developed wires were evaluated to be better than those of imported wires. As a result observing microstructures of single and tandem EG welded metals through optical and scanning electron microscope (OM&SEM), no grain boundary ferrite(PF(G)) were created in a prior austenite grain boundary and a volume fraction of a fine acicular ferrite were observed very high.

• Carbon letters
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• v.7 no.1
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• pp.19-26
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• 2006

Three point bending tests of single edge notched beam (SENB) specimens were carried out to evaluate the fracture behavior of the fine-grain isotropic nuclear grade graphite, IG-11. To measure the crack initiation point and the subsequent crack growth, the direct current potential drop (DCPD) method and a traveling microscope were used. The effects of test variables like initial crack length, specimen thickness, notch type and loading rate on the measured fracture toughness, $K_Q$, were investigated. Based on the test results, the ranges of the test variables to measure the reliable fracture toughness value were proposed. During the crack growth, the rising R-curve behavior was observed in IG-11 graphite when the superficial crack length measured on the specimen surface was used. The increase of crack growth resistance was discussed in terms of crack bridging, crack meandering, crack branching, microcracking and crack deflection, which increase the surface energy and friction force.

• Korean Journal of Food Science and Technology
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• v.11 no.2
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• pp.81-85
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• 1979

A Neotec infrared instrument was evaluated for determination of protein contents of wheat and barley. Correlation coefficients between protein content determined on the instrument and by the Kjeldahl method were highly significant (0.97 to 0.98). Accuracy of analyses, measured by the standard error of a single test was 0.07 to 0.16, giving a coefficient of variability of 0.6 to 1. 1%. Method of grinding samples affected particle size and type. Particle size did not directly influence protein values; however, greater accuracy and reproducibility were achieved with smaller particle sizes. Packing density inside the loading tell also influenced the analytical results.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.15 no.4
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• pp.308-313
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• 2002

Samples with the norminal composition, $Bi_{2-x}Au_xSr_2CaCu_2O_{8+\delta}$ (x = 0, 0.05. 0.1, 0.15) were prepared by the solid-state reaction method. The superconducting properties, x-ray powder diffraction patterns, critical temperature and microstructure of surface were measured the samples. x-ray patterns show the single phase(2212) nature of the samples. But, the peaks of 2201 at $2\theta=30^{\circ}$ and Au peak at $2\theta=38.31^{\circ}$ are observed in the Au additive samples. The grain sire are enlarged with the increase of x. As the result of enlargement the grain size, the onset and offset critical temperature($T_c^{on}$,$T_c^{zero}$) increased with increase of x.

• Journal of Environmental Impact Assessment
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• v.9 no.1
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• pp.1-11
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• 2000

An environmental geochemical survey of heavy metal distribution in marine surface sediments around the ocean of Samcheonpo coal-fired power plant was conducted to investigate the possibility of coal-ash leakage from ash pond and the associated heavy metal pollution in sedimental deposits due to the operation of the coal-fired power plant. The X-Ray Diffractometry (XRD) analysis showed that the main leakage point of coal-ash was limited to a single site of the first ash pond. It also appeared that the amounts of organic carbon and metal elements were positively correlated to the grain size distribution, and that Co, Cr, Cu, Fe, Ni, and Zn were bounded to organic ligands. However, the distributions of Cd, Hg, and Mn did not have any significant correlation with the sediment grain size and organic matters. In particular, the distribution of Cd appeared to be affected by the concentration of the carbonate materials in the study area.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.12 no.1
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• pp.56-61
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• 1999

Highly conductive oxide films of BaRuO$_3$ have been grown heteroepitaxially on (100) LaAlO$_3$ single crystalline substrates by using pulsed laser deposition. The films are c-axis oriented with an in-plane epitaxial relationship of <010><100>BaRuO$_3$ // <110>LaAlO$_3$. Atomic force microscopy (AFM) observation shows that they consist of a fine-arranged network of grains and have a mosaic microstructure. Generally temperature-dependent resistivity shows the transition from metallic curve to semiconductor-metallic twofold curve by the deposition conditions for Ru oxide based materials like SrRuO$_3$, CaRuO$_3$, BaRuO$_3$, etc.. This twofold curve comes from the structural similarity of Ru oxide based materials including BaRuO$_3$. We find that the distance of Ru-Ru bonding in the unit cell of BaRuO$_3$ as well as the grain boundary scattering could be the two important causes of these interesting conductive properties.

• Journal of the Korean Society for Heat Treatment
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• v.8 no.1
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• pp.53-64
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• 1995

A study was made to characterize the microstructures and mechanical properties of the base metal and the heat-affected zone(HAZ) in Cu-bearing HSLA-100 steel. The Gleeble thermal/mechanical simulator was used to simulated the weld HAZ. The relationship between microstructure and toughness of HAZ was studied by impact test, O. M, SEM, TEM, and DSC. The toughness requirement of military specification value was met in all test temperatures for the base metal. The decrease of HAZ toughness comparing to base plate is ascribed to the coarsed-grain and the formation of bainite. Obliquely sectioned Charpy specimens show that secondary crack propagate easily along bainite lath. Improved toughness(240J) at HAZ of $Tp_2=950^{\circ}C$ is due to the fine grain, and reasonable toughness(160~00J) in the intercritical reheated HZA is achieved by the addition of small amount of carbon which affects the formation of "M-A". Cu precipitated during ageing for increasing the strength of base metal is dissolved during single thermal cycle to $1,350^{\circ}C$ and is precipitated little on cooling and heating during subsequent weld thermal cycle. Thus, the decrease of toughness does not occur owing to the precipitation of Cu.

• Journal of the Korean institute of surface engineering
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• v.49 no.4
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• pp.376-381
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• 2016

The effects of ICP (Inductively Coupled Plasma) power, ranging from 0 to 200 W, on the crystal structure, microstructure, surface roughness and mechanical properties of magnetron sputtered VN coatings were systematically investigated with FE-SEM, AFM, XRD and nanoindentation. The results show that ICP power has a significant influence on coating microstructure and mechanical properties of VN coatings. With the increasing of ICP power, coating microstructure evolves from a porous columnar structure to a highly dense one. Average crystal grain size of single phase cubic fcc VN coatings was decreased from 10.1 nm to 4.0 nm with increase of ICP power. The maximum hardness of 28.2 GPa was obtained for the coatings deposited at ICP power of 200 W. The smoothest surface morphology with Ra roughness of 1.7 nm was obtained from the VN coating sputtered at ICP power of 200 W.

• Journal of Ceramic Processing Research
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• v.20 no.6
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• pp.582-588
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• 2019

FeVSb1-xTex (0.02 ≤ x ≤ 0.10) half-Heusler alloys were fabricated by mechanical alloying process and subsequent vacuum hot pressing. Near single half-Heusler phases are formed in vacuum hot pressed samples but a second phase of FeSb2 couldn't be avoided. After doping, the lattice thermal conductivity in the system was shown to decrease with increasing Te concentration and with increasing temperature. The lowest thermal conductivity was achieved for FeVSb0.94Te0.06 sample at about 657 K. This considerable reduction of thermal conductivities is attributed to the increased phonon scattering enhanced by defect structure, which is formed by doping of Te at Sb site. The phonon scattering might also increase at grain boundaries due to the formation of fine grain structure. The Seebeck coefficient increased considerably as well, consequently optimizing the thermoelectric figure of merit to a peak value of ~0.24 for FeVSb0.94Te0.06. Thermoelectric properties of various Te concentrations were investigated in the temperature range of around 300~973 K.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.24 no.12
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• pp.969-976
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• 2011

In this study we aims to evaluate the effects of 1/3 mol% $Co_3O_4$ addition on the reaction, microstructure development, resultant electrical properties, and especially the bulk trap and grain boundary properties of $ZnO-Bi_2O_3-Sb_2O_3$ (Sb/Bi=2.0, 1.0, and 0.5) system (ZBS). The samples were prepared by conventional ceramic process, and characterized by XRD, density, SEM, I-V, impedance and modulus spectroscopy (IS & MS) measurement. In addition of $Co_3O_4$ in $ZnO-Bi_2O_3-Sb_2O_3$ (ZBSCo), the phase development, density, and microstructure were controlled by Sb/Bi ratio. Pyrochlore on cooling was reproduced in all systems. The more homogeneous microstructure was obtained in ZBSCo (Sb/Bi=1.0) system. In ZBSCo, the varistor characteristics were improved drastically (non-linear coefficient ${\alpha}$=23~50) compared to ZBS. Doping of $Co_3O_4$ to ZBS seemed to form $V^{\cdot}_o$(0.33 eV) as dominant defect. From IS & MS, especially the grain boundary of Sb/Bi=0.5 system is composed of electrically single barrier (0.93 eV) and somewhat sensitive to ambient oxygen with temperature.