• Journal of the Korean Magnetics Society
• /
• v.20 no.5
• /
• pp.182-186
• /
• 2010

Effect of cobalt substitution on the sintering behavior and magnetic properties of a NiZnCu ferrite was studied. $Ni_{0.36-x}Co_xZn_{0.44}Cu_{0.22}Fe_{1.98}O_4(0{\leq}x{\leq}0.04)$ ferrite was fabricated by a solid stat reaction method. It was proposed and experimentally verified that $Co^{2+}$ substituted NiZnCu ferrite was effective on improving the quality factor and magnetic properties of NiZnCu ferrites for multilayer chip inductors. The ferrite was sintered without sintering aids, at $880{\sim}920^{\circ}C$, for 2 h and the initial permeability, quality factor, density, shrinkage, saturation magnetization, and coercivity were also measured. The quality factor (Q) was increased linearly up to x = 0.01 and decreased rapidly over x = 0.01. As the cobalt content increased, the initial permeability and density of the ferrites decreases. The initial permeability of toroidal sample for $Ni_{0.35}Co_{0.01}Zn_{0.44}Cu_{0.22}Fe_{1.98}O_4$ ferrites sintered at $900^{\circ}C$ was 130 at 1 MHz and quality factor was 230.

• Journal of the Korean Magnetics Society
• /
• v.12 no.5
• /
• pp.195-200
• /
• 2002

Low temperature sintering of Co$_2$Z type Ba ferrites with various oxide additives has been studied. Co$_2$Z phase was obtained by 2 step calcination and XRD peaks showed a good agreement with the peaks of the standard Co$_2$Z phase, except for some minor extra peaks. ZnO-B$_2$O$_3$ glass, ZnO-B$_2$O$_3$ and CuO, ZnO-B$_2$O$_3$ and Bi$_2$O$_3$, and ZnO-Bi$_2$O$_3$ glass were added to lower sintering temperatures. Specimens were sintered at the temperature range between 900 $^{\circ}C$ and 1000 $^{\circ}C$. In the single addition of ZnO-B$_2$O$_3$ glass, the specimen with 7.5 wt％ showed the highest shrinkage. Specimens with complex addition of ZnO-B$_2$O$_3$ glass with CuO or Bi$_2$O$_3$ showed higher shrinkages and initial permeabilities than single addition of ZnO-B$_2$O$_3$ glass. Shrinkages and initial permeabilities of the specimens with ZnO-Bi$_2$O$_3$ glass were higher than those of ZnO-B$_2$O$_3$ glass addition.

• Journal of the Korean Society of Clothing and Textiles
• /
• v.23 no.6
• /
• pp.853-863
• /
• 1999

the change of physical properties (thickness, weight, air permeability) and mechanical properties(abrasion resistance breaking load and displacement) of samples were determined after heat exposure by a RPP tester. The effect of exposure time and heat flux intensity on the changes and the relationship between physical properties and mechanical properties were investigated. FR treated cotton Kevlar/PBI and Nomex with different structureal characteristics were chosen for specimens. The changes of physical properties and mechanical properties were calculated based on their initial values before heat exposure. The longer exposure time and the high heat flux intensity the more changes of those properties. Heat flux intensity was more effective on the changes, The showed to be affected by an interplay of shrinkage and pyrolysis products loss. The changes of thickness and abrasion resistance showed to be higher for plain weave fabric and those of air permeabiliyt and breaking load and displacement for twill weave fabric. While FR treated cotton which have high RPP value experienced serious and detrimental changes after heat exposure Kevlar/PBI which has low RPP value showed no high changes. In conclusion it could be confirmed that when total performance of a protective clothing is estimated retention capability of physical and mechanical properties after heat exposure as well as RPP value must be considered.

• Journal of the Korea Institute of Building Construction
• /
• v.20 no.5
• /
• pp.433-440
• /
• 2020

In this study, a new type of Durometer was invented by modifying the currently used Durometer with the hemisphere shaped needle to columnar shaped needle. The aim of the study is, hence, to provide the feasibility of the advanced Durometer for assessing setting time of the concrete. Generally, the finishing of concrete surface should be conducted to secure the smooth surface, improve the permeability, and prevent the plastic shrinkage cracking. Although this surface finishing work should be conducted during the plastic phase between initial and final setting, currently in practical situations, the timing of starting the finishing work was determined by the sense of the worker. To improve this situation, Kato Junji suggested to use the hemisphere and needle shaped Durometers to determine the initial and final setting time, respectively. However, in this case, there are difficulties of using two different Durometers and of occurring failure of the Durometer due to the intruded cement paste. To prove the feasibility of new typed Durometer, setting time and surface hardness were evaluated by applying for the concrete with various replacing ratios of fly-ash and coal gasification slag as an aggregate.

• KSCE Journal of Civil and Environmental Engineering Research
• /
• v.29 no.1A
• /
• pp.101-108
• /
• 2009

The performance of high-early strength pavement concrete for large areas is influenced by the physical and chemical environment during service life. Generally, penetration, diffusion, and absorption of harmful materials that exist outside the concrete cause damage to its structure. Thus, we have to use a mixture for durability to keep the required quality for the planned service life. Moreover, in using high-early-strength cement and accelerators, a high heat of hydration to create the initial strength can cause cracks. Based on evaluations from optimal mix proportions of high-early-strength pavement concrete for large areas, we conducted water permeability, abrasion resistance, freeze-thaw, plastic, drying, and autogenous shrinkage tests. Test result showed that a mix of accelerator and PVA fibers showed excellent performance.

• Journal of the Korean Magnetics Society
• /
• v.18 no.2
• /
• pp.58-62
• /
• 2008

$Ni_{0.4}Zn_{0.4}Cu_{0.2}Fe_2O_4$ ferrite was fabricated by solid stat reaction method and sol-gel method. Because of the drawbacks of each method, we combined these two methods together. We proposed and experimentally verified that nanocrystalline ferrite additive was effective on improving the densification behavior and magnetic properties of NiZnCu ferrites for multilayer chip inductors. The initial permeability of the toroidal core Sample with 20 wt% nanocrystalline ferrite increased from 78.1 to 178.2 as annealing temperature is increased from $880^{\circ}C$ to $920^{\circ}C$. The density, shrinkage and saturation magnetization were increased with increasing annealing temperature, which was attributed to the decrease of additive grain size and increase of sintering density.

• Magazine of the Korean Society of Agricultural Engineers
• /
• v.26 no.1
• /
• pp.52-72
• /
• 1984

This study was performed to obtain the basic data which can be applied to the use of epoxy resin mortars. The data was based on the properties of epoxy resin mortars depending upon various mixing ratios to compare those of cement mortar. The resin which was used at this experiment was Epi-Bis type epoxy resin which is extensively being used as concrete structures. In the case of epoxy resin mortar, mixing ratios of resin to fine aggregate were 1: 2, 1: 4, 1: 6, 1: 8, 1:10, 1 :12 and 1:14, but the ratio of cement to fine aggregate in cement mortar was 1 : 2.5. The results obtained are summarized as follows; 1.When the mixing ratio was 1: 6, the highest density was 2.01 g/cm$^3$, being lower than 2.13 g/cm$^3$ of that of cement mortar. 2.According to the water absorption and water permeability test, the watertightness was shown very high at the mixing ratios of 1: 2, 1: 4 and 1: 6. But then the mixing ratio was less than 1 : 6, the watertightness considerably decreased. By this result, it was regarded that optimum mixing ratio of epoxy resin mortar for watertight structures should be richer mixing ratio than 1: 6. 3.The hardening shrinkage was large as the mixing ratio became leaner, but the values were remarkably small as compared with cement mortar. And the influence of dryness and moisture was exerted little at richer mixing ratio than 1: 6, but its effect was obvious at the lean mixing ratio, 1: 8, 1:10,1:12 and 1:14. It was confirmed that the optimum mixing ratio for concrete structures which would be influenced by the repeated dryness and moisture should be rich mixing ratio higher than 1: 6. 4.The compressive, bending and splitting tensile strenghs were observed very high, even the value at the mixing ratio of 1:14 was higher than that of cement mortar. It showed that epoxy resin mortar especially was to have high strength in bending and splitting tensile strength. Also, the initial strength within 24 hours gave rise to high value. Thus it was clear that epoxy resin was rapid hardening material. The multiple regression equations of strength were computed depending on a function of mixing ratios and curing times. 5.The elastic moduli derived from the compressive stress-strain curve were slightly smaller than the value of cement mortar, and the toughness of epoxy resin mortar was larger than that of cement mortar. 6.The impact resistance was strong compared with cement mortar at all mixing ratios. Especially, bending impact strength by the square pillar specimens was higher than the impact resistance of flat specimens or cylinderic specimens. 7.The Brinell hardness was relatively larger than that of cement mortar, but it gradually decreased with the decline of mixing ratio, and Brinell hardness at mixing ratio of 1 :14 was much the same as cement mortar. 8.The abrasion rate of epoxy resin mortar at all mixing ratio, when Losangeles abation testing machine revolved 500 times, was very low. Even mixing ratio of 1 :14 was no more than 31.41%, which was less than critical abrasion rate 40% of coarse aggregate for cement concrete. Consequently, the abrasion rate of epoxy resin mortar was superior to cement mortar, and the relation between abrasion rate and Brinell hardness was highly significant as exponential curve. 9.The highest bond strength of epoxy resin mortar was 12.9 kg/cm$^2$ at the mixing ratio of 1:2. The failure of bonded flat steel specimens occurred on the part of epoxy resin mortar at the mixing ratio of 1: 2 and 1: 4, and that of bonded cement concrete specimens was fond on the part of combained concrete at the mixing ratio of 1 : 2 ,1: 4 and 1: 6. It was confirmed that the optimum mixing ratio for bonding of steel plate, and of cement concrete should be rich mixing ratio above 1 : 4 and 1 : 6 respectively. 10.The variations of color tone by heating began to take place at about 60˚C, and the ultimate change occurred at 120˚C. The compressive, bending and splitting tensile strengths increased with rising temperature up to 80˚ C, but these rapidly decreased when temperature was above 800 C. Accordingly, it was evident that the resistance temperature of epoxy resin mortar was about 80˚C which was generally considered lower than that of the other concrete materials. But it is likely that there is no problem in epoxy resin mortar when used for unnecessary materials of high temperature resistance. The multiple regression equations of strength were computed depending on a function of mixing ratios and heating temperatures. 11.The susceptibility to chemical attack of cement mortar was easily affected by inorganic and organic acid. and that of epoxy resin mortar with mixing ratio of 1: 4 was of great resistance. On the other hand, when mixing ratio was lower than 1 : 8 epoxy resin mortar had very poor resistance, especially being poor resistant to organicacid. Therefore, for the structures requiring chemical resistance optimum mixing of epoxy resin mortar should be rich mixing ratio higher than 1: 4.