• 제목/요약/키워드: sensitivity increasing method

검색결과 245건 처리시간 0.031초

Simultaneous Analysis of Cholesterol Oxidation Products (COPs) in Powdered Milk Using HPLC/UV-Vis

  • Lee, Jin Joo;Myung, Seung-Woon
    • Bulletin of the Korean Chemical Society
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    • 제34권9호
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    • pp.2787-2794
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    • 2013
  • Cholesterol and cholesterol oxidation products (COPs) may accumulate in foods of animal origin during processing or storage. An effective and sensitive analytical method was developed by increasing the UV absorption of compounds through derivatization by attaching a chromophore to the functional groups of cholesterols (cholesterol, 20-hydroxycholesterol, 7-ketocholesterol, cholestane-$3{\beta}$-$5{\alpha}$-$6{\beta}$-triol, 25-hydroxycholesterol, and $5,6{\alpha}$-epoxycholesterol). The influences of the reaction time, volume of reaction solvent, amounts of derivatizing reagent, and extraction solvents were investigated, as they may influence the reaction and extraction yield. The derivatized COPs were analyzed simultaneously on a C18 column (2.1 mm i.d. ${\times}$ 100 mm length, $3.5{\mu}m$ particle size) using a gradient elution with water and acetonitrile. The derivatized COPs showed increased sensitivity and selectivity in HPLC/UV-Vis. The LOD and LOQ were in the concentration ranges of 0.018-0.55 mg/kg and 0.059-1.84 mg/kg from the powdered milk. And the accuracy and precision were 78.1-116.7% and 1.1-9.9%, respectively.

레이저 스페클 간섭법을 이용한 면내변위 측정시스템 개발 (The Development of In-Plane Displacement Measurement System on Laser Speckle Interferometry)

  • 윤홍석;김경석;박찬주;최태호;최정석
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 2005년도 춘계학술대회 논문집
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    • pp.556-560
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    • 2005
  • The measurement method by Laser Speckle Interferometry which uses the interference law which will grow precedes and with it explains a resolution measurement ability and together the change of place arrowhead and general measurement, at real-time measurement sensitivity it has application boat song from candle precise measurement field it is increasing. But, currently the domestic application technique to sleeps and optical science military merit by optical science interferometer and directness it composes purchases to the level which it applies the expensive commercial business equipment the outside and in spite of the technical ripple effect is deficient even in many strong point. The hazard which complements like this problem point form technical development it leads from the research which it sees and an application degree and to sleep as the measurement equipment which tries to develop the small-sized optical science interference sensor and an interpretation program it raises it does.

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Optimum time-censored ramp soak-stress ALT plan for the Burr type XII distribution

  • Srivastava, P.W.;Gupta, T.
    • International Journal of Reliability and Applications
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    • 제15권2호
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    • pp.125-150
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    • 2014
  • Accelerated life tests (ALTs) are extensively used to determine the reliability of a product in a short period of time. Test units are subject to elevated stresses which yield quick failures. ALT can be carried out using constant-stress, step-stress, progressive-stress, cyclic-stress or random-stress loading and their various combinations. An ALT with linearly increasing stress is ramp-stress test. Much of the previous work on planning ALTs has focused on constant-stress, step-stress, ramp-stress schemes and their various combinations where the stress is generally increased. This paper presents an optimal design of ramp soak-stress ALT model which is based on the principle of Thermal cycling. Thermal cycling involves applying high and low temperatures repeatedly over time. The optimal plan consists in finding out relevant experimental variables, namely, stress rates and stress rate change points, by minimizing variance of reliability function with pre-specified mission time under normal operating conditions. The Burr type XII life distribution and time-censored data have been used for the purpose. Burr type XII life distribution has been found appropriate for accelerated life testing experiments. The method developed has been explained using a numerical example and sensitivity analysis carried out.

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Free vibrations of precast modular steel-concrete composite railway track slabs

  • Kimani, Stephen Kimindiri;Kaewunruen, Sakdirat
    • Steel and Composite Structures
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    • 제24권1호
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    • pp.113-128
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    • 2017
  • This paper highlights a study undertaken on the free vibration of a precast steel-concrete composite slab panel for track support. The steel-concrete composite slab track is an evolvement from the slab track, a form of ballastless track which is becoming increasingly attractive to asset owners as they seek to reduce lifecycle costs and deal with increasing rail traffic speeds. The slender nature of the slab panel due to its reduced depth of construction makes it susceptible to vibration problems. The aim of the study is driven by the need to address the limited research available to date on the dynamic behaviour of steel-concrete composite slab panels for track support. Free vibration analysis of the track slab has been carried out using ABAQUS. Both eigenfrequencies and eigenmodes have been extracted using the Lanczos method. The fundamental natural frequencies of the slab panel have been identified together with corresponding mode shapes. To investigate the sensitivity of the natural frequencies and mode shapes, parametric studies have been established, considering concrete strength and mass and steel's modulus of elasticity. This study is the world first to observe crossover phenomena that result in the inversion of the natural orders without interaction. It also reveals that replacement of the steel with aluminium or carbon fibre sheeting can only marginally reduce the natural frequencies of the slab panel.

광학식 자유곡면 형상복원 알고리즘 개발 (A algorithm development on optical freeform surface reconstruction)

  • 김병창
    • 한국융합학회논문지
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    • 제7권5호
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    • pp.175-180
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    • 2016
  • 광기전공학 기술이 융합된 광학계의 발달은 광학계를 구성하는 부품의 표면이 비구면 또는 자유곡면으로 진화하고 있다. 본 논문에서는 광학식 자유곡면의 국부영역으로부터 직교하는 2방향의 곡률을 정의하여 전체 형상을 복원하는 알고리즘을 제안하였다. 8.4 m 자유곡면 형상을 가진 반사거울에 구현된 알고리즘을 적용한 결과 형상 복원 최대오차 0.065 nm, 평균제곱근 오차 0.013 nm로 복원됨을 확인하였다. 프루브의 위치오차 발생에 대한 노이즈 민감도를 해석한 결과, 2 mm 오차에 대해서도 형상복원 최대오차 30 nm, 제곱평균제곱근 오차 8.7 nm로 위치 오차에 매우 둔감한 알고리즘임을 확인하였다.

Ag/AsGeSeS 다층박막에서의 이색성 측정 (Measurement of the photoinduced Dichoism in Ag/AsGeSeS multilayer thin films)

  • 신경;여철호;이정태;박정일;이영종;정홍배
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2002년도 춘계학술대회 논문집 디스플레이 광소자 분야
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    • pp.81-84
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    • 2002
  • The chalcogenide glasses of thin films have the superior property of photoinduced anisotrophy(PA). In this study, we observed the linear dichroism(D) using the irradiation with polarized He-Ne laser light, in the $Ag/As_{10}Ge_{10}Se_{15}S_{35}$ multi-layer. Mutilayer structures formed by alternating metal(Ag) and chalcogenide($As_{10}Ge_{10}Se_{15}S_{35}$). The Ag polarized photodoping result in reducing time of saturation anisotrophy and increasing sensitivity of linearly anisotrophy intensity, up to maximum 220%. In the thin films of chalcogenide, the Ag polarized photodoping will be show a capability of new method that suggested more improvement of photoinduced anisotrophy property.

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마이크로파 Reflectometry의 소신호 응답 특성 (Small Signal Response Characteristics of Microwave Reflectometry)

  • 방성근
    • 한국전자파학회논문지
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    • 제14권7호
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    • pp.699-704
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    • 2003
  • 레이다기법을 이용한 마이크로파 Reflectometry를 비균질 매질의 밀도 특성을 조사하기 위한 비파괴검사 장치로 응용하기 위한 시스템 특성을 연구하였다. 마이크로파 Reflectometry로 비균질 매질을 조사하기 위해서는 대상에 따른 시스템의 하드웨어 구성이 최적화되어야 하며, 각 시스템에서의 소신호 반응특성이 이해되어야만 전체적인 시스템 해법을 제공하는 것이 된다. 그 중에서 플라즈마 연구분야에 응용하기 시작한 것은 비교적 최근의 일로서 그 활용도가 점차 증가하고 있는 경향이다. 조사하는 대상의 특성에 따른 시스템의 구성을 이해하고, 파동수 및 밀도 섭동에 관한 시스템의 특성을 조사하기 위한 장치를 제안하며, 실험적 방법의 결과와 1차원 파동방정식을 이용한 수치해석적 결과를 비교 검증하였다.

Damped frequencies of precast modular steel-concrete composite railway track slabs

  • Kaewunruen, Sakdirat;Kimani, Stephen Kimindiri
    • Steel and Composite Structures
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    • 제25권4호
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    • pp.427-442
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    • 2017
  • This paper presents unprecedented damped oscillation behaviours of a precast steel-concrete composite slab panel for track support. The steel-concrete composite slab track is an innovative slab track, a form of ballastless track which is becoming increasingly attractive to asset owners as they seek to reduce lifecycle costs and deal with increasing rail traffic speeds. The slender nature of the slab panel due to its reduced depth of construction makes it susceptible to vibration problems. The aim of the study is driven by the need to address the limited research available to date on the dynamic behaviour of steel-concrete composite slab panels for track support. Free vibration analysis of the track slab has been carried out using ABAQUS. Both undamped and damped eigenfrequencies and eigenmodes have been extracted using the Lancsoz method. The fundamental natural frequencies of the slab panel have been identified together with corresponding mode shapes. To investigate the sensitivity of the natural frequencies and mode shapes, parametric studies have been established, considering concrete strength and mass and steel's modulus of elasticity. This study is the world first to observe crossover phenomena that result in the inversion of the natural orders without interaction. It also reveals that replacement of the steel with aluminium or carbon fibre sheeting can only marginally reduce the natural frequencies of the slab panel.

소형 연료전지 연계형 DC GRID 부하 특성 실험 (Load Characteristics of the DC GRID Connected to Small Fuel Cells)

  • 이상우;권오성;이상철;배준형;박태준;강진규;이동하
    • 한국태양에너지학회:학술대회논문집
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    • 한국태양에너지학회 2012년도 춘계학술발표대회 논문집
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    • pp.414-418
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    • 2012
  • In recent years, understanding the dynamics of DC distribution system has become critically important due mainly to the increasing needs for the interconnection of DC distributed generators and the (DC-based) electric vehicle (EV) charging systems. In this paper, the characteristics of the DC grid system connected to the compact proton exchange membrane fuel cell (PEMFC) has been studied. In particular, the voltage and current transient phenomena were measured by varying the load of the DC grid system. Also, the voltage and current ripple were measured at the different load conditions. Our experimental results clearly manifested that the study contributes to the establishment of fundamental method to characterize the small DC grid system including distributed generation.

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문화간호역량 개념 분석 (A Concept Analysis of Cultural Nursing Competence)

  • 정금희;박혜숙;김경원;김영희;이선희;김현경
    • 여성건강간호학회지
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    • 제22권2호
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    • pp.86-95
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    • 2016
  • Purpose: The aim of this study was to conduct a concept analysis of cultural nursing competence. Methods: Cultural nursing competence was analyzed using Rodgers' evolutionary concept development method. A literature search using the keywords "cultural nursing competence", "intercultural nursing competence", "cultural nursing", "cultural health nursing", and "cultural competence" was conducted in PubMed, CINAHL, ERIC, and RISS on material published before 2015. Database and bibliographic searches yielded 35 records. Results: Cultural nursing competence comprised cognitive, affective, and behavioral domains. The critical attributes of the concept were sensitivity, equality, and activity. The analysis identified the following dimensions: awareness, openness, and coherence. The consequences of cultural nursing competence were personal satisfaction and social justice. The definition contained competence on both an individual and social level. Conclusion: Cultural competency enhances quality of care by narrowing health disparities and increasing client satisfaction. The concept analysis of cultural nursing competence may offer an acceptable framework which can be used to develop psychometric tools of this concept and provide guidelines in nursing practice.