• Title/Summary/Keyword: self calibration

Search Result 186, Processing Time 0.021 seconds

Mapping of Work Function in Self-Assembled V2O5 Nanonet Structures

  • Park, Jeong Woo;Kim, Taekyeong
    • Journal of the Korean Chemical Society
    • /
    • v.61 no.1
    • /
    • pp.12-15
    • /
    • 2017
  • We presented a mapping the work function of the vanadium pentoxide ($V_2O_5$) nanonet structures by scanning Kelvin probe microscopy (SKPM). In this measurement, the $V_2O_5$ nanonet was self-assembled via dropping the solution of $V_2O_5$ nanowires (NWs) onto the $SiO_2$ substrate and drying the solvent, resulting in the networks of $V_2O_5$ NWs. We found that the SKPM signal as a surface potential of $V_2O_5$ nanonet is attributed to the contact potential difference (CPD) between the work functions of the metal tip and the $V_2O_5$ nanonet. We generated the histograms of the CPD signals obtained from the SKPM mapping of the $V_2O_5$ nanonet as well as the highly ordered pyrolytic graphite (HOPG) which is used as a reference for the calibration of the SKPM tip. By using the histogram peaks of the CPD signals, we successfully estimated the work function of ~5.1 eV for the $V_2O_5$ nanonet structures. This work provides a possibility of a nanometer-scale imaging of the work function of the various nanostructures and helps to understand the electrical characteristics of the future electronic devices.

Electrochemical Detection of Self-Assembled Viologen Modified Electrode as Mediator of Glucose Sensor

  • Lee, Dong-Yun;Choi, Won-Suk;Park, Sang-Hyun;Kwon, Young-Soo
    • Journal of Electrical Engineering and Technology
    • /
    • v.4 no.1
    • /
    • pp.106-110
    • /
    • 2009
  • An amperometric glucose biosensor has been developed using viologen derivatives as a charge transfer mediator between a glucose oxidase (GOD) and a gold electrode. A highly stable self-assembled monolayer (SAM) of thiol-based viologen was immobilized onto the gold electrode of a quartz crystal microbalance (QCM) and GOD was immobilized onto the viologen modified electrode. This biosensor response to glucose was evaluated amperometrically in the potential of -300mV. Upon immobilization of the glucose oxidase onto the viologen modified electrode, the biosensor showed rapid response towards glucose. Experimental conditions influencing the biosensor performance, such as pH potential, were optimized and assessed. This biosensor offered excellent electrochemical responses for glucose concentration below ${\mu}$ mol level with high sensitivity and selectivity and short response time. The levels of the RSDs (<5%) for the entire analyses reflected the highly reproducible sensor performance. A linear calibration range between the current and the glucose concentration was obtained up to $4.5{\times}10^{-4}M$. The detection limit was determined to be $3.0{\times}10^{-6}M$.

Experimental investigation of thin steel plate shear walls with different infill-to-boundary frame connections

  • Vatansever, Cuneyt;Yardimci, Nesrin
    • Steel and Composite Structures
    • /
    • v.11 no.3
    • /
    • pp.251-271
    • /
    • 2011
  • To make direct comparisons regarding the cyclic behavior of thin steel plate shear walls (TSPSWs) with different infill-to-boundary frame connections, two TSPSWs were tested under quasi-static conditions, one having the infill plate attached to the boundary frame members on all edges and the other having the infill plate connected only to the beams. Also, the bare frame that was used in the TSPSW specimens was tested to provide data for the calibration of numerical models. The connection of infill plates to surrounding frames was achieved through the use of self-drilling screws to fish plates that were welded to the frame members. The behavior of TSPSW specimens are compared and discussed with emphasis on the characteristics important in seismic response, including the initial stiffness, ultimate strength and deformation modes observed during the tests. It is shown that TSPSW specimens achieve significant ductility and energy dissipation while the ultimate failure mode resulted from infill plate fracture at the net section of the infill plate-to-boundary frame connection after substantial infill plate yielding. Experimental results are compared to monotonic pushover predictions from computer analysis using strip models and the models are found to be capable of approximating the monotonic behavior of the TSPSW specimens.

Development of Self-Driven Pneumatic Robot for Boresonic Examination of Turbine Rotor (터빈로터 중심공 검사용 자기주행 공압형 로봇 개발)

  • Kang, Baejun;An, Myungjae;Lee, Chul-Hee
    • Journal of Drive and Control
    • /
    • v.18 no.1
    • /
    • pp.31-38
    • /
    • 2021
  • This study presents a new principle for driving the robot aimed at reducing the position error for the boresonic examination of turbine rotor. The conventional method of inspection is performed by installing manipulator onto the flange of the turbine rotor and connecting a pipe, which is then being pushed into the bore. The longer the pipe gets, the greater sagging and distortion appear, making it difficult for the ultrasonic sensor to contact with the internal surface of the bore. A pneumatic pressure will ensure the front or rear feet of the robot in close contact with the inner wall to prevent slipping, while the ball screw on the body of the robot will rotate to drive it in the axial direction. The compression force required for tight contact was calculated in the form of a three-point support, and a static structural simulation analysis was performed by designing and modeling the robot mechanism. The driving performance and ultrasonic detection ability have been tested by fabricating the robot, the test piece for ultrasonic calibration and the transparent mock-up for robot demonstration. The tests have confirmed that no slipping occurs at a certain pneumatic pressure or over.

The Characteristic Test for Gage Factors of Strain Gages in Cryogenic Environment (극저온 환경에서 스트레인 게이지의 게이지상수 및 변형률 측정에 관한 연구)

  • 김갑순;주진원
    • Transactions of the Korean Society of Mechanical Engineers
    • /
    • v.17 no.9
    • /
    • pp.2205-2213
    • /
    • 1993
  • The characteristic test for gage factors of temperature self-compensated strain gages at cryogenic temperature is presented. By joining the international round robin test on electrical strain gages at cryogenic temperatures, the gage factors of three kinds of widely-used strain gages are obtained at the room temperature, the temperatures of liquid nitrogen and liquid helium. The calibration system which produce precise bending strain is by mechanical loading at cryogenic temperature. This paper also presents the creep characteristic of strain gages at maximum strain level.

A 6-bit 3.3GS/s Current-Steering DAC with Stacked Unit Cell Structure

  • Kim, Si-Nai;Kim, Wan;Lee, Chang-Kyo;Ryu, Seung-Tak
    • JSTS:Journal of Semiconductor Technology and Science
    • /
    • v.12 no.3
    • /
    • pp.270-277
    • /
    • 2012
  • This paper presents a new DAC design strategy to achieve a wideband dynamic linearity by increasing the bandwidth of the output impedance. In order to reduce the dominant parasitic capacitance of the conventional matrix structure, all the cells associated with a unit current source and its control are stacked in a single column very closely (stacked unit cell structure). To further reduce the parasitic capacitance, the size of the unit current source is considerably reduced at the sacrifice of matching yield. The degraded matching of the current sources is compensated for by a self-calibration. A prototype 6-bit 3.3-GS/s current-steering full binary DAC was fabricated in a 1P9M 90 nm CMOS process. The DAC shows an SFDR of 36.4 dB at 3.3 GS/s Nyquist input signal. The active area of the DAC occupies only $0.0546mm^2$ (0.21 mm ${\times}$ 0.26 mm).

A Constrained Self-Calibration Technique (제약 조건을 적용한 셀프 캘리브레이션 방법)

  • Kim, Seong-Yong;Han, Jun-Hui
    • Journal of KIISE:Software and Applications
    • /
    • v.28 no.4
    • /
    • pp.358-368
    • /
    • 2001
  • 셀프 캘리브레이션은 영상 시퀀스에 대한 특징점 정합 결과를 이용하여 카메라 내부 파라미터를 계산하는 기법이다. 이는 임의로 움직이는 카메라를 이용하여 얻은 영상 시퀀스를 이용하여 유클리디안 복원을 수행하는데 응용될 수 있다. 안정적인 3차원 복원결과를 얻기 위하여 본 논문에서는 두 가지 제약 조건을 사용한다(카메라 내부 파라미터의 개수에 대한 제약 조건과 복원할 장면의 기하학적 구조를 이용한 제약 조건). 카메라 내부 파라미터에 대한 제약 조건은 카메라의 하드웨어적인 특성을 반영하며 이러한 제약 조건을 적용함으로써 셀프 캘리브레이션 중 비선형 최적화 과정의 수렴도를 높일 수 있다. 또, 기하학적 제약 조건은 대상 장면의 직각 구조를 이용하여 이에 대한 조건을 분석하여 제약 조건에 대한 수식을 유도한 다음 이를 최적화 과정에 포함시킨다. 합성 영상과 다양한 종류의 실제 영상에 대한 실험을 통하여 본 논문에서 제안된 방법을 이용하면 개선된 유클리디안 복원 결과를 얻을 수 있음을 보인다.

  • PDF

The Use of Gas Chromatograph for the Measurement of Engine Exhaust Gas Composition (엔진 배기가스 성분 측정 을 위한 Gas Chromatograph 의 이용)

  • 김승수;정영교
    • Transactions of the Korean Society of Mechanical Engineers
    • /
    • v.9 no.6
    • /
    • pp.743-749
    • /
    • 1985
  • In this study the usefulness of Gas Chromatograph for the measurement of engine exhaust gas composition was confirmed. It was found that the composition of standard gas which was used for the calibration of Gas Chromatograph should not be greatly different from that of exhaust gas. Although self-evident, it cannot be overemphasized that utmost attention should be paid to prevent even a minute amount of air being mixed into the gas throughout the sampling process.

The Multiethnic Cohort Study of Diet and Cancer: Design and Early Findings

  • Kolonel, Laurence N.
    • Nutritional Sciences
    • /
    • v.7 no.1
    • /
    • pp.53-58
    • /
    • 2004
  • The Multiethnic Cohort Study was designed to study prospectively the relationship of diet and other lifestyle factors to the risk of cancer. The cohort was established in 1993-1996 in Hawaii and California (primarily Los Angeles) and included a representative sample of more than 215,000 men and women primarily from five different ethnic groups: Japanese, whites, Native Hawaiians, Latinos, and African- Americans. Because of the emphasis on diet, great attention was paid to developing and pre-testing a self-administered quantitative food frequency questionnaire that would adequately assess food and nutrient intakes in these groups. An extensive food composition database was also created for the study. In addition, during data collection, a calibration study was conducted that makes possible adjustment for measurement error in nutrient intakes and valid comparison of intakes across the several ethnic groups. At the present time, blood and urine specimens are being collected from cohort participants and should yield a biorepository of more than 80,000 subjects. Baseline data indicate that the cohort is well representative of the general population of Hawaii and California, so that results can be generalized. These data also show a wide range in dietary intakes and in other lifestyle variables that should facilitate the testing of etiologic hypotheses.

Measurement of Magnetic Field Generated by the Operations of Electric Appliance (전기기구의 운전에 의하여 발생되는 자계의 측정)

  • 이복희;길경석;박형기
    • The Transactions of the Korean Institute of Electrical Engineers
    • /
    • v.43 no.6
    • /
    • pp.1001-1009
    • /
    • 1994
  • The present paper deals with a new developed sensor for measuring the time-varying magnetic fields and describes the experimental results of trasient magnetic field that takes place during the operations of electric appliance. The operation principle of the self-integrating magnetic field sensor by using coaxial cable is analyzed and a calibration investigation is carried out. The frequency bandwidth of the magnetic field measurement system is from 40 Hz to about 300 kHz. The magnetic field induced by the starting and/or operation of electric appliance mainly includes the odd harmonics such as the third, the fifth and the seventh harmonics. The magnetic field intensity caused during the operation of ultrasonic washer is inversely proportional to distance, this correspodns to induction component. As a result, it was known that the odd harmonics of magnetic field in the desing of electromagnetic shield employed for protecting electronic circuit and control devices have to be considered.

  • PDF