• Title/Summary/Keyword: scanning microscopy

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An Evaluation of Antibacterial Titanium Surface For Dental Implant (치과용 임플란트 적용을 위한 항균력을 가진 티타늄 표면의 평가)

  • Kang, Min-Kyung;Moon, Seung-Kyun;Kim, Kyoung-Nam
    • Journal of dental hygiene science
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    • v.11 no.5
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    • pp.405-410
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    • 2011
  • The aim of this study was to evaluate antibacterial effect of Cl coated titanium. To coat the Cl on the titanium, first, the titanium was modified by blasting treatment with hydroxyapatite and alumina powder. Anodization process was completed using electrolyte solution of 0.04 M ${\beta}$-glycerol phosphate disodium salt n-hydrate, 0.4 M calcium acetate n-hydrate and 1 M NaCl on the condition of 250 voltages for 3 min. Surface morphology and elements' observation were performed with scanning electron microscopy and energy dispersive spectroscopy and surface profiler was used to analyze the surface roughness. Antibacterial effect was evaluated by film adhesion method. The anodized titanium after blasting showed dimpled surface contained the Cl. Surface average roughness of these surfaces had significantly higher compared to polished titanium. Result of antibacterial test showed that anodized titanium after blasting had an enhanced antibacterial effect compared to the polished titanium. Therefore, these results suggested that titanium contained Cl by anodization after blasting had a rough surface as well as antibacterial effect.

Erosive Effect and Color of Mouthrinsing Solutions on Enamel Surface (시판중인 구강양치용액의 법랑질 표면의 착색과 침식에 미치는 영향)

  • Jeong, Kyung-Yi;Lee, Hye-Jin;Park, Young-Nam
    • Journal of dental hygiene science
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    • v.11 no.5
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    • pp.397-404
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    • 2011
  • The aims of this study were to evaluate the effect of native acidity upon dental hard tissues by measuring pH in mouth-rinse, which is on the market, and to evaluate even influence of dental stain caused by mouse-rinse given using for a long time. The experimental group was used Garglin, Nextcare, Listerine, and Hexamedin. The control group was used sterile distilled water. As a result, pH was indicated to be low in Nextcare(4.70) and Listerine(4.16). In a change of color tone, $b^*$ value of indicating Yellow-blue showed the lower value than the early color tone in all groups. There was statistical significance in Nextcare and Listerine. ${\Delta}L^*$ value of indicating light -dark gets darker after using Nextcare, Listerine and Hexamedine. A change(VHN) in surface hardness of enamel showed reduction in surface hardness after 14 days in Nexcare and Listerine. As a result of confirming a change in enamel surface by using Scanning Electron Microscopy, the erosion aspect on the enamel surface could be confirmed in groups of Nexcare and Listerine. Ra value in surface roughness of enamel could be observed the enamel surface, which got rougher compared to other experimental groups.

Quality Characteristics of Yellow Layer Cake Prepared with Different Levels of Adenophora remotiflora Powder (모시대 분말 첨가 수준에 따른 옐로우 레이어 케이크의 품질 특성)

  • Choi, Yoon-Hee;Bae, Song-Hwan;Park, Jeong-Woo;Cho, Nam-Ji;Han, Myung-Ryun;Kim, Young-Ho;Yoon, Seong-Jun;Kim, Myung-Hwan;Kim, Ae-Jung
    • Journal of the East Asian Society of Dietary Life
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    • v.19 no.5
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    • pp.736-742
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    • 2009
  • The purpose of this study was to improve the quality of yellow layer cake by adding the Adenophora remotiflora powder. The effects of the Adenophora remotiflora powder in on the final product quality of yellow layer cake and the optimum amount of the Adenophora remotiflora powder in the yellow layer cake formula were investigated. The more increased amounts of Adenophora remotiflora powder was added to the samples, the resulted in "L", and Hunter's "a" and "b" values of the crust color of yellow layer cake were significantly decreased (p<0.05). In the case of crumb color, the more increased levels of Adenophora remotiflora powder led to the samples, the "L" and "a" values were significantly decreased (p<0.05), but "b" value increased significantly (p<0.05). As more Adenophora remotiflora powder was added to the cake samples, the Hardness, Gumminess and Chewiness were significantly increased (p<0.05), but Springiness and Cohesiveness were did not. The results of sensory evaluation showed revealed that the addition of 2% of Adenophora remotiflora powder of overall acceptability were most preferred. Larger scanning electron microscopy revealed the presence of numbers of greater concentrations of cells with different sizes were observed for in samples from products that received 1 % Adenophora remotiflora powder addition. Collapsed cells and cell coalescence with big large and irregular shapes were shown observed in samples that were amended with at 2, 4, and 8% addition Adenophora remotiflora power. The addition of Adenophora remotiflora powder was shown to improved the functionality and quality characteristics such as color, taste and flavor of yellow layer cake. Therefore, it was expected that the 2% addition of Adenophora remotiflora powder will improve the preference to the yellow layer cake.

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The systematic consideration of leaf epidermal microstructure in the tribe Forsythieae and its related genera (Oleaceae) (개나리족 및 근연분류군(물푸레나무과)의 잎 표피 미세구조에 대한 분류학적 검토)

  • Song, Jun-Ho;Hong, Suk-Pyo
    • Korean Journal of Plant Taxonomy
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    • v.43 no.2
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    • pp.118-127
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    • 2013
  • A comparative study of leaf epidermal microstructure in tribes Forsythieae (Abeliophyllum: 1 species, Forsythia: 12 taxa - 10 species, 2 varieties), Fontanesieae (Fontanesia: 2 species) including one related genus Myxopyrum belonging to Myxopyreae (Myxopyrum: 5 taxa - 4 species, 1 subspecies) was carried out using scanning electron microscopy (SEM) in order to evaluate their significance in the taxonomy. The leaves of investigated taxa are either hypostomatic or amphistomatic, but former is more frequent. The size range of the guard cells is 17.14-47.58 ${\times}$ 11.59- 44.25 ${\mu}m$: the smallest one was found in Forsythia giraldiana (17.48-22.96 ${\times}$ 11.64-12.88 ${\mu}m$), while the largest one was measured to Myxopyrum pierrei (31.50-41.75 ${\times}$ 32.53-44.25 ${\mu}m$). Anomocytic stomatal complex are most frequent type (rarely paracytic), usually both anomocytic and anisocytic occur in one leaf. In surface view both adaxial and abaxial anticlinal walls of the subsidiary cells are variable (e.g., straight/curved, undulate, sinuate, undulate/sinuate). Three types (simple unicellular and multicellular non-glandular, subsessile glandular) of trichomes are found in leaves. Finally, the systematic significance of the leaf epidermal micromorphological characters in idenfitication and elucidation of these tribe, between or within the genera including among the species is also briefly discussed.

Effects of Whitmania pigra on the expressions of cytokine genes in human THP-1 cells (수질(水蛭)이 THP-1세포의 사이토카인 유전자 발현에 미치는 영향)

  • Kim, Hyun-Ji;Kim, Gyung-Jun
    • The Journal of Korean Medicine Ophthalmology and Otolaryngology and Dermatology
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    • v.26 no.1
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    • pp.19-34
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    • 2013
  • Objective : This study was performed to evaluate the effect of immune reaction inductive substances such as PMA, LPS, DPE, DNCB and WP, the whitman pigra extracting substance at simultaneously on the translocation of $NF{\kappa}B$ towards to the nucleus and the mRNA expression patterns of various cytokine genes in THP-1 cells, monocytes of human. Methods : To analyze the cytokine genes expressions, the RT-PCR method was used, and measuring TNF-${\alpha}$ that had been secreted during cell culture by the ELISA method. The morphological changes were observed during THP-1 cell by a scanning electron microscope and the quantitative distribution of $NF{\kappa}B$ in the cell that was analyzed through immunocytochemistry and a confocal microscopy. Results : WP showed different influences onto the mRNA expression patterns of cytokine genes with PMA, LPS. DPE and DNCB according to the types of immune inductive substances in the THP-1 cells. Upon treating PMA and DPE on the THP-1 cells at the same time or either additionally treating WP thereon, the movement of $NF{\kappa}B$ increase towards the nucleus from cell cytoplasm was able to be observed. The expressions of IL-$1{\alpha}$ and IFN-${\gamma}$ induced by PMA and PMA+DNCB were suppressed by WP while the expression of TGF-${\beta}$ was promoted. Regarding the secretion pattern of TNF-${\alpha}$ according to the treatment of PMA, its secretion amount was incredibly increased by concurrent treatment of WP, however, in case of co-treatment of WP with PMA and DNCB, it was found that the secretion amount of TNF-${\alpha}$ decreased. Conclusions : In this study, the WP extracting substance was confirmed that it had an influence on expression patterns of cytokine genes according to the actions of a variety kinds of immune reaction inductive substances treated on the THP-1 cells. Especially, WP co-treatment with PMA and DNCB was suppressed the expression of inflammatory cytokines, such as IL-$1{\alpha}$, IFN-${\gamma}$ and TNF-${\alpha}$.

The Effects of the Addition of Cheese in the Manufacture of Rice Cakes Colored with 5 Vegetable-Derived Natural Coloring Materials (오색(五色) 채소 유래 천연 색소를 이용한 건강 맞춤형 컬러 치즈 떡 개발에 관한 연구)

  • Choi, Heeyoung;Lee, Seunggu;Choi, Haneul;Park, Jonghyuk;Heo, Changki;Oh, Jeonhui;Oh, Hyunhee;Jung, Hookil
    • Journal of Dairy Science and Biotechnology
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    • v.31 no.1
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    • pp.85-91
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    • 2013
  • In this study, the effects of adding cheese in the manufacture of rice cakes having 5 different vegetable-derived natural coloring materials were investigated with respect to quality characteristics during storage. Rice cake samples were prepared without (control) or with the addition of 2.0%, 3.0%, or 4.0% cheese. Changes in pH, external appearance, total solid content, and scanning electron microscopy (SEM), texture and sensory characteristics were monitored during storage. The sensory and texture characteristics of the rice cakes with cheese were investigated with respect to color, flavor, and overall acceptability. The total solid content and pH of the cheese-treated rice cakes were higher than that of the control during storage. Rice cakes added with cheese had higher liquid flavor than control. Results revealed that rice cakes added with cheese at less than 4% addition had the best taste, appearance, and sensory properties. Moreover, the addition of cheese to five-colored rice cakes provides additional nutrients while maintaining flavor and quality.

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Effect of Potassium Silicate on Growth and Leaf Epidermal Characteristics of Begonia and Pansy Grown in Vitro

  • Lim, Mi Young;Lee, Eun Ju;Jana, Sonali;Sivanesan, Iyyakkannu;Jeong, Byoung Ryong
    • Horticultural Science & Technology
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    • v.30 no.5
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    • pp.579-585
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    • 2012
  • This study was carried out to investigate the effect of potassium silicate on the growth and leaf epidermal characteristics of horticultural crops viz., begonia (Begonia semperflorens Link et Otto) 'Super Olympia Red' and 'Super Olympia Rose' and pansy (Viola ${\times}$ wittrockiana Hort.) 'Matrix White Blotch' and 'Matrix Yellow Blotch' in vitro. Seeds after germination were grown on a quarter strength MS medium supplemented with potassium silicate ($K_2SiO_3$) at 0, 100, 200, or $300mg{\cdot}L^{-1}$ and were maintained under a photoperiod of 16 hours at $25^{\circ}C$. Growth parameters such as plant height, root length, chlorophyll content, fresh, and dry weights have been recorded after a growth period of 58 days for begonia and 94 days for pansy. In begonia, fresh weight was significantly greatest in the $200mg{\cdot}L^{-1}$ $K_2SiO_3$ treatment in both 'Super Olympia Red' and 'Super Olympia Rose'. In both pansy cultivars, fresh weight was the greatest in the $200mg{\cdot}L^{-1}$ $K_2SiO_3$ treatment than other treatments. Chlorophyll content was significantly greater in the $100mg{\cdot}L^{-1}$ $K_2SiO_3$ treatment for both the cultivars of begonia. Leaf area significantly increased with the higher concentrations of $K_2SiO_3$ treatment in both cultivars of pansy. Stomatal structures on the leaf epidermis were observed with scanning electron microscopy (SEM). In begonia 'Super Olympia Rose', the structure of stomata were more compact in size in the $300mg{\cdot}L^{-1}$ $K_2SiO_3$ treatment than in the control. Similarly, in pansy 'Matrix White Blotch' the surface of stomata appeared to be smoother in the $300mg{\cdot}L^{-1}$ $K_2SiO_3$ treatment than those wrinkled appearance in the control. The surface of the leaf epidermis appeared to be compact due to Si deposition, and thus results indicated that Si positively affected the growth and biomass production of these species. Our data show that the effect of Si on growth parameters is strongly dependent on cultivar of the plant species tested.

Effect of the Structure of MoO3/bismuth molybdate Binary Phase Catalysts on the Selective Oxidation of Propylene (MoO3/bismuth molybdate 혼합 2상 촉매의 구조에 따른 프로필렌 선택산화반응 특성)

  • Cha, T.B.;Choi, M.J.;Park, D.W.;Chung, J.S.
    • Applied Chemistry for Engineering
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    • v.3 no.1
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    • pp.53-63
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    • 1992
  • M/BM -series catalysts, $MoO_3$ supported on ${\alpha}-Bi_2Mo_3O_{12}$ were also prepared by impregnation method. BM/M-series catalysts, ${\alpha}-Bi_2Mo_3O_{12}$ supported on $MoO_3$ were also prepared by coprecipitation. Structure and catalytic properties of the two phase catalysts were studied by means of using nitrogen adsorption, X-ray diffraction, and scanning electron microscopy. The reaction test for the selective oxidation of propylene to acrolein over Bi-molybdate catalysts was studied using a fixed-bed reactor system. In M/BM-series catalysts, $MoO_3$ was dispersed on ${\alpha}-Bi_2Mo_3O_{12}$, and the crystal structure of ${\alpha}-Bi_2Mo_3O_{12}$ remains unchanged by the presence of excess $MoO_3$. However the surface morphology and bulk structure of BM/M-series catalysts were altered probably because the precipitated $Bi(OH)_3$ reacted with $MoO_3$ during the calcination to form ${\alpha}-Bi_2Mo_3O_{12}$ phase. The results of propylene oxidation on both series catalysts showed that the reaction took place over the surface of ${\alpha}-Bi_2Mo_3O_{12}$ particle and the role of excess $MoO_3$ was to supply oxygen to ${\alpha}-Bi_2Mo_3O_{12}$. These increasing effects on activity were also observed in the mechanical mixtures of ${\alpha}-Bi_2Mo_3O_{12}$ and $MoO_3$.

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Synthesis and Properties of Hyperbranched Liquid Crystalline Polyesters by Direct Polycondensation (직접중축합법에 의한 하이퍼브랜치 액정 폴리에스터의 합성 및 성질)

  • Park, Jong-Ryul;Kim, Hye-Mi;Yoon, Doo-Soo;Sohn, Jeong Sun;Bang, Moon-Soo
    • Applied Chemistry for Engineering
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    • v.28 no.2
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    • pp.237-244
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    • 2017
  • Hyperbranched liquid crystalline polymers with azomesogenic and cholesteryl groups in their terminal positions were designed and synthesized by direct polycondensation reaction. The chemical structures and thermal and mesomorphic properties of the synthesized polymers were investigated by FT-IR, $^1H-NMR$, differential scanning calorimetry (DSC), thermogravimetry analysis (TGA), and polarizing optical microscopy (POM). The inherent viscosities (${\eta}_{inh}$) of the polymers were measured to be between 0.30 and 0.50 dL/g in phenol/p-chlorophenol/1,1,2,2-tetrachloroethane (25/40/35 = w/w/w). The degree of branching (DB) in these polymers ranged from 0.37 to 0.75; they, as amorphous polymer, showed glass transition temperatures ranging from 80 to $120^{\circ}C$; the polymers readily dissolved in most of the organic solvents used in the experiments. Only hyperbranched polymers with a cholesteryl group as their mesogenic group showed liquid crystalline phases.

Comparison of Mechanical properties and Surface Friction of White Metals Produced by Centrifugal and Laser Cladded on SCM440 (원심주조방식과 레이저 클래딩 증착법을 통한 화이트메탈의 기계 및 마찰특성 비교)

  • Jeong, Jae-Il;Kim, Dong-Hyuk;Park, Jin-Young;Oh, Joo-Young;Choi, Si-Geun;Kim, Seock-Sam;Cho, Young Tae;Lee, Ho;Ham, Seung-Sik;Kim, Jong-Hyoung
    • Tribology and Lubricants
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    • v.34 no.3
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    • pp.84-92
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    • 2018
  • Bearings are essential for reducing vibration and wear, in order to achieve high durability and increase longevity. White metal treatment of tilting pads via centrifugal casting method has the possibility of increasing durability. However, this manufacturing method has drawbacks such as long processing time, high defect rate, and harmful health effects. Laser cladding deposition technique is a powerful method that can address these issues by decreasing the processing time and providing good adhesion. In this study, we suggest optimum conditions for laser cladding deposition that can be used in industrial applications. We deposited a soft white metal layer on SCM440 that is primarily used in shafts to minimize wear of bearing pads. During the laser deposition process, we controlled factors such as laser power, powder feed rate, and laser head speed to determine the optimum conditions. In addition, we measured the hardness using micro Vickers, and performed field emission scanning electron microscopy, energy dispersive X-ray spectroscopy, X-ray diffraction, and friction tests to investigate the mechanical properties and surface characteristics for different parameters. Based on the experimental results, we suggest that laser power, powder feed rate, and laser head speed of 1.3 kW, 2.5 rpm, and 10 mm/s, respectively, constitute the optimum conditions for producing white metals using laser cladding.