• Title/Summary/Keyword: scanning microscopy

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Wood Identification of Neolithic Charcoals Excavated at Giheung Nongseori Ruins (기흥 농서리유적에서 발굴된 신석기시대 목탄의 목재 식별)

  • Eom, Young-Geun;Xu, Guang Zhu
    • Journal of the Korean Wood Science and Technology
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    • v.38 no.4
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    • pp.275-281
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    • 2010
  • Wood identification was conducted for the 8 Neolithic charcoals excavated at Giheung Nongseori Ruins through scanning electron microscopy. They were all identified as hardwood: 6 and 1 were found to be Prinus section and Cerris section of subgenus Lepidobalanus under genus Quercus, respectively, and the remaining 1 to be genus Betula. This species composition was thought to indicate the temperate to warm temperate climate region.

Nano-identification for the Cleavage of Disulfide Bond during the Self-Assembly Processes of Unsymmetric Dialkyl Disulfides on Au(111)

  • Noh, Jae-Geun
    • Bulletin of the Korean Chemical Society
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    • v.26 no.4
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    • pp.553-557
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    • 2005
  • The formation of striped phases of unsymmetric hexyl octadecyl disulfide ($CH_3(CH_2)_5SS(CH_2)_{17}CH_3$, HOD) and 1-hydroxyundecyl octadecyl disulfide ($CH_3(CH_2)_{17}SS(CH_2)_{11}$OH, HUOD) on Au(111) and graphite has been investigated by scanning tunneling microscopy (STM) to understand the self-assembly processes of dialkyl disulfides. STM imaging clearly shows the formation of striped phases having corrugation periodicities that are nearly consistent with the molecular length of alkanethiolate moieties formed after the S-S bond cleavage of dialkyl disulfide on a gold surface. On the other hand, self-assembled monolayers (SAMs) of dialkyl disulfides on a graphite surface displayed long-range, well-ordered monolayers with one striped pattern that shows periodicity as a function of molecular length via nondissociative adsorption. From a nonoscopic viewpoint, we have clearly demonstrated that dialkyl disulfide SAMs on gold form via S-S bond cleavage of disulfide.

Synthesis and Characterization of 1-D BiSI and 2-D BiOI Nanostructures

  • Lee, Juheon;Min, Bong-Ki;Cho, Insu;Sohn, Youngku
    • Bulletin of the Korean Chemical Society
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    • v.34 no.3
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    • pp.773-776
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    • 2013
  • We have prepared 1-D BiSI and 2-D BiOI nanostructures, and characterized them by scanning electron microscopy, transmission electron microscopy (TEM), X-ray diffraction crystallography, thermogravimetric analysis/differential scanning calorimetry, and UV-visible absorption. Here, we first report clear HR-TEM image of BiSI. In addition, we first found that the growth direction of BiSI is [12-1] plane, with the neighboring distance of 0.30 nm. The crystal structures of BiSI and BiOI are found to be orthorhombic (Pnam) and tetragonal (P4/nmm), respectively. The absorption band gaps of BiSI and BiOI are measured to be 1.55 and 1.92 eV, respectively. Our study could further highlight the applications of V-VI-VII compounds.

Characteristics of Die Sinking Electical Discharge Machining for Pulse Duration (펄스지속시간에 따른 형상방전가공 특성)

  • 우정윤;왕덕현;윤존도
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 1997.04a
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    • pp.827-831
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    • 1997
  • Conductive veramic matrix composite(CMC) workpiece of TiC 33%/Al /sab 2/O /sab 3/ 66% Y /sab 2/ O /sab 3/ was machined by die sinking electrical discharge machining(EDM) according to different pulse duration and suty factor for reverse polarity of electrode. Material removal rate(MRR) was examined by process under various operating conditions. The surface morphology was evaluated by surface roughness values and scanning electron microscopy(SEM) research. The more MRR was obtained according to increase pulse duration and duty factor. Also the maximum surface roughness(Rmax) of EDMed surface was slightly changed with increased pulse duration and duty factor. The SEM photographs of EDMed surface showed wide recast wide recast distribution region of melting materials in purse duration 0.130(ms) than 0.048(ms).

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Classification of the Length of Ceramic Fibers by Settling Process (중력침강에 의한 세라믹 섬유의 길이분류)

  • 김제균;최광훈;오승진;정윤중;강대갑;이재춘
    • Journal of the Korean Ceramic Society
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    • v.31 no.2
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    • pp.161-170
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    • 1994
  • For the preparation of short ceramic fibers of which average length might be in accordance with the opening size of sieve, e.g., 150${\mu}{\textrm}{m}$ or 300${\mu}{\textrm}{m}$, bulk fibers were grounded on sieve screen by applying both compressing and shearing force, and passed through the sieve screen. The grounded fibers were subjected to gravitational settling processes. The classified fibers were observed by scanning electron microscopy and the length of each fiber was measured to correlate the average length with the opening size of the sieve used for grinding bulk fibers. Theoretical analysis show that a free settling technique is ineffective for the classification of fibers by length compared with that of particles. The average lengths of classified fibers estimated by scanning electron microscopy were in good agreement with those obtained by relative packing volume of the fibers. Accordingly, it is confirmed that average fiber lengths can be determined from bulk volume data without photographing, counting and averaging results for hundreds of fibers.

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Real time observation of reconstruction transition on GaAs (111)B vicinal surface by scanning electron microscopy

  • Ren, Hong-Wen;Tatau Nishinaga
    • Proceedings of the Korea Association of Crystal Growth Conference
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    • 1996.06a
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    • pp.19-37
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    • 1996
  • Scanning electron microscopy (SEM) has been applied to observe directly the {{{{ SQRT { 19} }}}}${\times}${{{{ SQRT { 19} }}}} and (1${\times}$1)HT reconstructions and the transition associated step bunching on the GaAs (111)B surfaces under As pressure. Close to the transition point, {{{{ SQRT { 19} }}}}${\times}${{{{ SQRT { 19} }}}}an d (1${\times}$1)HT reconstructions are observed in dark and bright domains by SEM and determined by micro-probe reflection high-energy electron diffraction (${\mu}$-RHEED). The reconstruction diagram shows hyster-esis. The stepped surface morphology during the reconstruction transition was unstable. Heavy step bunching with rough macrostep edges was observed.

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Improvement of field emission character by surface treatment of carbon thin film (탄소계 박막의 표면 처리에 의한 전계전자방출 특성의 개선)

  • ;K.-Y. Lee;S.-I. Honda;M. Katayama;;K. Oura
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2002.07a
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    • pp.147-150
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    • 2002
  • The electron field emission properties of amorphous carbon (a-C) films deposited using a RF magnetron sputtering system have been improved by introducing a simple method of argon plasma treatment at room temperature. Surface morphologies and structural properties of the a-C films were investigated by scanning electron microscopy and Raman spectroscope, respectively. Structural properties and surface morphologies of the a-C films were changed by argon plasma treatment. The emission properties improved with the plasma treatment.

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Deposition of Carbon Thin Film using Laser Ablation and Its Field Emission Properties (레이저 증착법에 의한 탄소계 박막의 구조 및 전계방출특성)

  • ;Kenjiro Oura
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.15 no.7
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    • pp.634-639
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    • 2002
  • Using laser ablation technique carbon thin films were deposited on Si(100) substrate as a function of substrate temperature. In this study, the surface morphologic, structural and field emission properties of these carbon thin films were investigated using Raman spectroscopy, scanning electron microscopy, and a diode technique, respectively. With increasing of the substrate temperature, the surface morphologies were changed significantly. Moreover, the intensity of D-band and the full width at half maximum of these bands were dependent on substrate temperatures. As the substrate temperature was increased, the field emission properties were improved. As the result, we find that the field emission properties of the films were changed significantly with the substrate temperature and structural features of carbon than films.

Mechanical Properties of Carbon/Carbon Composites Densified by HIP Technique

  • Manocha, L.M.;Warrier, Ashish;Manocha, S.;Banerji, S.;Sathiyamoorthy, D.
    • Carbon letters
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    • v.6 no.1
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    • pp.6-14
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    • 2005
  • The study of mechanical properties and fracture behaviour of carbon/carbon composites is significant to its application and development. These are dependent on microstructure and properties of reinforcing fibers and matrix, fiber/matrix interface and porosity/cracks present in the composites. In the present studies high-density carbon/carbon composites have been prepared using PAN and various pitch based carbon fibers as reinforcements and pitch as matrix with repeated densification cycles using high-pressure impregnation and carbonization technique. Scanning electron microscopy has been used to study the fracture behaviour of the highly dense composites and correlated with structure of the composites. The geometry of reinforcement and presence of unfilled voids/cracks was found to influence the path of crack propagation and thereby the strength of composites. The type of stresses (tensile or compressive) accumulated also plays an important role in fracture of composites.

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Structural change of charcoal during carbonization Process (탄화과정 중 목탄의 구조적 변화)

  • Kwon, Sung-Min;Kim, Nam-Hun
    • Journal of Forest and Environmental Science
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    • v.22 no.1
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    • pp.32-40
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    • 2006
  • Structure change of Quercus variabilis charcoal during the carbonization temperature was investigated by scanning electron microscopy. Volume of wood sample decreased with increasing the carbonization temperature, and checks were occurred along with radial direction. SEM observation indicated that the all wood cells presented the layering structure at $250^{\circ}C$ and $300^{\circ}C$. However, the cross section of cell walls at $340^{\circ}C$ and over showed an amorphous-like structure without cell wall layering.

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