• Title/Summary/Keyword: rock sample

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Engineering characterization of intermediate geomaterials - A review

  • T. Ashok Kumar;Ramanandan Saseendran;V. Sundaravel
    • Geomechanics and Engineering
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    • v.33 no.5
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    • pp.453-462
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    • 2023
  • Intermediate Geomaterials (IGMs) are natural formation materials that exhibit the engineering behavior (strength and compressibility) between soils and rocks. The engineering behavior of such material is highly unpredictable as the IGMs are stiffer than soils and weaker/softer than rocks. Further, the characterization of such material needs exposure to both soil and rock mechanics. In most conventional designs of geotechnical structures, the engineering properties of the IGMs are either aligned with soils or rocks, and this assumption may end up either in an over-conservative design or under-conservative design. Hence, many researchers have attempted to evaluate its actual engineering properties through laboratory tests. However, the test results are partially reliable due to the poor core recovery of IGMs and the possible sample disturbance. Subsequently, in-situ tests have been used in recent years to evaluate the engineering properties of IGMs. However, the respective in-situ test finds its limitations while exploring IGMs with different geological formations at deeper depths with the constraints of sampling. Standard Penetration Test (SPT) is the strength-based index test that is often used to explore IGMs. Moreover, it was also observed that the coefficient of variation of the design parameters (which represents the uncertainties in the design parameters) of IGMs is relatively high, and also the studies on the probabilistic characterization of IGMs are limited compared with soils and rocks. With this perspective, the present article reviews the laboratory and in-situ tests used to characterize the IGMs and explores the shear strength variation based on their geological origin.

Variation of Geomechanical Characteristics of Granite and Orthogneiss in Wonju Area due to Accelerated Artificial Chemical Weathering Tests (강원도 원주일대에 분포하는 화강암 및 화강편마암의 화학풍화실험에 의한 물성 변화 연구)

  • Woo, Ik;Um, Jeong-Gi;Park, Hyuck-Jin
    • Tunnel and Underground Space
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    • v.19 no.3
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    • pp.213-225
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    • 2009
  • The purpose of the study is to evaluate the effects of chemical weathering on the granite and orthogneiss in Wonju area based on accelerated artificial chemical weathering. The rock samples were scrutinized the variation of index properties and ion exchanges caused by artificial chemical weathering which was implemented with leaching test for 170 days using double soxhlet extractor. The differential weathering and decrease of p wave velocity were obtained by weathering process without significant changes of porosity. In case of granite samples, the uniaxial compression strength was reduced by 20% and 16% for the F-grade and SW-grade, respectively. For MW-grade granite, however, was not able to examine the effect of strength reduction due to lack of sample number. Also, for orthogneiss, it is difficult to compare the values of uniaxial compressive strength between before and after the test because of its strong anisotropy.

Determination of Damage Thresholds and Acoustic Emission Characteristics of Pocheon Granite under Uniaxial Compression

  • Jang, Hyun-Sic;Jang, Bo-An
    • The Journal of Engineering Geology
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    • v.28 no.3
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    • pp.349-365
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    • 2018
  • The strain and acoustic emission (AE) signals of Pocheon granite were measured during uniaxial compression tests to investigate microcrack formation and damage. Crack closure, initiation, and damage stresses of each sample were determined through an analysis of the crack volumetric strain and stiffness. The samples experienced four damage stages according to stress levels: stage 1 = crack closure stage; stage 2 = elastic stage; stage 3 = crack initiation stage; stage 4 = crack damage stage. At least 75% of all AE signals occurred in stages 3 and 4, and different AE parameters were detected in the four stress stages. Rise time, count, energy, and duration clearly showed a tendency to gradually increase with the damage stress stage. In particular, the rise time, energy, and duration increased by at least 95% in stage 4 as compared with stage 1. However, the maximum amplitude showed a smaller increase, and the average frequency decreased slightly at higher stages. These results indicate that as the degree of rock damage increases, the crack size grows larger. The crack types corresponding to the AE signals were determined using the relationship between RA (Rise time / Amplitude) values and average frequencies. Tension cracking was dominant in all stress stages. Shear cracking was rare in stages 1 and 2, but increased in stages 3 and 4. These results are consistent with previous studies that reported cracking begins after samples have already been damaged. Our study shows that the state of rock damage can be investigated solely through an analysis of AE parameters when rocks are under compressive stress. As such, this methodology is suitable for understanding and monitoring the stress state of bedrock.

The Effects of Storytelling Technique on pre-service teachers' Acquisition of Science Concept and Science Teaching Efficacy (초등예비 교사의 스토리텔링 기법 적용이 과학개념 습득 및 과학교수효능감에 미치는 효과)

  • Lee, Yong-seob
    • Journal of the Korean Society of Earth Science Education
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    • v.10 no.2
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    • pp.226-234
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    • 2017
  • The purpose of this study is to investigate the effect of the application of storytelling on pre-service teachers of elementary school who take courses in 'earth's strata and rock' on science teaching concept and science teaching efficacy. The experiment was aimed at one class (32 students) enrolled in the 'earth's strata and rock' course at intensive course through 15 weeks from March to June. The experiment was taking lectures of "earth's strata and rock" for one semester, and the pre-service teachers of elementary school finished class demonstration with storytelling technique by group. The results and analysis of the study were analyzed by the corresponding sample test in before and after the group test. The conclusion of the study is as follows. First, the application of storytelling method on pre-service teachers of elementary school was effective in science concept. teaching efficacy. Second, the application of storytelling method on pre-service teachers of elementary school was effective in science teaching efficacy. Third, the application of storytelling method on pre-service teachers of elementary school responded positively.

Analysis of Spiramycin in Fish Using High Performance Liquid Chromatography (HPLC를 이용한 어류 중의 Spiramycin 분석)

  • Lee Tae-Seek;Lee Hee-Jung;Jo Mi-Ra;Byun Han-Seok;Son Kwang-Tae;Park Mi-Jung;Yi Young-Ho
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.39 no.2
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    • pp.78-84
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    • 2006
  • A high performance liquid chromatography assay method for spiramycin in fish muscle was developed. The developed method was evaluated and validated by monitoring spiramycin in olive flounder (Paralichthys olivaceus), black rock fish (Sebastes schlegeli) and in live conger eel (Anguilla japonica) in fish farms and distribution centers. Using the developed method, the recovery rate was up to 82.4-88.8%, which was higher than that of conventional methods (77.6-87.1%). In particular, the proposed sample treatment protocol was suitable for use with fish samples to remove low molecular weight materials and pigments that could interfere an accurate analysis. The prepared stock solution was very stable, and it remained chemically stable for 5 weeks at $4^{\circ}C$. The performance limit of the developed method for spiramycin acid in fish muscle was 0.05 ppm. One hundred thirty-four fish samples including olive flounder, black rock fish and live conger eel were analyzed to evaluate the overall efficiency of the modified method and to monitor the actual condition of spiramycin usage in fish farms. Olive flounder and black rock fish were collected from fish farms in coastal areas of Korea, and live conger eels were purchased from a fish market in the Busan area from September 2001 to March 2002. According to the overall performance of the developed method, it was considered suitable for the monitoring of spiramycin in fish muscle. The suggested method of analysis for spiramycin in fish muscle is registered in the Korean Official Methods of Food Analysis and is currently tieing utilized for fishery products inspection by the Korea Food and Drug Administration and the National Fisheries Products Quality Inspection Service.

Analysis for Bearing Capacity of Basalt by Vesicle Area Ratio (현무암 기공면적에 따른 지지력분석)

  • Nam, Kwan-Woo;Kim, Sang-Ho;Kim, Ju-Tae;Park, Gun-Soo;Seo, Seok-Hyun
    • Proceedings of the Korean Geotechical Society Conference
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    • 2009.09a
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    • pp.1001-1010
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    • 2009
  • The study that unconfined compression strength of intact rock which is the most important factor to determine the bearing capacity effects discontinuities in rock mass has been carried out actively so far. However, the study which is related to lithological characters such as vesicle which is one of the primary characteristics of Basalt has barely been conducted. On this study, We have analyzed the correlation-ship between vesicle and unconfined compression strength and the effect on the bearing capacity, based on the reviewing on the changes of unconfined compression strength as the amount of vesicle of Basalt. It is impossible to analyze the amount of vesicle of Basalt as measuring unit. So it was analyzed by the ratio of the core sample's surface area and another area that vesicle takes up. Also, unconfined compression strength was calculated by point load test and unconfined compression strength test. The analysis shows that vesicle area ratio and unconfined compression strength have the exponential relationship and vesicle area ration is the factor to determine the bearing capacity of Basalt. It is considered that the reliability of calculating of the bearing capacity of Basalt will be improved as we study the correlation-ship between the vesicle area ratio and rock mass grade hereafter.

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A Study on the P Wave Arrival Time Determination Algorithm of Acoustic Emission (AE) Suitable for P Waves with Low Signal-to-Noise Ratios (낮은 신호 대 잡음비 특성을 지닌 탄성파 신호에 적합한 P파 도달시간 결정 알고리즘 연구)

  • Lee, K.S.;Kim, J.S.;Lee, C.S.;Yoon, C.H.;Choi, J.W.
    • Tunnel and Underground Space
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    • v.21 no.5
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    • pp.349-358
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    • 2011
  • This paper introduces a new P wave arrival time determination algorithm of acoustic emission (AE) suitable to identify P waves with low signal-to-noise ratio generated in rock masses around the high-level radioactive waste disposal repositories. The algorithms adopted for this paper were amplitude threshold picker, Akaike Information Criterion (AIC), two step AIC, and Hinkley criterion. The elastic waves were generated by Pencil Lead Break test on a granite sample, then mixed with white noise to make it difficult to distinguish P wave artificially. The results obtained from amplitude threshold picker, AIC, and Hinkley criterion produced relatively large error due to the low signal-to-noise ratio. On the other hand, two step AIC algorithm provided the correct results regardless of white noise so that the accuracy of source localization was more improved and could be satisfied with the error range.

Experimental Study for Optimal Method in Measuring the Basic Friction Angle of Rock (최적의 기본마찰각 측정법에 관한 실험적 연구)

  • Lee, Kook-Hyun;Jang, Hyun-Sic;Jang, Bo-An
    • The Journal of Engineering Geology
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    • v.29 no.4
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    • pp.565-578
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    • 2019
  • Basic friction angles of Hwangdeung granite, Berea sandstone, Jeongsun marble, Hongcheon gneiss, Pungam shale and Eumseong sandy shale were measured by direct shear test, tilt test and pull test. Characteristics of basic friction angle and the accuracy of test methods were compared and the optimal method in measuring basic friction angle was suggested. Although basic friction angles might be measured accurately by direct shear test, the test apparatus is expensive and procedures are complicated. Tilt tests which is the suggested method for measuring basic friction angle by International Association for Rock Mechanics also provided similar basic friction angles measured by direct shear test. However, the error measured for the same rock type is higher than 7° and values by repeated measurements in one sample show different trends, such as increasing or decreasing or almost constant as measurements continued. The difference measured in one gneiss sample is higher 12°, indicating that tilt test may be not a reliable method for measuring basic friction angle. Not only pull test provided accurate and consistent results under low normal stresses, but also test apparatus is simple and inexpensive and procedure is not complicated, indicating that pull test may be the optimal method for measuring basic friction angle.

Variations of Physico-Mechanical Properties of the Cretaceous Mudstone in Haman, Gyeongnam due to Freeze-Thaw Weathering (경남 함안군 백악기 이암의 동결-융해에 따른 물성변화 및 미세균열 발현특성)

  • Um, Jeong-Gi;Shin, Mi-Kyoung
    • Tunnel and Underground Space
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    • v.19 no.2
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    • pp.146-157
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    • 2009
  • An experimental study of accelerated weathering on mudstone sample specimens from Haman, Gyeongnam was performed to investigate the variations of physico-mechanical properties of deteriorated rocks due to freeze-thaw weathering. Each complete cycle of freeze and thaw lasted 24 hours, comprising 2 hours of saturating in vacuum chamber, 8 hours of freezing at $-16{\pm}1^{\circ}C$ and 14 hours of thawing at room temperature. Total of 55 cycles of freeze-thaw were completed with measuring the index properties as well as geometries of microfractures. The measured specific gravity and P-wave velocity found to decrease with increasing freeze-thaw cycles. On the other hand, absorption ratio and effective porosity were continuously increased with increasing freeze-thaw cycles. It was found that the index properties of deteriorated sample specimen depend on its initial properties and flaws in rock. The size and density of the traces of the microfracture on slab specimen exhibited abrupt changes after 30 cycles of freeze-thaw weathering. The results obtained in this study show that the box fractal dimension($D_B$) given in this paper has the strong capability of quantifying the size and density of the microfracture.

Optimal Conditions for Pretreated Sample for Sr Isotope Analysis by MC-ICP-MS: A Comparison Between Eichrom (SR-R50-S)'s and Bio-Rad(AG®50W-X8)'s Resins (다검출기 유도결합 플라즈마 질량분석기에 의한 Sr 동위원소 분석을 위해 전처리된 시료의 최적 조건: Eichrom사 Sr 수지(SR-R50-S)와 Bio-Rad사 수지(AG®50W-X8) 비교)

  • Myoung Jung, Kim;Seung-Gu, Lee
    • Korean Journal of Mineralogy and Petrology
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    • v.35 no.4
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    • pp.507-520
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    • 2022
  • The Sr isotope ratio, which is used as basic data for rock formation time, crustal and mantle evolution studies, is determined by mass spectrometer such as thermal ionization mass spectrometry (TIMS) or multi-detector inductively coupled plasma mass spectrometry (MC-ICP-MS). In this technical report, we compared how incomplete chemical separation of elements affects the determination of Sr isotope ratios. For the experiment, commercial resin, NBS987(NIST SRM987) Sr isotope standard, and rock standard samples from the Geological Survey of Japan (GSJ) such as JG1a, JB3 and JA1 were used. As a result of the comparative experiment, it was clearly observed that the measured values of 87Sr/86Sr change when Rb remains due to incomplete separation of the NBS987 Sr isotope standard sample as well as the rock standard samples of GSJ. This indicates that complete separation is an important factor since the calculated value deviates from the true value even though correction for isotope interference by isobar is performed when measuring the isotope ratio with MC-ICP-MS. This also suggests that, when reporting the measurement result of Sr isotope ratio using MC-ICP-MS, the measurement strength of 85Rb should be reported together with the measurement strength of all isotopes of Sr so that isotope interference by isobar can be judged.