• Title/Summary/Keyword: residual structure

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Characterization of $RuO_2$ Thin Films by Hot-wall Metal Organic Chemical Vapor Deposition (Hot-wall MOCVD에 의한 $RuO_2$ 박막의 특성)

  • 신웅철;윤순길
    • Journal of the Korean Ceramic Society
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    • v.33 no.9
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    • pp.969-976
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    • 1996
  • RuO2 thin films were deposited on SiO2(1000 $\AA$)/Si by hot-wall Metal Organic Chemical Vapor Depositon. The crystallinity of RuO2 thin films increased with increasing deposition temperature and the preferred orienta-tion of RuO2 films converted (200) plane to (101) plane with increasing film thicknesses. Such a change in preferred orientation was influenced on the crystallographic structure and the residual stress of RuO2 thin films. The resistivity of the 2700$\AA$-thick RuO2 thin films deposted at 30$0^{\circ}C$ was 52.7$\mu$$\Omega$-cm and they could be applicable to bottom electrodes of high dielectric materials. However the resistivity of RuO2 thin films increased with decreasing film thicknesses. The grain size and the resistivity of RuO2 thin films were densified with increasing the annealing temperature and showed the decrease of resistivity.

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The PTCR Effect of Semiconducting Zn-Ti-Ni-O Ceramics (Zn-Ti-Ni-O 반도성 세라믹스의 PTCR 현상)

  • Ko, Il-Young;Choi, Seung-Chul;Kim, Hwan
    • Journal of the Korean Ceramic Society
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    • v.30 no.8
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    • pp.609-614
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    • 1993
  • Semiconducting Zn-Ti-Ni-O and Zn-Ti-O system were investigated. The specimens sintered at the temperature between 125$0^{\circ}C$ and 145$0^{\circ}C$ exhibited PTCR effect between -5$0^{\circ}C$ and 35$0^{\circ}C$ with resistivity ration exceeding three decades. Semiconducting Zn-Ti-Ni-O is consisted of two phases, one is n-type ZnO and the other is p-type spinel structure. The mechanism of PTCR effect was explained in relation to the piezoelectric property of ZnO and the residual stress caused by thermal expansion difference between two phases during cooling process.

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Structural Control Aiming for High-performance SiC Polycrystalline Fiber

  • Ishikawa, Toshihiro;Oda, Hiroshi
    • Journal of the Korean Ceramic Society
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    • v.53 no.6
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    • pp.615-621
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    • 2016
  • SiC-polycrystalline fiber (Tyranno SA, Ube Industries, Ltd.) shows very high heat-resistance and excellent mechanical properties up to very high temperatures. However, further increase in the strength is required. Up to now, we have already clarified the relationship between the strength and the defect-size of the SiC-polycrystalline fiber. The defects are formed during the conversion process from the raw material (amorphous Si-Al-C-O fiber) into SiC-polycrystalline fiber. In this conversion process, a degradation of the Si-Al-C-O fiber and a subsequent sintering of the degraded fiber proceed as well, accompanied by a release of CO gas and compositional changes, to obtain the dense SiC-polycrystalline fiber. Since these changes proceed in each filament, the strict control should be needed to minimize residual defects on the surface and in the inside of each filament for achieving the higher strength. In this paper, the controlling factors of the fiber strength and the fine structure will appear.

Change of the Microstructure of ZnO Arrester block by Lightning Surge Current and Ageing test (뇌서지전류와 Ageing에 의한 산화아연형 피뢰기 소자의 미세구조변화)

  • Lee, Bok-Hee;Kang, Sung-Man
    • Proceedings of the KIEE Conference
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    • 2000.07c
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    • pp.1877-1879
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    • 2000
  • This paper deals with the change of the micro-structure of ZnO associated with lightning surge current and ageing test. In this work, a surge current generator which can produce 8/20 [${\mu}s$], 6 [kA] impulse current is designed and fabricated to simulate the lightning impulse current. The residual voltage and leakage current flowing to ZnO blocks are observed. Also a compensation circuit was used in resistive current measurement. The micro-structures of ZnO arrester block were significantly changed by lightning surge current and accelerated temperature ageing test.

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Permeabilization of Ochrobactrum anthropi SY509 Cells with Organic Solvents for Whole Cell Biocatalyst

  • Park, Kyung-Oh;Song, Seung-Hoon;Yoo, Young-Je
    • Biotechnology and Bioprocess Engineering:BBE
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    • v.9 no.3
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    • pp.147-150
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    • 2004
  • Permeabilization is known to overcome cell membrane barriers of whole cell biocatalysts. The use of organic solvents is advantageous in terms of cost, simplicity, and efficiency. In this study, Ochrobactrum anthropi SY509 was permeabilized with various organic solvents. Treatment with organic solvents resulted in lower permeability barriers due to falling out lipids of the cell membrane. Therefore, permeabilized cells showed higher enzyme activity with no cell viability. Among various organic solvents, 0.5% (v/v) chloroform was selected as the most efficient permeabilizing reagent. Changes in the cell membrane structure were observe d and the residual amounts of phospholipids of the cell membrane were measured to investigate the mechanism of the improved permeability.

A study on the mechanical properties of the polymer cement mortar in a high temperature region (고온영역에서의 폴리머시멘트모르타르의 역학적 특성연구)

  • Yoon, Ung-Gi;Seo, Dong-Goo;Kwon, Young-Jin;Kim, Hyung-Jun
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2014.11a
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    • pp.113-114
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    • 2014
  • Though polymer cement mortar is widely used to repair or reinforce concrete as it has superior adhesion, dense internal structure, chemical resistance, and workability in comparison to those of general cement mortar, studies on its behaviors in high temperature environment such as fire is urgently required. Accordingly, in this experiment, the degrees of reduction in the compressive strength at different temperatures was grasped applying ISO834 Heating Curve, and the effect of polymer content and type on compressive strength could be determined. As a result of this experiment, it is found that polymer type and content have a big effect on reduction of compressive strength in high temperature range, and not only the dynamic characteristics but also the combustion characteristics in high temperature range are required to be studied considering occurrence of a fire in the future.

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A Study on Smart Cure of Filament Wound Composite Flywheel (필라멘트 와인딩 플라이휠의 스마트 경화에 관한 연구)

  • 이도훈;김선경;김동진;이우일;하성규
    • Composites Research
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    • v.16 no.1
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    • pp.34-41
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    • 2003
  • A cure process control model was proposed to optimize the curing process of thick filament wound structure. There are two types of smart cure, one is that the boundary conditions of the hollow cylinder are same between inner surface and outer surface, and the other is that inner surface temperature is slightly higher than outer surface to initiate cure reaction from the inner side to the outer side to reduce residual stress.

A new mindlin FG plate model incorporating microstructure and surface energy effects

  • Mahmoud, F.F.;Shaat, M.
    • Structural Engineering and Mechanics
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    • v.53 no.1
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    • pp.105-130
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    • 2015
  • In this paper, the classical continuum mechanics is adopted and modified to be consistent with the unique behavior of micro/nano solids. At first, some kinematical principles are discussed to illustrate the effect of the discrete nature of the microstructure of micro/nano solids. The fundamental equations and relations of the modified couple stress theory are derived to illustrate the microstructural effects on nanostructures. Moreover, the effect of the material surface energy is incorporated into the modified continuum theory. Due to the reduced coordination of the surface atoms a residual stress field, namely surface pretension, is generated in the bulk structure of the continuum. The essential kinematical and kinetically relations of nano-continuums are derived and discussed. These essential relations are used to derive a size-dependent model for Mindlin functionally graded (FG) nano-plates. An analytical solution is derived to show the feasibility of the proposed size-dependent model. A parametric study is provided to express the effect of surface parameters and the effect of the microstructure couple stress on the bending behavior of a simply supported FG nano plate.

Detection and quantification of structural damage under ambient vibration environment

  • Yun, Gun Jin
    • Structural Engineering and Mechanics
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    • v.42 no.3
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    • pp.425-448
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    • 2012
  • In this paper, a new damage detection and quantification method has been presented to perform detection and quantification of structural damage under ambient vibration loadings. To extract modal properties of the structural system under ambient excitation, natural excitation technique (NExT) and eigensystem realization algorithm (ERA) are employed. Sensitivity matrices of the dynamic residual force vector have been derived and used in the parameter subset selection method to identify multiple damaged locations. In the sequel, the steady state genetic algorithm (SSGA) is used to determine quantified levels of the identified damage by minimizing errors in the modal flexibility matrix. In this study, performance of the proposed damage detection and quantification methodology is evaluated using a finite element model of a truss structure with considerations of possible experimental errors and noises. A series of numerical examples with five different damage scenarios including a challengingly small damage level demonstrates that the proposed methodology can efficaciously detect and quantify damage under noisy ambient vibrations.

Physical modelling of a downdraft outflow with a slot jet

  • Lin, W.E.;Savory, E.
    • Wind and Structures
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    • v.13 no.5
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    • pp.385-412
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    • 2010
  • This article provides a time-resolved characterisation of the wind field in a recently-commissioned, downdraft outflow simulator at The University of Western Ontario. A large slot jet approach to physical simulation was used. The simulator performance was assessed against field observations from a 2002 downdraft outflow near Lubbock, Texas. Outflow wind speed records were decomposed according to classical time series analysis. Length scales, characterising the coarse and fine flow structure, were determined from the time-varying mean and residual components, respectively. The simulated downdraft outflow was approximately 1200 times smaller in spatial extent than the 2002 Lubbock event.