• Title/Summary/Keyword: pre-bonding

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Analysis of Characteristics and Dyeing Properties of Gromwell Colorants(Part III) - Dyeing Properties of Cotton with Gromwell Colorants- (자초색소의 특성분석 및 염색성(제3보) -면섬유에 대한 자초색소의 염색성-)

  • Shin, Youn-sook;Choi, Hee
    • Journal of the Korean Society of Clothing and Textiles
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    • v.26 no.3_4
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    • pp.422-430
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    • 2002
  • Dyeing properties of the colorants from gromwell on cotton fabric were investigated. The effects of dyeing conditions on dye uptake and the effects of mordants and mordanting methods on K/S value, color change and colorfastness were explored. Gromwell colorants showed low affinity to cotton fabric, and its adsorption isotherm was Freundlich type close to Langmuir type. Therefore, it was considered that hydrogen bonding and Vander Waals force were involved in the adsorption of gromwell colorants to cotton fabric. Pre-mordanting method except Sn mordant gave higher K/S value but it was not significant. Gromwell colorants produced mainly R and RP color on cotton fabric depending on mordants and mordanting method. Dyed cotton fabric showed generally high colorfastness irrespective of mordanting treatment. Light colorfastness was increased by repeat dyeing and Fe and Sn mordanting.

Butt-fusing Procedures and Qualifications of High Density Polyethylene Pipe for Nuclear Power Plant Application (원자력발전소 적용 고밀도 폴리에틸렌 배관의 맞대기 융착절차 및 검증절차 분석)

  • Oh, Young-Jin;Park, Heung-Bae;Shin, Ho-Sang
    • Journal of Welding and Joining
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    • v.31 no.6
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    • pp.1-7
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    • 2013
  • In nuclear power plants, lined carbon steel pipes or PCCPs (pre-stressed concrete cylinder pipes) have been widely used for sea water transport systems. However, de-bonding of linings and oxidation of PCCP could make problems in aged NPPs (nuclear power plants). Recently at several NPPs in the United States, the PCCPs or lined carbon steel pipes of the sea water or raw water system have been replaced with HDPE (high density polyethylene) pipes, which have outstanding resistance to oxidation and seismic loading. ASME B&PV Code committee developed Code Case N-755, which describes rules for the construction of buried Safety Class 3 polyethylene pressure piping systems. Although US NRC permitted HDPE materials for Class 3 buried piping, their permission was limited to only 10-year operation because of several concerns including the quality of fusion zone of HDPE. In this study, various requirements for fusion qualification test of HDPE and some regulatory issues raised during HDPE application review in foreign NPPs are introduced.

Aural-visual two-stream based infant cry recognition (Aural-visual two-stream 기반의 아기 울음소리 식별)

  • Bo, Zhao;Lee, Jonguk;Atif, Othmane;Park, Daihee;Chung, Yongwha
    • Proceedings of the Korea Information Processing Society Conference
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    • 2021.05a
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    • pp.354-357
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    • 2021
  • Infants communicate their feelings and needs to the outside world through non-verbal methods such as crying and displaying diverse facial expressions. However, inexperienced parents tend to decode these non-verbal messages incorrectly and take inappropriate actions, which might affect the bonding they build with their babies and the cognitive development of the newborns. In this paper, we propose an aural-visual two-stream based infant cry recognition system to help parents comprehend the feelings and needs of crying babies. The proposed system first extracts the features from the pre-processed audio and video data by using the VGGish model and 3D-CNN model respectively, fuses the extracted features using a fully connected layer, and finally applies a SoftMax function to classify the fused features and recognize the corresponding type of cry. The experimental results show that the proposed system classification exceeds 0.92 in F1-score, which is 0.08 and 0.10 higher than the single-stream aural model and single-stream visual model.

Direct Bonding of Si(100)/NiSi/Si(100) Wafer Pairs Using Nickel Silicides with Silicidation Temperature (열처리 온도에 따른 니켈실리사이드 실리콘 기판쌍의 직접접합)

  • Song, O-Seong;An, Yeong-Suk;Lee, Yeong-Min;Yang, Cheol-Ung
    • Korean Journal of Materials Research
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    • v.11 no.7
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    • pp.556-561
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    • 2001
  • We prepared a new a SOS(silicon-on-silicide) wafer pair which is consisted of Si(100)/1000$\AA$-NiSi Si (100) layers. SOS can be employed in MEMS(micro- electronic-mechanical system) application due to low resistance of the NiSi layer. A thermally evaporated $1000\AA$-thick Ni/Si wafer and a clean Si wafer were pre-mated in the class 100 clean room, then annealed at $300~900^{\circ}C$ for 15hrs to induce silicidation reaction. SOS wafer pairs were investigated by a IR camera to measure bonded area and probed by a SEM(scanning electron microscope) and TEM(transmission electron microscope) to observe cross-sectional view of Si/NiSi. IR camera observation showed that the annealed SOS wafer pairs have over 52% bonded area in all temperature region except silicidation phase transition temperature. By probing cross-sectional view with SEM of magnification of 30,000, we found that $1000\AA$-thick uniform NiSi layer was formed at the center area of bonded wafers without void defects. However we observed debonded area at the edge area of wafers. Through TEM observation, we found that $10-20\AA$ thick amourphous layer formed between Si surface and NiSix near the counter part of SOS. This layer may be an oxide layer and lead to degradation of bonding. At the edge area of wafers, that amorphous layer was formed even to thickness of $1500\AA$ during annealing. Therefore, to increase bonding area of Si NiSi ∥ Si wafer pairs, we may lessen the amorphous layers.

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Wafer Level Hermetic Sealing Characteristics of RF-MEMS Devices using Non-Conductive Epoxy (비전도성 에폭시를 사용한 RF-MEMS 소자의 웨이퍼 레벨 밀봉 실장 특성)

  • 박윤권;이덕중;박흥우;송인상;김정우;송기무;이윤희;김철주;주병권
    • Journal of the Microelectronics and Packaging Society
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    • v.8 no.4
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    • pp.11-15
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    • 2001
  • In this paper, hermetic sealing technology was studied for wafer level packaging of the RF-MEMS devices. With the flip-chip bonding method. this non-conductive B-stage epoxy sealing will be profit to the MEMS device sealing. It will be particularly profit to the RF-MEMS device sealing. B-stage epoxy can be cured by 2-step and hermetic sealing can be obtained. After defining 500 $\mu\textrm{m}$-width seal-lines on the glass cap substrate by screen printing, it was pre-baked at $90^{\circ}C$ for about 30 minutes. It was, then, aligned and bonded with device substrate followed by post-baked at $175^{\circ}C$ for about 30 minutes. By using this 2-step baking characteristic, the width and the height of the seal-line could be maintained during the sealing process. The height of the seal-line was controlled within $\pm$0.6 $\mu\textrm{m}$ in the 4 inches wafer and the bonding strength was measured to about 20MPa by pull test. The leak rate, that is sealing characteristic of the B-stage epoxy, was about $10^{-7}$ cc/sec from the leak test.

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Effect of surface treatment of FRC-Post on bonding strength to resin cements (FRC-포스트의 표면처리가 레진시멘트와의 접착력에 미치는 영향)

  • Park, Chan-Hyun;Park, Se-Hee;Kim, Jin-Woo;Cho, Kyung-Mo
    • Restorative Dentistry and Endodontics
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    • v.36 no.2
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    • pp.125-131
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    • 2011
  • Objectives: The purpose of this study was to evaluate the effect of surface treatment of FRC-Post on bonding strength to resin cements. Materials and Methods: Pre-surface treated LuxaPost (DMG), Rely-X Fiber Post (3M ESPE) and self adhesive resin cement Rely-X Unicem (3M ESPE), conventional resin cement Rely-X ARC (3M ESPE), and Rely-X Ceramic Primer (3M ESPE) were used. After completing the surface treatments of the posts, posts and resin cement were placed in clear molds and photo-activation was performed. The specimens were sectioned perpendicular to the FRC-Post into 2 mm-thick segments, and push-out strength were measured. The results of bond strength value were statistically analyzed using independent samples t-test and oneway ANOVA with multiple comparisons using Scheffe's test. Results: Silanization of posts affect to the bond strength in LuxaPost, and did not affect in Rely-X Fiber Post. Rely-X ARC showed higher value than Rely-X Unicem. Conclusions: Silanization is needed to enhance the bond strength between LuxaPost and resin cements.

Hardening mechanism associated with post-firing heat treatment of softening heat treated and then firing simulated Pd-Ag-Au alloy for bonding porcelain (연화 열처리 후 모의소성된 금속-세라믹용 Pd-Ag-Au계 합금의 후열처리에 의한 경화기전)

  • Kim, Sung-Min;Yu, Young-Jun;Cho, Mi-Hyang;Kwon, Yong-Hoon;Kim, Hyung-Il;Seol, Hyo-Joung
    • Korean Journal of Dental Materials
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    • v.42 no.2
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    • pp.95-106
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    • 2015
  • Hardening mechanism associated with post-firing heat treatment of softening heat treated and then firing simulated Pd-Ag-Au alloy for bonding porcelain was examined by observing the change in hardness, crystal structure and microstructure. By post-firing heat treatment of as-cast, solution treated and pre-firing heat treated specimens at $650^{\circ}C$ after casting, the hardness value increased within 10 minutes. Then, hardness consistently increased until 30 minutes, and gap of hardness value among the specimens was reduced. The increase in hardness after post-firing heat treatment was caused by grain interior precipitation in the matrix. The softening heat treatment did not affect the increase in hardness by post-firing heat treatment. The precipitated phase from the parent Pd-Ag-Au-rich ${\alpha}$ phase with face-centered cubic structure by post-firing heat treatment was $Pd_3$(Sn, In) phase with face-centered tetragonal structure, which has lattice parameters of $a_{200}=4.0907{\AA}$, $c_{002}=3.745{\AA}$. From above results, appropriate post-firing heat treatment in order to support the hardness of Pd-Ag-Au metal substructure was expected to bring positive effects to durability of the prosthesis.

Manufacturing and testing of flat-type divertor mockup with advanced materials

  • Nanyu Mou;Xiyang Zhang;Qianqian Lin;Xianke Yang;Le Han;Lei Cao;Damao Yao
    • Nuclear Engineering and Technology
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    • v.55 no.6
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    • pp.2139-2146
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    • 2023
  • During reactor operation, the divertor must withstand unprecedented simultaneous high heat fluxes and high-energy neutron irradiation. The extremely severe service environment of the divertor imposes a huge challenge to the bonding quality of divertor joints, i.e., the joints must withstand thermal, mechanical and neutron loads, as well as cyclic mode of operation. In this paper, potassium-doped tungsten (KW) is selected as the plasma facing material (PFM), oxygen-free copper (OFC) as the interlayer, oxide dispersion strengthened copper (ODS-Cu) alloy as the heat sink material, and reduced activation ferritic/martensitic (RAFM) steel as the structural material. In this study, a vacuum brazing technology is proposed and optimized to bond Cu and ODS-Cu alloy with the silver-free brazing material CuSnTi. The most appropriate brazing parameters are a brazing temperature of 940 ℃ and a holding time of 15 min. High-quality bonding interfaces have been successfully obtained by vacuum brazing technology, and the average shear strength of the as-obtained KW/Cu and ODS-Cu alloy joints is ~268 MPa. And a fabrication route for manufacturing the flat-type divertor target based on brazing technology is set. For evaluating the reliability of the fabrication technologies under the reactor relevant condition, the high heat flux test at 20 MW/m2 for the as-manufactured flat-type KW/Cu/ODS-Cu/RAFM mockup is carried out by using the Electron-beam Material testing Scenario (EMS-60) with water cooling. This paper reports the improved vacuum brazing technology to connect Cu to ODS-Cu alloy and summarizes the production route, high heat flux (HHF) test, the pre and post non-destructive examination, and the surface results of the flat-type KW/Cu/ODS-Cu/RAFM mockup after the HHF test. The test results demonstrate that the mockup manufactured according to the fabrication route still have structural and interfacial integrity under cyclic high heat loads.

Natural Dyeing using the Colorants extracted from American Fleabane (Part II) - Dyeing properties on cotton - (개망초 추출물을 이용한 천연염색 (제2보) -면섬유에 대한 염색성-)

  • Shin Younsook;Cho Arang
    • Journal of the Korean Society of Clothing and Textiles
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    • v.28 no.12 s.138
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    • pp.1625-1631
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    • 2004
  • The purpose of this study was to investigate dyeing properties of cotton fabrics by American fleabane extract. Effect of dyeing condition on dye uptake and effect of mordanting on dye uptake, color change and colorfastness were explored. Its affinity to cotton fiber was considerably lower than wool, and its hydrogen bonding was involved in the absorption of American fleabane colorants to cotton fiber. K/S value of pre­mordanting was higher than sim-mordanting or post-mordanting. Except that Sn mordanted showed high K/S value, it did not significantly increase. American fleabane produced mainly yellowish color on mordants and mordanting method. Cotton fabrics showed generally high colorfastness except colorfastness to washing.

Effect of chlorhexidine application on the bond strength of resin core to axial dentin in endodontic cavity

  • Kim, Yun-Hee;Shin, Dong-Hoon
    • Restorative Dentistry and Endodontics
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    • v.37 no.4
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    • pp.207-214
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    • 2012
  • Objectives: This study evaluated the influence of chlorhexidine (CHX) on the microtensile bonds strength (${\mu}TBS$) of resin core with two adhesive systems to dentin in endodontic cavities. Materials and Methods: Flat dentinal surfaces in 40 molar endodontic cavities were treated with self-etch adhesive system, Contax (DMG) and total-etch adhesive system, Adper Single Bond 2 (3M ESPE) after the following surface treatments: (1) Priming only (Contax), (2) CHX for 15 sec + rinsing + priming (Contax), (3) Etching with priming (Adper Single Bond 2), (4) Etching + CHX for 15 sec + rinsing + priming (Adper Single Bond 2). Resin composite build-ups were made with LuxaCore (DMG) using a bulk method and polymerized for 40 sec. For each condition, half of specimens were submitted to ${\mu}TBS$ after 24 hr storage and half of them were submitted to thermocycling of 10,000 cycles between $5^{\circ}C$ and $55^{\circ}C$ before testing. The data were analyzed using ANOVA and independent t-test at a significance level of 95%. Results: CHX pre-treatment did not affect the bond strength of specimens tested at the immediate testing period, regardless of dentin surface treatments. However, after 10,000 thermocycling, all groups showed reduced bond strength. The amount of reduction was greater in groups without CHX treatments than groups with CHX treatment. These characteristics were the same in both self-etch adhesive system and total-etch adhesive system. Conclusions: 2% CHX application for 15 sec proved to alleviate the decrease of bond strength of dentin bonding systems. No significant difference was shown in ${\mu}TBS$ between total-etching system and self-etching system.