• Title/Summary/Keyword: powder method

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Measurement of High Temperature Dielectric Property at Microwave Frequency Using Cavity Perturbation Method (Cavity Perturbation Method를 이용한 마이크로파 주파수대의 고온 유전특성 측정 연구)

  • Kim, Dong-Eun;Jung, Jin-Ho;Lee, Sung-Min;Kim, Hyung-Tae
    • Journal of Powder Materials
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    • v.13 no.6 s.59
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    • pp.455-461
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    • 2006
  • High temperature dielectric constants of the various ceramic materials have been measured using cavity perturbation method. The measurements were applied to refractory, traditional and fine ceramic powder compacts from room temperature to $1200^{\circ}C$. Calibration constant in the equation suggested by Hutcheon et al., was determined from the dielectric constants of reference specimen (teflon and alumina) at room temperature. From these results, informations on the refectory materials were obtained for the microwave kiln design and understanding of the microwave heating effects of ceramics have been improved.

A Study on the Optimization for the Blasting Process of Glass by Taguchi Method (다구찌 기법을 이용한 유리소재의 블라스팅 가공공정의 최적화에 관한 연구)

  • Yoo, Woo-Sik;Jin, Quan-Qia;Chung, Young-Bae
    • Journal of Korean Society of Industrial and Systems Engineering
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    • v.30 no.2
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    • pp.8-14
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    • 2007
  • The powder blasting process has become an important machining technique for the cost effective fabrication of micro devices. This process is similar to sand blasting, and effectively removes hard and brittle materials. A large number of investigations on the abrasive jet machining with such output parameters as material removal rate, penetration and surface roughness have been carried out and reported by various authors. To achieve higher surface roughness, to increase material removal rate and to identify the influence of blasting parameters on the output parameters, we use the taguchi method which is one of the design methods of experiments. We can select process parameters to optimize the blasting process of glass. Experimental results indicate that the taguchi method is useful as a robust design methodology for the powder blasting process.

Optimization of the Plasma Spray Coating Parameters of Ni-5%Al Alloy Powder Using the Taguchi Experimental Method (다꾸찌방법에 의한 Ni-5%Al 합금 분말의 플라즈마 용사코팅 조건의 최적화)

  • 이형근
    • Journal of Welding and Joining
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    • v.20 no.5
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    • pp.120-126
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    • 2002
  • Ni-5%Al alloy powder is widely used as the bond coating powder to improve the adhesive strength between the substrate and coating. The important properties in the bond coating are the deposition efficiency and surface roughness. In this study, it was tried to optimize the plasma spray parameters to maximize the deposition efficiency and surface roughness. In the first step, spray current and hydrogen gas flow rate were optimized in order to increase the deposition efficiency. In the next step, the seven plasma spray variables were selected and optimized to improve both the deposition efficiency and surface roughness using the Taguchi experimental method. By these optimization, the deposition efficiency was improved from about 10 % at the frist time to 51.2 % by the optimization of spray current and hydrogen gas flow rate and finally to 65.2 % by the Taguchi experimental method. The average surface roughness was increased from about $12.9\mu\textrm{m}$ to $15.4\mu\textrm{m}$.

Comparision of Immobilized TiO2 Catalyst for Water Purification (정수처리용 TiO2 고정화 촉매 비교)

  • Jeon, En Ju;Kang, Sung Hwan;Kim, Byung Ug;Rim, Jay Myung
    • Journal of Korean Society of Water and Wastewater
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    • v.13 no.3
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    • pp.101-106
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    • 1999
  • This research aims to compare immobilized catalysts prepared by various methods and determine suitable $TiO_2$ catalyst for water purification. Sol-gel method by Anderson and powder coation method by Tanaka ate famous in the methods to immobilize catalyst. Therefore, the $TiO_2$ catalyst for this research was prepared by sol-gel method and powder coating method. Its structure was tested by X-ray diffractometer (XRD), Scanning electron microseope (SEM). Durability of a catalyst-support couple in an solution was investigated. too. Experimental results were summarized as following; i) Optimum ratio of Ti : $H_2O$ : $H^+$ to obtain stable sol was 1 : 10 : 0.1 and the XRD patterns of $TiO_2$ film immobilized by sol-gel method which were fired at $700^{\circ}C$ showed that the catalyst had an anatase structure. ii) The particle size of $TiO_2$ prepared by sol-gel method was less than $5{\mu}$, but it was observed that coated side was not unifiom. iii) Sol-gel method was very effective to obtain $TiO_2$ catalyst of thin film, but spreadability and durability of a catalyst-support couple in a solution were than $TiO_2$ film immobilized by powder coating method. iv) The particle size of $TiO_2$ immobilized by powder coating method was a little larger than it prepared by sol-gel method, but spreadability and uniformity of $TiO_2$ film and durability of a catalyst-support couple in a solution were better than it immobilized by sol-gel method.

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The Characteristic Studies of Powder Coating System in Wet Slurry Processing Powder Foundation (습식공정 파우더 파운데이션에서 파우더 코팅 시스템의 특성 연구)

  • Lee, Chan-Ki;Lee, Su-Jin;Choi, Jae-Wook;Choi, Yeong-Jin;Han, Shang-Hoon
    • Journal of the Society of Cosmetic Scientists of Korea
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    • v.36 no.3
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    • pp.227-231
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    • 2010
  • Among various make-up products, foundations are widely used to express clear and flawless skin. Foundations can be classified by its formula to 3 types, liquid foundation, powder foundation, and oil dispersion foundation. Powder foundations are easy to carry and use, so it is commonly possessed. In the R&D point of view, the developing method of powder foundations can be classified again to 3 types. Dry-process, baked-process, and the wet slurry-process. The fact that the wet slurry-process goes through either the back injection method or the front injection method is previously known. The front injection process is used as the main method in this study. We observed the quality dependence on the kind of solvent and the powder coating system. In brief, when water was used as the main solvent, the hardness increased than when volatile silicones or hydrocarbons were used. And the sensory results were shown to prefer volatile solvents (silicones or hydrocarbons) over water. Similarly, when the amino acid-coating system was applied, the hardness was shown to increase, when silicone-coating system shown no specific change. By these results, tailor-made powder foundations targeting specific customer grades can be easily produced.

Development of Metal nano Powder Imprinting Process for Fabrication of Conductive Tracks (금속 배선 제작을 위한 메탈 나노 파우더 임프린팅 공정기술 개발)

  • Kim, J.;Kim, H.;Lim, J.;Bae, H.;Choi, M.;Kang, S.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2007.05a
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    • pp.371-374
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    • 2007
  • A method for metal nano powder imprinting is proposed as a patterning process for conductive tracks that is inexpensive and scalable down to the nanoscale. Conductive tracks with line widths of $0.5{\sim}20{\mu}m$ were fabricated using this method. The processing conditions were optimized to avoid various types of defects, and to increase the degree of sintering and electric conductivity of the imprinted conductive tracks. The mean electric resistivity of the conductive tracks imprinted under optimum conditions was $8.95{\mu}{\Omega}{\cdot}cm$, which is in the range required for practical applications.

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Epitaxial growth of Tin Oxide thin films deposited by powder sputtering method

  • Baek, Eun-Ha;Kim, So-Jin;Gang, Hyeon-Cheol
    • Proceedings of the Korean Vacuum Society Conference
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    • 2015.08a
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    • pp.185.2-185.2
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    • 2015
  • Tin Oxide (SnO2) has been widely investigated as a transparent conducting oxide (TCO) and can be used in optoelectronic devices such as solar cell and flat-panel displays. In addition, it would be applicable to fabricating the wide bandgap semiconductor because of its bandgap of 3.6 eV. There have been concentrated on the improvement of optical properties, such as conductivity and transparency, by doping Indium Oxide and Gallium Oxide. Recently, with development of fabrication techniques, high-qulaity SnO2 epitaxial thin films have been studied and received much attention to produce the electronic devices such as sensor and light-emitting diode. In this study, powder sputtering method was employed to deposit epitaxial thin films on sapphire (0001) substrates. A commercial SnO2 powder was sputtered. The samples were prepared with varying the growth parameters such as gas environment and film thickness. Then, the samples were characterized by using XRD, SEM, AFM, and Raman spectroscopy measurements. The details of physical properties of epitaxial SnO2 thin films will be presented.

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Fabrication of WC-17%Co Composite Powder for Thermal Spray by Spray-Drying Method and HVOF Thermal Spray Characteristics (분무건조법에 의한 용사용 WC-17%Co 복합분말제조 및 HVOF(High Velocity Oxy-Fuel) 용사특성)

  • 설동욱;김병희;임영우;정민석;서동수
    • Journal of Welding and Joining
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    • v.14 no.6
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    • pp.101-108
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    • 1996
  • In this study, WC-l7wt% Co composite powder for thermal spray was fabricated by spray drying method. The agglomerated composite powder had spheroidal morphology and the particle size distribution was 20~60${\mu}{\textrm}{m}$. WC and Co were distributed homogeneously. However, the strength of the spray-dried agglomerate was low due to the pores within the agglomerate. Therefore, the spray-dried agglomerate was broken down during HVOF thermal spray and the microstructure was inhomogeneous with many pores within the coating layer. And the decomposition of WC to W and $W_{6}$ $C_{2.54}$ was accelerated. The strength and flowability of the agglomerate were greatly improved by sintering heat treatment(110$0^{\circ}C$, 1 hour, hi atmosphere), and then the coating layer showed dense and homogeneous microstructure with well-developed splats. The hardness of the coating layer was H $v_{300}$ = 1072.2.2.

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Fabrication of fine BSCCO-2223 precursor powder by spray pyrolysis process (분무 열분해방법에 의한 미세 BSCCO-2223 전구분말의 제조)

  • 김성환;유재무;고재웅;김영국;박기호
    • Progress in Superconductivity
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    • v.5 no.1
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    • pp.65-69
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    • 2003
  • Many researches on fabrication process for BSCCO precursor powders have been developed for high J$_{c}$ BSCCO-2223 tape. Spray pyrolysis method for fabrication of precursor powder has many advantages, such as high purity, fine particle size and low carbon content of BSCCO precursor powder. Fine, spherical powders were prepared by ultrasonic spray pyrolysis from the aqueous solution of metal nitrates. BSCCO precursor powders were synthesized with various solutes concentration and heat treatment conditions. Average particle size for spray pyrolysis powders was $1.5∼3\mu\textrm{m}$. Bi-2223/Ag tape was prepared by PIT method and followed by various sintering conditions. BSCCO precursor powders were characterized by XRD, SEM, EDS, Carbon content and particle size analysis.s.

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A Study on the Electromagnetic Shielding Characteristics of Crash Pad Using Electrically Conductive Powders and Al-coated Glass Fiber as Filler in Automotive (전기전도성 분말과 알루미늄 코팅 유리섬유를 사용한 자동차용 크래쉬패드의 전자파 차폐 특성에 관한 연구)

  • Cho, Hong;Jeoung, Sun-Kyoung;Kim, Byeong-Woo
    • Journal of Powder Materials
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    • v.21 no.2
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    • pp.124-130
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    • 2014
  • The automotive industry is moving from the internal combustion engine to electric drive motors. Electric motors uses a high voltage system requiring the development of resources and components to shield the system. Therefore, in this study, we analyze electromagnetic interference (EMI) shielding effectiveness (SE) characteristics of an auto crash pad according to the ratio of electrically conductive materials and propylene. In order to combine good mechanical characteristics and electromagnetic shielding of the automotive crash pad, metal-coated glass fiber (MGF) manufacturing methods are introduced and compared with powder-type methods. Through this study, among MGF methods, we suggest that the chopping method is the most effective shielding method.