• Journal of Technologic Dentistry
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• v.18 no.1
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• pp.5-13
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• 1996

Among investment for dental casting, we selected 4 kinds of investment(2 Gypsum-bonded and 2 Phosphate-bonded) and prepard 120 specimen by dividing into two cast of using Ring and Ringless case from $0^{\circ}C$ to $30^{\circ}C$ at interval of $10^{\circ}C$ to invest in fluence on the fitness of casting body according to the liquid temperature of Gypsum-bonded and Phosphate-bonded investment. The result was as follows; 1. Gypsum-bonded investment showed best fitness at $30^{\circ}C$ representing difference of singnificance in order of $20^{\circ}C$, $10^{\circ}C$, and $0^{\circ}C$, From the difference of investment, Deguvest was proved superior than Cristobalite. 2. Phosphate-bonded investment showed no severe difference at $10^{\circ}C$ and $20^{\circ}C$, but showed better fitness at $10^{\circ}C$, representing difference of significance in order of $0^{\circ}C$, $30^{\circ}C$, difference of significance was shown between investment also. 3. In Ringless investing method, there were no difference of significance in Deguvest CF and Unovest. 4. When using a Ring with a Sheet of asbestos liner installed, there was some difference of significance representing superiority of Ringless investing method.

• The Journal of Korean Academy of Prosthodontics
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• v.41 no.3
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• pp.342-350
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• 2003

Statement of problem. Titanium-Nickel alloy might be used in various prosthetic restorations since it has a unique property such as super-elasticity and high fatigue resistance. However, little is known about the casting ability of this alloy. Purpose. This in vitro study compared the casting accuracy and the porosity made with different investments and various sprue designs to ascertain what casting condition would be better for the fabrication of Ti-Ni cast restorations. Material and methods. A total of 70 Ti-Ni alloy crowns were made and divided into 7 groups of 10 copings on a metal master die. For measuring the effect of the sprue numbers, two groups with one and two 8-gauge sprues were compared. Moreover, the results of the conventional sprue and the double thickness sprues were compared. Three investments were used; carbon free phosphate bonded investment, titanium investment and gypsum bonded investment. The cast restorations were evaluated at 48 points on the entire circumferential margin with a stereomicroscope measuring in micrometers. Each crown was radiographically examined for casting defects and porosity. Data on casting accuracy were analyzed using two-way and Post hoc Scheffe's comparison to determine whether significant differences existed at the 95% confidence level. Student-Newman-Keuls test were performed to identify significant differences in the number of voids. Results. The double sprueing group and double thickness group had significantly less marginal discrepancy than the single sprueing group (P<.05 and P<.01, respectively). The castings with phosphate bonded investment showed the least marginal discrepancy and the smoothest surface. The castings invested in the gypsum bonded investment had the greatest gaps in margin and the largest failure rate. The double sprueing group and phosphate bonded investment group had significantly smaller void numbers and smaller void size than the other groups. Conclusion. Within the limitations of this in vitro study, the casting accuracy of the groups using thicker, double sprue design and the phosphate bonded investment was significantly superior. Moreover, void number and size were less than other groups.

• Journal of Technologic Dentistry
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• v.27 no.1
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• pp.57-63
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• 2005

Experimental Ti-13%Zr and Ti-13%Zr-5%Cu alloys were made in an argon-arc melting furnace. The grade 2 CP Ti was used to control. To investigate the surface reaction layers produced by the reaction with mold materials and the influence of the reaction layers on the hardness of castings, A phosphate bonded $SiO_2$ base investment was used as mold material, and microstructure observation and hardness test were performed. The surface reaction layers of Ti-13%Zr and Ti-13%Zr-5%Cu alloys were thinner than that of CP Ti had a clearly multiple structure. A difference of the hardness between surface and inner of the Ti-13%Zr and Ti-13%Zr-5%Cu alloys became less than that of CP Ti. From the results, it was found that the Ti-Zr-(Cu) based alloys were possible to cast with $SiO_2$ base investment without the great changes of mechanical properties of the castings.

• Journal of Technologic Dentistry
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• v.19 no.1
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• pp.55-61
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• 1997

To observe the difference of the special liquid influencing to the fitness of casting body among the many elements influencing to the die fitness of the casting body, we fit L/P ratio each investment, using two kinds of phosphate bonded investment, divided the density of the special liquid by 5 groups(Density 100, 75, 50, 25, 0), made 10 copying per each group and experiment 10 groups, totally 100 copying and finally we could get the result as following ; 1) In such a case of CB-30, the casting fitness of the density 100 of special liquid, group 6, was the best and in order of the density 75, 50, 25, 0 the fitness is better. 2) In such of Denti-vest, the fitness of the density 100 of the special liquid, group 1, was the best and in order of the density 75, 50, 25, 0 the fitness is better. 3) Therefore we should change the density according to the transformation of the environment as investing because of increasing the expansion of phosphate bonded investment, as increasing the density of the special liquid.

• Journal of Technologic Dentistry
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• v.27 no.1
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• pp.73-78
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• 2005

The surface-reacted layer of titanium castings greatly affects their mechanical properties. This study analyzed the interfacial zone of Ti-20%Zr-5%Cr alloy castings obtained from phosphate bonded investment and examined the relationship between the surface-reacted layer and hardness. The Vickers hardness of cast disks were tested at 20$\mu m$ intervals from the surface to 120$\mu m$ in depth. The cross-section was observed metallurgically, and line profile of the reacted layer was conducted under the EDX. The surface-reacted layer of Ti-20%Zr-5%Cr alloy is showed a similar tendency to Ti-6%Al-4%V alloy in thickness, and also Si diffusion in multiple reacted layer of Ti-20%Zr-5%Cr alloy is less than cp Ti and similar to Ti-6%Al-4%V alloy. The Vickers hardness in the surface layer was greater than in the inner part, and the Vickers hardness of Ti-20%Zr-5%Cr alloy ranged 650 to 390 and cp Ti ranged 810 to 160, Ti-6%Al-4%V alloy ranged 710 to 530 respectively.

• Journal of Technologic Dentistry
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• v.28 no.1
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• pp.9-17
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• 2006

The purpose of this study was to evaluate the titanium castability with a spin type casting machine(TiCast, Super R, Selec, Osaka. Japan). We tested phosphate bonded investment "Rematitan$^{(R)}$Plus(Dentaurum, Inc., Pforzheim, Germany)"of mesh grid pattern and plate pattern. Four different mold temperatures(room temperature, 200$^{\circ}C$, 400$^{\circ}C$ and 600$^{\circ}C$) were prepared for the present study. In mesh grid pattern with spruing of $\varphi$0.88㎜ dimeter, when the mold temperature increased, high percentage of castability was gained. Mold temperature showed a highly significant(p<0.05) correlation on the castability, In plate pattern, the higher the mold temperature during casting, the greater the adhesive phenomenon between Ti surface and the investment.

• Journal of Technologic Dentistry
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• v.32 no.4
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• pp.297-305
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• 2010

Purpose: The purpose of this study was to observe the change of metal-mold reaction and surface roughness in titanium casting specimens for phosphate-silica alumina bonded investment with mold temperatures. Methods: The metal-phosphate silica alumina bonded mold interface reaction and surface roughness of titanium casting specimens according to mold temperatures were investigated. The Specimens were analysed by scanning electron microscopy and surface roughness tester. Results: The oxidation behavior indicated by the growth of oxide thickness. The titanium-oxide layer were consisted two layer of a porous external and a dense internal one. The reaction layer and surface roughness increased with increasing investment material temperature. Conclusion: In this work, The most suitable mold temperature in casting of pure titanium was $200^{\circ}C$.

• Journal of Technologic Dentistry
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• v.23 no.1
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• pp.115-121
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• 2001

This study was investigated on effect of implant system about investment condition and burn out temperature. Posterior bridges were fabricated by using plastic sleeve and gold sylinder. The results were as follows; In plastic sleeve test and fitting cast copings. the phosphate bonded investment showed better gypsum bonded investment. The pure special liquid showed better margin fitness compared with mixed liquid (special liquid + distilled water). In gold cylinder test. the good burn out temperature of Ceramic PFG and Crown Gold was evaluated $0^{\circ}C$ to $820^{\circ}C$ and was decreased on $780^{\circ}C$ for 30 minutes. $0^{\circ}C$ to $750^{\circ}C$ and was decreased on $650^{\circ}C$ for 30 minutes.

• Journal of Technologic Dentistry
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• v.23 no.2
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• pp.203-210
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• 2002

This test is to conduct applied research the reaction area of the Ti-cast metal body which is made use of Dental Phosphate-silica alumina bonded investment material selling at a market, and the cooling method is how to effect on the acicular. The experimentation is as followings, 1. Experimental specimens After invest with Dental Phosphate-silica alumina bonded investment material, the $10{\times}10{\times}1.0mm^3$ wax pattern was casted by Dental high vacuum argon centrifugal casting machine. 2. Test We can analyze SEM/EDS, XRD utilize the fractography(an optical microscope). 3. Conclusion The pure cast metal body constituted of reaction products layer, stability layer and contamination layer. This pure cast have no connection with the cooling condition. The pure Titanium shows difference in a component distribution according to the cooling condition. Through this experimentation we can establish that acicular in the pure Ti-cast metal is consist of Hexagonal structure a=2.9505$\AA$, c=4.6826$\AA$.

• The Journal of Korean Academy of Prosthodontics
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• v.28 no.1
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• pp.203-216
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• 1990

The purpose of this study was to evaluate the cervical margin fitness in the collarless metal ceramic crowns formed by different techniques. Specimens were divided as follows : the metal ceramic crowns with metal butt margin as group I, the collarless metal ceramic crowns formed with resin binder technique as group II, and the collarless metal ceramic crowns formed with shoulder powder mixed with phosphate-bonded investment liquids on a refractory die as group III. Each group was made of five specimens, and their marginal fitness on each epoxy die was evaluated under scanning electron microscope of x200 magnification at three measuring points : mesial, central, distal. The following results were obtained. 1. The metal ceramic crowns with metal butt margin exhibited significantly better marginal fitness than the collarless metal ceramic crowns. The marginal fitness in descending order was group I, III, II. 2. The collarless metal ceramic crown formed with resin binder technique had the worst marginal fitness & showed cervical color variation and dermacation between the corrected porcelain & the dentin porcelain. 3. The collarless metal ceramic crowns formed with shoulder powder mixed with phosphate-bonded investment liquids on a refractory die exhibited significantly better marginal fitness & sharper marginal configuration than the other collarless group.