• Title/Summary/Keyword: optimal experimental design

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Optimization of Ingredient Mixing Ratio for Preparation of Steamed Foam Cake with Added Saltwort (Salicornia herbacea L.) (함초 첨가 거품형 찜케이크의 재료 혼합비율의 최적화)

  • Kim, Yu-Suk;Kwak, Sung-Ho;Jang, Myung-Sook
    • Korean journal of food and cookery science
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    • v.22 no.5 s.95
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    • pp.666-680
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    • 2006
  • To obtain basic data for the utilization of saltwort (Salicornia herbacea L.) as a functional ingredient in steamed foam cake, the optimum component ratios for major raw ingredients (saltwort, salt, and wheat flour) as independent variables that affect the product quality were scientifically determined using RSM (response surface methodology) technique. A three-factor and five-level rotational central composite design was used for treatment arrangement. The complete design consisted of 16 experimental points. The three independent variables selected for the RSM experiment were amounts of saltwort (X$_1$, 5${\sim}$25 g), salt (X$_2$, 0${\sim}$10 g), and wheat flour (X$_3$, 470${\sim}$530 g). The optimum responses in specific gravity of the batter and volume, color, texture, and sensory evaluation result of the cake were obtained. The specific gravity and viscosity of the batter at p<0.01 was verified from the regression curve. The characteristic of the batter was influenced by all independent variables, but was extremely dependent on the amount of saltwort ordinary points of the surface responses from the batter formed the minimum points for specific gravities of the batter while viscosities of the batter appeared with the saddle points. Analysis of the response indicated that the amount of saltwort was the most influential factor over the physical properties of the cake, among the dependent variables. Ordinary points of the surface responses from the cake formed the maximum points for loaf volume, hardness gumminess, and chewiness, while Hunter colorimetric parameters appeared with the saddle points. The result indicated that level of the saltwort deviating more or less from the optimal amount decreased the volume and increased the specific gravity with less tender product. Ordinary points of the surface responses of the sensory evaluation scores from the cake formed the maximum points for appearance, flavor, softness, and overall acceptability, while color values appeared with the saddle points. The result also indicated that the level of the saltwort deviating more or less from the optimal amount reduced the preference for the product. Integration of the optimum responses common to all dependent variables that overlapped all the contour maps finally indicated that the combination of 8.3${\sim}$13.8 g saltwort, 2.5${\sim}$6.6 g salt, and 486.5${\sim}$511.5 g wheat flour under the selected preparation recipe optimized the physical and sensory properties in the teamed foam cakes. Practical preparation of the product with median amounts of the ingredients, i.e., 11.0 g saltwort, 4.6 g salt, and 499.0 g wheat flour resulted in similar qualities to the predicted responses. In conclusion, these study results indicated that preparation of steamed foam cake with added saltwort ingredient could potentially produce a more nutritious product with less salt. Further research is required to acquire the optimum levels for sub-ingredients to improve the product quality.

Optimization of O/W Emulsion with Natural Surfactant Extracted from Medicago sativa L. using CCD-RSM (CCD-RSM을 이용한 알팔파 추출물인 천연계면활성제가 포함된 O/W 유화액의 최적화)

  • Seheum Hong;Jiachen Hou;Seung Bum Lee
    • Applied Chemistry for Engineering
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    • v.34 no.2
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    • pp.137-143
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    • 2023
  • In this study, natural surfactants were extracted from Medicago sativa L. The O/W emulsification processes with the extracted natural surfactants were optimized using central composite design model-response surface methodology (CCD-RSM) and a 95% confidence interval was used to confirm the reasonableness of the optimization. Herein, independent parameters were the ratio of saponins to total surfactant (P), amount of surfactant (W), and emulsification speed (R), whereas the reaction parameters were the emulsion stability index (ESI), mean droplet size (MDS), and viscosity (V). Using the multiple reaction, the optimal conditions for the ratio of saponins to total surfactant, amount of surfactant, and emulsification speed for O/W emulsification were 49.5%, 9.1 wt%, and 6559.5 rpm, respectively. Under these optimal conditions, the expected values of ESI, MDS, and V as the reaction parameters were 89.9%, 1058.4 nm, and 1522.5 cP, respectively. The values of ESI, MDS, and V from these expected values were 88.7%, 1026.4 nm, and 1486.5 cP, respectively, and the average experimental error for validating the accuracy was about 2.3 (± 0.4)%. Therefore, it was possible to design an optimization process for evaluating the O/W emulsion process with Medicago sativa L. using CCD-RSM.

A Study on Determining the Optimal Size of Bicycle Waiting Zone under Hook-Turn Operation (Hook-Turn 통행방식의 적정 자전거 대기공간 크기 결정에 관한 연구)

  • Lim, Guk-Hyun;Kim, Nam-Sun;Lee, Sang-Soo;Nam, Doohee;Kim, Jeong-Tae
    • The Journal of The Korea Institute of Intelligent Transport Systems
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    • v.15 no.5
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    • pp.42-53
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    • 2016
  • This study aims to evaluate the performance of Hook-turn operation with various sizes of bicycle waiting zone(WZ) and to determine the optimal size of bicycle WZ under various traffic and control circumstances. An extensive simulation study was performed to examine bicycle and vehicle delay trends for given experimental design. Results showed that vehicle delay was insensitive to the size of waiting zone, but bicycle delay was reduced as the size of waiting zone increased in general. The delay performance indicated a similar trend between with RTOR and without RTOR operation, but vehicle delay slightly increased and bicycle delay slightly decreased without RTOR. Regarding to optimal waiting zone size, 6 WZ was recommended for general conditions with RTOR, but 9 WZ was recommended when bicycle left-turn volume was greater than 120 v/h. 6 WZ was recommended for general conditions without RTOR, but 12 WZ was recommended when bicycle left-turn volume was greater than 90 v/h.

An Experimental Approach to Evaluate the Desulfurization Yield in Spray Drying Sorber (반건식 세정기의 산성가스 제거성능에 관한 실험적 연구)

  • Yang, Hyun-Mo;Kim, Sang-Soo
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.24 no.4
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    • pp.589-598
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    • 2000
  • A pilot-scale Spray Drying Sorber (SDS) system was set up to evaluate the effect of spray characteristics on the desulfurization yield. The size distribution and the Sauter Mean Diameters of slurry droplets were measured in advance using the optical size measurement system, Malvern 2600. The desulfurization yield of the drying chamber by size was measured for the conditions of inlet gas and spray injection. As a reagent, 10% limestone slurry of $Ca(OH)_2$ was treated with flue gas containing $SO_2$, and the combustion gas analyzer and gas detectors were attached to measure the $SO_2$ concentration. With a flow rate of 144 Nm3/h and a temperature range of $200{\sim}300^{\circ}C$, the experiments were performed for the Stoichiometric Ratio (SR) of 1.0 to 3.0 and droplet mean diameter of 6.5 to $34.3{\mu}m$. In case of smaller spray droplets, the desulfurization efficiency improved due to the increase of total droplet surface area, while the reduction in evaporation time reduced the contact time between the droplets and $SO_2$ gas. In some typical region of droplet diameter, this negative effect, reduction of contact time, became dominant and the desulfurization yield decreases the desulfurization yield in spite of the expansion in absorption area. These results revealed that there exists the optimal size of spray droplets for a given state, which is determined by the compromise between the total surface area of slurry droplets and the evaporation time of droplets. The measurements also indicated that the inlet temperature of flue gas changes the optimal injection condition by varying the driving force for evaporation. The results confirm that the effect of the evaporation time of slurry droplets should be considered in analyzing the desulfurization yield as well as the total surface area, for it is a significant aspect of the correlation with the capabilities of $SO_2$ absorption in wet droplets. In conclusion, the optimal condition of spray can be determined based on these results, which might be applied to design or scale-up of SDS system.

The Optimal Addition Level of Loquat Leaf Extract in the Rice Beverages (반응 표면 분석을 통한 비파엽 첨가 쌀음료의 비파엽 첨가량의 결정)

  • Kim, Il Gon;Kim, Ki Myong
    • The Korean Journal of Food And Nutrition
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    • v.26 no.2
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    • pp.226-233
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    • 2013
  • The optimal amount of loquat leaf extract (LLE, $18^{\circ}$ Brix), fructose, and cream were determined to develop a rice beverage supplemented with LLE. The loquat leaves were extracted by water at $80^{\circ}C$ for 6 hrs and then concentrated to 18% of solid for 1 hr at the same temperature to extraction. To investigate the optimal concentration of the additives, the response surface methodology (RSM) was employed for the experimental design. The addition amounts of the additives were coded. Sweetness, bitterness, off-taste, color, taste preference, and total preference were affected significantly (P<0.05) by the addition of LLE, fructose, and cream. Cream masked the bitterness and off-taste. The total preference of the LLEsupplemented rice beverage showed a lower score than the commercialiy available rice beverages. To achieve the preference level of the commercial rice beverages, the regression between fructose and LLE concentration was calculated as: fructose= $0.618{\times}(LLE)^2+0.406{\times}(LLE)$. Conclusively, cream had an effect of masking the bitterness of rice milk, and the preference was highly related to the addition amount of fructose.

Optimal Hydraulic Loading for Ammonia Control in Water Recycling Fish Culture System (순환여과식 양어장의 암모니아 제어를 위한 최적 수리학적 부하)

  • LEE Suk-Mo;KIM Do-Hee;SONG Kyo-Ouk
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.25 no.3
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    • pp.176-180
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    • 1992
  • Nitrification Is an important facet of water recycling fish culture system, because the toxic cation ammonia is converted to the innocuous anion nitrate. This study was attempted to find the optimal design factor of submerged filter for ammonia removal in water recycling fish culture system. The experimental system was designed submerged filter with corrugated skylight plate, and operated in the fish farm, National Fisheries University of Pusan. When the influent ammonia concentration was about 10mg/l (9.43-13.66mg/l) nitrification rates were tested for the removal of ammonia over a four stage of the hydraulic loadings. The submerged filter removed 76.24, 62.88, 39.09 and $9.20\%$ of the ammonia to hydraulic load of 0.028, 0.037, 0.056 and $0.111m^3/m^2$. day, respectively. We can apply the above data to the material balance on the ammonia concentration in a fish reservoir, and conclude that the maximum allowable ammonia production was 1.52mg/min, and the optimal hydraulic loading was $0.047m^3/m^2$\;\cdot day$, in order to maintain the ammonia concentration below 10mg/l in the fish reservoir.

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Optimal Abrasion Conditions for Separating Aggregate and Cement paste for Using Waste Concrete Fine Powder as Decarbonization Raw Material (폐콘크리트 미분말을 탈탄산 원료로 사용하기 위한 골재와 시멘트페이스트 분리의 최적 마쇄 조건 분석)

  • Ha-Seog Kim;Min-Chul Lee
    • Land and Housing Review
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    • v.14 no.4
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    • pp.121-129
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    • 2023
  • In this study, we attempted to reduce CO2 generated during manufacturing by replacing limestone (CaCO3), a carbonate mineral used to produce cement clinker, with a decarbonated raw material to which CO2 is not bound. The raw material for decarbonization was cement paste attached to waste concrete, among various industrial by-products. Waste concrete has cement paste adhered to the aggregate, which cannot be separated efficiently by general crushing and grinding methods. Peeling and grinding methods effectively remove only the cement paste without damaging the original aggregate. The abrasion time, steel ball type, and steel ball ratio were selected as effective factors for Abrasion. An optimal abrasion experiment was conducted to produce waste concrete fine powder containing decarbonated CaO as a cement clinker raw material through an experimental design method. The experiment revealed that the optimal conditions for producing waste concrete fine powder were an abrasion time of 7 minutes, a steel ball size for pulverization of 8 mm, and a steel ball ratio for pulverization of 0.6.

Antibacterial Properties of Extracts from Abies holophyllaand Pinus koraiensisNeedles Against Escherichia coli and Staphylococcus aureus (전나무와 잣나무 잎 추출물의 대장균과 황색포도상구균에 대한 항균특성)

  • Young Woo Choi;Seung Bum Lee
    • Applied Chemistry for Engineering
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    • v.35 no.3
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    • pp.248-254
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    • 2024
  • In this study, functional substances with antibacterial properties were extracted from the needles of Abies holophylla and Pinus koraiensis, and optimized using the central composite design-response surface methodology (CCD-RSM). The optimal extraction conditions for Abies holophylla were an extraction temperature of 59.5 ℃ and an ethanol/ultrapure water volume ratio of 69.5 vol.%, resulting in an extraction yield of 13.5% and inhibition diameters of 11.6 mm against Escherichia coli (E. coli) and 9.3 mm against Staphylococcus aureus (S. aureus). For Pinus koraiensis, the optimal extraction conditions were an extraction temperature of 59.2 ℃ and an ethanol/ultrapure water volume ratio of 67.8 vol.%, resulting in an extraction yield of 4.8% and inhibition diameters of 7.9 mm against E. coli and 12.5 mm against S. aureus. The actual experimental results under these optimal conditions showed that an extraction yield from Abies holophylla needles was 13.0% and an inhibition diameter of 11.7 mm against E. coli and 9.2 mm against S. aureus, indicating an error rate of approximately ± 2.3%. For Pinus koraiensis needles, the extraction yield was 5.1%, with inhibition diameters of 7.5 mm against E. coli and 12.3 mm against S. aureus, indicating an error rate of ± 4.23%.

Assessment of Biochemical Efficiency for the Reduction of Heavy Metal and Oil Contaminants in Contaminated Soils (토양내 중금속 및 유류 오염농도 저감을 위한 생화학적 기작의 효율성 평가)

  • Kim, Man-Il;Jeong, Gyo-Cheol;Kim, Eul-Young
    • The Journal of Engineering Geology
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    • v.22 no.3
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    • pp.253-262
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    • 2012
  • With the aim of remediating soils contaminated by heavy metals and oil, experimental research was conducted to evaluate the optimal design factors for remediation in terms of efficient soil washing methods and processes. The experiments employed absorptiometric analysis and gas chromatography methods to reduce the concentration of heavy metals such as cooper (Cu), lead (Pb), and zinc (Zn), and total petroleum hydrocarbons (TPH) in contaminated soils. The experimental processes consisted of deciding on the washing solution, washing time, and dilution ratio for contaminated soils. A dissolution analysis of heavy metals was then performed by the addition of surfactant, based on the results of the decision experiments, and the injection processes of microbes and hydrogen peroxide were selected. The experimental results revealed that reduction effects in contaminated soils under the experimental conditions were most efficient with hydrochloric acid 0.1 mole, washing time 1 hour, and dilution ratio 1:3, individually. Additional reduction effects for heavy metals and TPH were found with the addition of a washing solution of 1% of surfactant. The addition of microbes and hydrogen peroxide caused a reduction in TPH concentration.

Production Medium Optimization for Monascus Biomass Containing High Content of Monacolin-K by Using Soybean Flour Substrates (기능성 원료를 기질로 이용하는 Monacolin-K 고함유 모나스커스 균주의 생산배지 최적화)

  • Lee, Sun-Kyu;Chun, Gie-Taek;Jeong, Yong-Seob
    • KSBB Journal
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    • v.23 no.6
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    • pp.463-469
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    • 2008
  • During the last decade, monacolin-K biosynthesized by fermentation of red yeast rice (Monascus strains) was proved to have an efficient cholesterol lowering capability, leading to rapid increase in the market demand for the functional red yeast rice. In this study, the production medium composition and components were optimized on a shake flask scale for monacolin-K production by Monascus pilosus (KCCM 60160). The effect of three different soybean flours on the monacolin-K production were studied in order to replace the nitrogen sources of basic production medium (yeast extract, malt extract and beef extract). Among the several experiments, the production medium with dietary soybean flour to replace a half of yeast extract was very good for monacolin-K production. Plackett-Burman experimental design was used to determine the key factors which are critical to produce the biological products in the fermentation. According to the result of Plackett-Burman experimental design, a second order response surface design was applied using yeast extract, beef extract and $(NH_4)_2SO_4$ as factors. Applying this model, the optimum concentration of the three variables was obtained. The maximum monacolin-K production (369.6 mg/L) predicted by model agrees well with the experimental value (418 mg/L) obtained from the experimental verification at the optimal medium. The yield of monacolin-K was increased by 67% as compared to that obtained with basic production medium in shake flasks.