• Title/Summary/Keyword: morphology method

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Pervaporation Separation of Water-isopropanol Mixtures through Modified Asymmetric Polyetherimide Membrane: the Effect of NaOH Concentration and Modification Reaction Times on the Morphology of the Morphology of the Modified Membranes (개질 비대칭 폴리에테르이미드막을 통한 물-이소프로판올 혼합물 투과증발 분리: NaOH용액의 농도와 개질반응 시간에 따른 몰폴로지 변화)

  • Kim, Sang-Gyun;Jegal, Jonggeon;Lee, Kew-Ho
    • Applied Chemistry for Engineering
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    • v.10 no.4
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    • pp.515-522
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    • 1999
  • Asymmetric polyetherimide membrane were prepared by phase inversion method, and the effects of NaOH concentration and reaction time on the morphology change of the polyetherimide membranes were studied. The morphology of skin layers varied from dense structure to sphere structure with increasing concentration of modification solution. The thickness of dense layer increased with increasing reaction time. However, when either the concentration of modifying solution was very high or the reaction time was very long, the dense layers of the asymmetric membrane were disappeared. From these results, it was found that the surface morphology of the asymmetric polyetherimide membranes depended strongly on the modification conditions such as concentration of modification solution and reaction time. These results might be explained by the hydrolysis reaction of polyetherimide into polyamic acid by the NaOH solution.

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Analysis of Filtration Performance by Brownian Dynamics (Brownian Dynamics 를 이용한 입자 포집 과정 및 여과 성능 해석)

  • Bang, Jong-Geun;Yoon, Yoong-Sup
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.33 no.10
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    • pp.811-819
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    • 2009
  • In the present study, deposition of discrete and small particles on a filter fiber was simulated by stochastic method. Trajectory of each particle was numerically solved by Langevin equation. And Lattice Boltzmann method (LBM) was used to solve flow field around the filter collector for considering complex shape of deposit layer. Interaction between the flow field and the deposit layer was obtained from a converged solution from an inner-loop calculation. Simulation method is properly validated with filtration theory and collection efficiency due to different filtration parameters are examined and discussed. Morphology of deposit layer and its evolution was visualized in terms of the particle size. The particle loaded effect on collection efficiency was also discussed.

A Laser-Applied Hybrid Focus Method for the Measurement of a Surface Morphology with Depth Discontinuity (깊이불연속 형상 측정을 위한 레이저 응용 하이브리드 초점법)

  • Kim, Gyung-Bum;Shin, Young-Su;Moon, Soon-Hwan
    • Journal of the Korean Society for Precision Engineering
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    • v.23 no.9 s.186
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    • pp.111-118
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    • 2006
  • A hybrid focus method with multiple laser slits is newly proposed for the measurement of surface morphology with depth discontinuity, and it is based on the integration of DFB and DFF. Rough depth information is estimated through calibration tables which are constructed by DFD with multiple laser slits, and then DFF is applied to only each specific depth range using the rough depth information resulting from DFD. The proposed hybrid method gives more accurate results than DFD and DFF, and faster measurement than DFF in the vicinity of depth discontinuity Its performance is verified through experiments of calibration blocks with sharp depth discontinuity.

Synthesis of ZnWO4 Nanopowders by Polymerized complex Method (Polymerized complex법에 의한 ZnWO4 nanopower의 제조)

  • Ryu, Jeong-Ho;Lim, Chang-Sung;Auh, Keun-Ho
    • Journal of the Korean Ceramic Society
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    • v.39 no.3
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    • pp.321-326
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    • 2002
  • ZnWO$_4$ nano-powders were successfully prepared by polymerized complex method using zinc nitrate and tungstic acid as starting materials. In order to investigate the thermal decomposition and crystallization process, the polymeric precursors were heat-treated at temperatures from 300 to 600$^{\circ}$C for 3 h, and the heat-treated powders were characterized by XRD and FTIR. The surface morphology of the heat-treated powders were observed using SEM and TEM. The crystallite size was measured by X-ray analysis. Crystallization of the ZnWO$_4$ powders were detected at 400$^{\circ}$C and entirely completed at a temperature of 600$^{\circ}$C. The particles heat-treated 400 and 500$^{\circ}$C showed primarily co-mixed morphology with spherical and silkworm-like forms, while the particles heat-treated at 600$^{\circ}$C showed more homogeneous morphology. The average crystalline size were 19.9∼24.nm showing an ordinary tendency to increase with the temperatures from 400 to 600$^{\circ}$C.

Characteristics of the Haute Couture Design in Paris and Rome (파리와 로마의 오뜨 꾸띄르(Haute Couture) 디자인의 특성)

  • 공미선
    • Journal of the Korean Society of Costume
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    • v.39
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    • pp.39-58
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    • 1998
  • In this research, first of all, the special feat-ures of Haute Couture design world (1990∼1996) prevailed in Paris and Rome are investigated, and additionally the understanding of collection concept and design structure analysis are performed to show the various method-ology of creative design. Expression method and design method are the main criteria in analyzing, and the main results of this research are summarized as follows : 1. Most of designers in Paris and Rome ex-press the traditional costume style. Paris designers are focusing on the expression of design morphology through the abstraction and re-appearance without being confined to theme expression ; Rome designers are expressing their main ideas utilizing the fashion image as their theme in lieu of expressing the design morphology. 2. Most of the designers in Paris and Rome are using simple lines for their design. Paris designers prefer the plastic design based upon formal and symmetrical balance of informal and asymmetrical balance to the partial trans-formation design ; Rome designers are enjoy-ing rather the partial transformation using the detail and trimming than the plastic design.

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Automatic Determination of Pacing Threshold by Surface ECG Morphology (ECG 형태에 의한 자동화된 pacing 문턱 전압 결정에 관한 연구)

  • Kim, J.;Huh, W.
    • Journal of Biomedical Engineering Research
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    • v.22 no.3
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    • pp.269-273
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    • 2001
  • Proper determination of pacing threshold is important for patient safety and pacemaker longevity. In general, cardiac muscle contractions caused by pacing pulses are verified by observing the morphology of surface ECG displayed on a monitor. In this study, a method of automatic pacing threshold determination based on morphological difference between intrinsic and paced ECGs was developed. First, characteristics of intrinsic ECG and paced ECG were analyzed in time and frequency domain and a proper discrimination parameter was extracted. Then, the automatic capture verification method based on the parameter was developed and applied to 23 pacemaker patients. The selected parameter was the area of ventricular depolarization wave during 80ms after pacing stimulus. It was found that the method was reliable and effective in identifying paced ECG and, thereby, determing a proper pacing threshold.

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A Study on Statistical Classification of Wear Debris Morphology

  • Cho, Unchung
    • KSTLE International Journal
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    • v.2 no.1
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    • pp.35-39
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    • 2001
  • In this paper, statistical approach is undertaken to investigate the classification of wear debris which is the key function of objective assessment of wear debris morphology. Wear tests are run to produce various kinds of wear debris. The images of wear debris from wear tests are captured with image acquisition equipment. By thresholding, two-dimensional binary images of wear debris are made and, then, morphological parameters are used to quantify the images of debris. Parametric and nonparametric discriminant method are employed to classify wear debris into predefined wear conditions. It is demonstrated that classification accuracy of parametric and nonparametric discriminant method is similar. The selected use of morphological parameters by stepwise discriminant analysis can generally improve the classification accuracy of parametric and nonparametric discriminant method.

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The wavelet Image Coding Using Band Adaptive Quantization and the Significant Cluster Extraction (대역 적응 양자화와 중요 클러스터 추출을 이용한 웨이브릿 영상 부호화)

  • Ryu Kwon-yeol
    • Journal of the Korea Institute of Information and Communication Engineering
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    • v.9 no.6
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    • pp.1234-1240
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    • 2005
  • In this paper, I propose the wavelet image coding method using band adaptive quantization and the significant cluster extraction. The proposed method can reduce to unnecessary additional seed data which create on conventional MRWD coding, because it eliminate cluster which smaller than structuring element by using morphology. And it make fast coding possible, because it is reduced to computational complexity by using band adaptive quantization. Consequently, the proposed method reduces computational complexity with $20\%{\~}33.3\%$ according to bit rate in quantization process.

A New Model for the Analysis of Non-spherical Particle Growth Using the Sectional Method (구간해석방법을 통한 새로운 비구형 입자성장해석 모델)

  • Jeong, Jae-In;Choi, Man-Soo
    • Proceedings of the KSME Conference
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    • 2000.04b
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    • pp.416-421
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    • 2000
  • We have developed a simple model for describing the non-spherical particle growth phenomena using modified 1-dimensional sectional method. In this model, we solve simultaneously particle volume and surface area conservation sectional equations which consider particles' irregularities. From the correlation between two conserved properties of sections, we can predict the evolution of the aggregates' morphology. We compared this model with a simple monodisperse-assumed model and more rigorous two dimensional sectional model. For the comparison, we simulated silica and titania particle formation and growth in a constant temperature reactor environment. This new model shows a good agreement with the detailed two dimensional sectional model in total number concentration, primary particle size. The present model can also successfully predict particle size distribution and morphology without costing very heavy computation load and memory needed for the analysis of two dimensional aerosol dynamics.

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Morphology Control of NTO Crystals with Various Recrystallization Techniques

  • Lee, H.Y.;K.K. Koo;Kim, K.J.;G.B. Lim;W.B. Jeong;Kim, S.H.;Kim, H.S.;Park, B.S.
    • Proceedings of the Korea Association of Crystal Growth Conference
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    • 1997.10a
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    • pp.123-127
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    • 1997
  • Various recrystallization techniques has been applied to control morphology and size of NTO(3-nitro-1, 2, 4-triazole-5-one) crystals. With cooling method, it was found that the size of NTO at aqueous solution was controlled in the range of 5 to 500 $\mu\textrm{m}$. The spherical or cubic shapes of particles were obtained by adjusting operating conditions. Hexagonal and cubic shaped crystals of NTO were also obtained by sonication and evaporative method using aqueous solution of NTO. Their particle sizes were ranged 20 to 30 $\mu\textrm{m}$. In gas anti-solvent method with NTO/DMF and NTO/DMSO solutions, cubic type of NTO was obtained and the range of their sizes was 0.5-2$\mu\textrm{m}$.

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