• Title/Summary/Keyword: microstructure effect

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Effect of Slurry Property on Preparation of Zirconia Film in Electrophoretic Deposition (전착법에서 용액특성이 지르코니아 막형성에 미치는 영향)

  • 김상우;이병호;손용배;송휴섭
    • Journal of the Korean Ceramic Society
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    • v.36 no.9
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    • pp.991-996
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    • 1999
  • Effect of solution property on the weight varation and microstructural change of film was studied by electrophoretic deposition in order to obtain a homogeneous and dense zirconia film. As a result of weight kinetics of film which obtained in alcohol or aqueous solution having different polarity experimental data showed large deviation from theoretical ones calculated by Zhang's kinetic model. It had been shown that the weight affecting factors was largely dependent on properties other than dielectric constant and viscosity of solvent zeta potential appiled field and time. In initial stage a main factor of the drastic weight increase was the capillary drag of porous substrate. The cause of weight decrease with time in aqueous solution after 300 s was attributed to the defect of film by sagging and electrolytic reaction. The electrolyte film which prepared in alcohol solution with good wetting for substrate had better homogeneous and dense microstructure than one in aqueous solution with high surface tension.

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Effect of SiC mean particle size on mechanical properties and microstructure of $Si_{3}N_{4}/SiC$ nanocomposites (SiC 입자크기가 $Si_{3}N_{4}/SiC$ 초미립복합재료의 기계적 특성과 미세구조에 미치는 영향)

  • 황광택;김창삼;정덕수;오근호
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.6 no.3
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    • pp.392-398
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    • 1996
  • $Si_{3}N_{4}/SiC$ nanocomposites reinforced with tow different mean particle size were fabricated by hot press. Grain growth of matrix gran was inhibited by adding of SiC particles, and then number of equiaxed and fine grains were increased. The effect of grain growth inhibition was higher in the nanocomposites dispersed small size SiC. herefore fracture strength and hardness were increased, but fracture toughness was decreased in small size SiC dispersed samples.

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Analysis of Bridging Stress Effect of Polycrystalline aluminas Using Double Cantilever Beam Method (Double Cantilever Beam 방법을 이용한 다결정 알루미나의 Bridging 응력효과 해석)

  • 손기선;이선학;백성기
    • Journal of the Korean Ceramic Society
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    • v.33 no.5
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    • pp.583-589
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    • 1996
  • In this study a new analytical model which can describe the relationship between the bridging stress and microstructure has beenproposed in order to investigate the microstructural effect on the R-curve behavior in polycrystalline aluminas since the R-curve can be derived via the bridging stress function. In the currently developed model function the distribution of grain size is considered as a microstructural factor in modeling of bridging stress function and thus the bridging stress function including three constants PM, n, and Cx, can be established analytically and quantitatively. The results indicate that the n value is closely related to the grain size distribution thereby providing a reliability of the current model for the bridging stress analysis. Thus this model which explains the correlation of the bridging stress distribution and microstructual parame-ters is useful for the systematic interpretation of microfracture mechanism including the R-curve behavior in polycrystalline aluminas.

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Effect of the $SiO_2$ Addition on the Electrical and Degradation Property of Bi based ZnO Varistor (비스무스계 ZnO 바리스타의 $SiO_2$ 첨가에 따른 전기적특성 및 열화특성)

  • Heo, Jong-Cheol;Kim, Hyung-Sik;Park, Tae-Gone
    • Proceedings of the KIEE Conference
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    • 1998.07d
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    • pp.1522-1524
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    • 1998
  • Experimental results on the effect of $SiO_2$ addition to Bi based ZnO varistor show that secondary phases in microstructure and nonlinear coefficient are increased, and that leakage current is decreased with $SiO_2$ additive content. The varistor with 0.1 mol%-$SiO_2$ additive exhibits lower resistive current than other specimen at ($E_{1mA}$ x 0.6) applied voltage and temperature of $115^{\circ}C$ for 350h.

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Influence of Sulfur on the Inoculation Effect of Gray Cast Iron (회주철의 접종효과에 미치는 S의 영향)

  • Chung, Yae-Soo;Kim, In-Bae;Park, Ik-Min
    • Journal of Korea Foundry Society
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    • v.9 no.3
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    • pp.221-227
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    • 1989
  • The effect of sulfur content and inoculant on solidification microstructure and mechanical properties of gray cast iron have been investigated. The main results obtained are as follows, 1. In the FeSi3Ca1Ba inoculated irons, with the variation of sulfur content, low sulfur levels (${\sim}0.03%$) yield low chill depth, high tensile strength, good wear resistance and type A graphite with a pearlite matrix. High sulfur levels( >0.08%) provide high chill depth, low mechanical proper ties and type D graphite with small amount ferrite. 2. In case of inoculant variation with normal FeSi, FeSi3Ca1Ba, 30CaSi and uninoculation at 0.03%S level, lower chill depth and higher tensile strength was obtained in the order ; 30CaSi, FeSi3Ca1Ba normal FeSi, uninoculation.

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The Effect of Austempering Treatment on Microstructure and Mechanical Properties of NICI and DCI for Rolls Used in Hot Rolling Mill (오스템퍼링 처리가 열간압연롤용 NICI재 및 DCI재의 미세조직 및 기계적 성질에 미치는 영향)

  • Kim, Jae-Jin;Oh, Seok-Jung;Yoo, Kook-Jong;Andy, Tirta;Baek, Eung-Ryul
    • Journal of Korea Foundry Society
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    • v.29 no.6
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    • pp.251-256
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    • 2009
  • The effect of austempering treatment on mechanical properties of nodular indefinite chilled iron(NICI) and ductile cast iron(DCI) was investigated. In microstructural observation, matrix phase(pearlite and ferrite) was changed to ausferrite after austempering treatment both DCI and NICI. In case of NICI, decomposition of cementite($Fe_3C$) during austempering treatment was induced. After austempering treatment, mechanical properties such as hardness, tensile strength and impact toughness was improved in NICI and DCI. The wear resistance is slightly decreased because of decomposition of cementite during austempering treatment in NICI but impact toughness and strength is dramatically increased.

Polysilicon anti-sticking structure by grain etching technique (결정립 식각 기술을 이용한 다결정 실리콘 부착 방지 구조)

  • 이영주;박명규;전국진
    • Journal of the Korean Institute of Telematics and Electronics D
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    • v.35D no.2
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    • pp.60-69
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    • 1998
  • Polysilicon surface mdoification tecnique is developed to reduce the sticking of microstructures fabricated by micromachining. Modified anti-sticking grain holes are simply formed by two-step dry eth without additional photolithography nor deposition of thin films. Both process-induced sticking and in-use sticking are successfully reduced more than two times by adopting grain holed polysilicon substrate. A sticking model for cantilever beam is derived. This model includes bending moment stems from stress gradient along the thickness directionof structural polysilicon. Because the surface tension of rinse liquid and the surface energy of the solids to be stuk tend to decrease in recently developed anti-sticking techniques, the effect of stress gradient will play an important role to analyze the sticking phenomena. Effect of the temperature during post-release rinse and dry is modelled and verified experimentally. Based on developed anti-sticking polysilicon structure and the sticking model, sticking of microstructure, fabricated by simple wet process including sacrificial layer etch and rinse with deionized water without special equimpment for post-release rinse and dry was alleviated more than 3.5 times.

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The Estimate of Abrasion resistance of High chromium white cast irons by Dry sand/rubber wheel tester (토사마모실험을 통한 고크롬철계 주조합금의 내마모성 평가)

  • 김상호;김기열;이범주;조정환;박채규
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 1998.10a
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    • pp.38-48
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    • 1998
  • To apply the high chromium white cast irons for sliding parts of construction equipments, the wear characteristics of these alloys which have three kinds of microstructure(hypoeutectic, near-eutectic, hypereutectic) were investigated by dry sand/rubber wheel tester. Also, the effect of heat treatment was investigated for the same alloys. As result of the test, heat treatment have no effect on the wear characteristics. And, hypereutectic composition alloy has the highest wear resistance against SiO$_2$. Also after test, cracking was observed in eutectic and primary carbides of all materials tested. This phenomenon was important factor in the wear resistance.

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A Study on the Tribolayer using Focused Ion Beam (FIB) (FIB를 이용한 트라이보층에 대한 연구)

  • Kim, Hong-Jin
    • Tribology and Lubricants
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    • v.26 no.2
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    • pp.122-128
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    • 2010
  • Focused Ion Beam (FIB) has been used for site-specific TEM sample preparation and small scale fabrication. Moreover, analysis on the surface microstructure and phase distribution is possible by ion channeling contrast of FIB with high resolution. This paper describes FIB applications and deformed surface structure induced by sliding. The effect of FIB process on the surface damage was explored as well. The sliding experiments were conducted using high purity aluminum and OFHC(Oxygen-Free High Conductivity) copper. The counterpart material was steel. Pin-on-disk, Rotational Barrel Gas Gun and Explosively Driven Friction Tester were used for the sliding experiments in order to investigate the velocity effect on the microstructural change. From the FIB analysis, it is revealed that ion channeling contrast of FIB has better resolution than SEM and the tribolayer is composed of nanocrystalline structures. And the thickness of tribolayer was constant regardless of sliding velocities.

Effect of Initial Microstructures on Hot Formability of Ti-10V-2Fe-3Al Alloy (Ti-10V-2Fe-3Al 합금의 열간성형성에 미치는 초기미세조직의 영향)

  • 신동혁
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 1999.03b
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    • pp.153.2-158
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    • 1999
  • A study has been made to investigate how the fomability of Ti-10V-2Fe-3Al alloy is related to the initial microstructure and process variables such as temperature and strain rate. It has been found that the deformation resistance at high temperature is increased with the increase in the thickness of grain boundary a (GB)a and/or acicular a phase and however the effect of a morphology on the hot formability is considered insignificant due to the breakage of GB a and/or acicular a into several equiaxed a particles

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