• Title/Summary/Keyword: microstructure effect

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The effect of annealing temperature and solvent on the fabrication of YBCO thin films by MOD-TFA process (MOD-TFA 공정으로 YBCO 박막제조 시 열처리 온도와 용매의 영향)

  • 허순영;유재무;김영국;고재웅;이동철
    • Progress in Superconductivity
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    • v.5 no.1
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    • pp.84-87
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    • 2003
  • $YBa_2$$Cu_3$$O_{7-x}$ (YBCO) thin films were fabricated by MOD-TFA process via dip-coating method on LaAlO$_3$, (LAO) single crystalline substrates. In this study, we investigated effect of annealing temperature and solvent on the microstructure and texture of YBCO thin films. The precursor films were annealed at various temperature to improve surface morphologies and phase purities. It was shown that the films annealed at relatively lower and higher temperature exhibit low phase purity and crystallinity. The effect of various solvents on surface morphologies and second phase has been investigated.

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Effect of Internal Stress due to Plastic Costraint On Fracture Ductility of Dual Phase Steel (複合組織鋼 의 破斷延性 에 미치는 塑性拘束 에 의한 內部應力 의 영향)

  • 김정규
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.7 no.2
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    • pp.123-129
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    • 1983
  • The effect of the micro-internal stress which is induced in the ferrite grain by plastic constraint, on fracture behavior was investigated. The specimen used has combined microstructure with matrix of ferrite encapsulated by second phase of martensite. The micro-internal stress in the ferrite grain was estimated using a simple mechanical model, and its effect on micro and macro fracture behaviors was discussed. The results obtained are summarized as follows; The micro-internal stress promotes the formation of cleavage cracks in the ferrite during deformation. Consequently, it was concluded that the internal stress is one of the significant factors which cause the fracture ductility to decrease.

Effect of $Al_2O_3$ and $Y_2O_3$ on Machining of Silicon itride (알루미나와 이트리아가 질화규소의 가공성에 미치는 영향)

  • 이수완;장태석;엄호성
    • Journal of the Korean Ceramic Society
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    • v.33 no.3
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    • pp.269-276
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    • 1996
  • The effect of sintering aids on the sinterability for silcion nitride has been studied by hundreds workers. However the effect of sintering aids on the machinability as the own trobles which is the major barrier for the field applications of the ceramic components has not been fully studied. in this study the contents of Al2O3 and Y2O3 in silicon nitride were varied from 0 to 8 wt% respectively. The physical and mechanical properties of the silcion nitride were measured. The optimal microstructure of silicon nitride balls with the excellent machinability by adding with various contents of sintering aids was studied by MGF(magnetic-fluid grinding)technique. An attempt to figure out how the mechanical properties influence the machinability of silicon-nitride ball was made.

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Effect of Post Heat Treatment on Wear Characteristics of Thermally Sprayed Co-based Self-flux Alloy Coating (코발트기 자융성합금 코팅의 마모특성에 미치는 후열처리의 영향)

  • Lee, Jae-Hong;Kim, Yeong-Sik
    • Journal of Power System Engineering
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    • v.18 no.1
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    • pp.106-111
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    • 2014
  • This article describes effect of post heat treatment on wear characteristics of thermally sprayed Co-based self-flux alloy coating. Co-based self-flux alloy coatings were deposited on steel substrates using a flame spray process. Post heat treatments were carried out at 800, 900, 1000 and $1100^{\circ}C$ for 30min in a vacuum chamber. For analysis of effect of post heat treatment on mechanical properties, wear test and hardness test were performed for post heat-treated coating specimen. Microstructures of heat treated coating layer and wear track were examined using SEM and EDS. Wear loss and hardness became lower with increasing post heat treatment temperature.

The Effect of Additives on Twining in ZnO Varistors

  • Han, Se-Won;Kang, Hyung-Boo
    • The Korean Journal of Ceramics
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    • v.4 no.3
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    • pp.207-212
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    • 1998
  • By comparison of the experimental results in two systems of ZnO varistors, it's appear that Sb2O3 is the indispensable element for twining in ZnO varistors and the Zn7Sb2O12 spinel acts as the nucleus to form twins. Al2O3 is not the origin of twining in ZnO varistor, but it was found that Al2O3 could strengthen the twining and form a deformation twining by ZnAl2O4 dragging and pinning effect. The inhibition ratios of grain and nonuniformity of two systems ZnO varistors increase with the increase of Al2O3 content. The twins affect the inhibition of grain growth, the mechanism could be explained follow as: twins increase the mobility viscosity of ZrO grain and grain boundary, and drag ZrO grain and liquid grain boundary during the sintering, then the grain growth is inhibited and the microstructure becomes more uniform.

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Photothermal and Photochemical Investigation on Laser Ablation of the Polyimide by 355nm UV Laser Processing (355nm UV 레이저 가공에 의한 폴리이미드의 광화학적 및 광열적 어블레이션에 관한 연구)

  • Oh, Jae-Yong;Shin, Bo-Sung
    • Journal of the Korean Society for Precision Engineering
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    • v.24 no.4 s.193
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    • pp.147-152
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    • 2007
  • UV laser ablation of polyimide is a combination of photochemical and photothermal mechanism. Photochemical mechanism is that molecular bonds are broken by photon energy and photothermal is evaporation and melt expulsion. When the laser processing, the etching depth needs to be calculated for prediction of processing result. In this paper, in order to predict the laser etching depth of polyimide by UV laser with the wavelength of 355nm, the theoretical model which includes both the photothermal and the photochemical effect was introduced. The model parameters were obtained by comparing with experimental results. The 3rd harmonic $Nd:YVO_4$ laser system was used in the experiment. From these experimental and theoretical results, the laser ablation of a polyimide was verified to achieve the highest quality microstructure.

An Effect of Blending Materials on the Strength Characteristics of High Strength Cement Composite (고강도 시멘트 복합체의 강도특성에 미치는 혼합재료의 영향)

  • 최일규;김정환;한기성
    • Journal of the Korean Ceramic Society
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    • v.31 no.3
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    • pp.330-336
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    • 1994
  • High strength cement composites (W/C=0.1) were prepared by using various blending materials such as SiC whisker and white carbon (hydrated silica: SiO2·nH2O). The effect of various blending materials on the microstructure and strength of the hardened cement paste were investigated in the view of fracture mechanics. The plain specimen showed 101 MPa of flexural strength, 81 GPa of Young's modulus and 1.32 MPam1/2 of fracture toughness. When the blending materials were added to the composites, their values were enhanced to about 110∼138 MPa, 95∼146 GPa and 1.32∼1.87MPam1/2 respectively. The improvement of the mechanical strength for the hardened cement paste may be due to the removal of macropores, the reduction of total porosity, pozzolanic reaction and the increase of various fracture toughening effect.

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THE EFFECT OF MICRO/NANOSCALE STRUCTURES ON CHF ENHANCEMENT

  • Ahn, Ho-Seon;Kim, Moo-Hwan
    • Nuclear Engineering and Technology
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    • v.43 no.3
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    • pp.205-216
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    • 2011
  • Recently, many research studies have investigated the enormous critical heat flux (CHF) enhancement caused by nanofluids during pool boiling and flow boiling. One of the main reasons for this enhancement is nanoparticle deposition on the heated surface. However, in real applications, nanofluids create many problems when used as working fluids because of sedimentation and aggregation. Therefore, artificial surfaces on silicon and metal have been developed to create an effect similar to that of nanoparticle deposition. These modified surfaces have proved capable of greatly increasing the CHF during pool boiling, and good results have also been observed during flow boiling. In this study, we demonstrate that the wetting ability of a surface, i.e., wettability, and the liquid spreading ability (hydrophilic surface property), are key parameters for increasing the CHF during both pool and flow boiling. We also demonstrate that when the fuel surface in nuclear power plants is modified in a similar manner, it has the same effect, producing a large CHF enhancement.

Electromagnetic Properties of Nano Composite Conductor (나노 복합전도체의 전기자기적 특성 연구)

  • Lee, Sang-Heon
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.29 no.2
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    • pp.106-109
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    • 2016
  • The YBaCuO superconducting bulks were prepared by the thermal diffusion process involving the peritectic reaction to investigate the effect on microstructure and superconductivity. All the diffused YBaCuO could be successively separated from superconducting 123 phase by applying the thermal diffusion process. Electromagnetic properties of treated and untreated YBaCuO superconductor were evaluated to investigate the pinning effect. It was confirmed experimentally that a large amount of magnetic flux was trapped in the thermal treated superconducting bulk than that in the untreated one, indicating that the pinning centers of magnetic flux are related closely to the occurrence mechanism of the magnetic effect.

The Effect of Cr and Mo Additions on the Improvement in Microstructural Homogeneity and Mechanical Properties of Ni-containing P/M Steels

  • Wu, Ming-Wei;Hwang, Kuen-Shyang;Huang, Hung-Shang
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.931-932
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    • 2006
  • The microstructures of Ni-containing P/M steels produced by admixed powders or diffusion alloyed powders are usually heterogeneous. To improve the microstructure homogeneity, the effects of Mo and Cr additions in the prealloyed powder form were examined. The results showed that the microstructural homogeneity was improved and superior mechanical properties were achieved with increases in the alloy content, particularly for the Cr. Such a beneficial effect was attained due to the reduction of the repelling effect between Ni and C, as was demonstrated through thermodynamic analysis using the Thermo-Calc software.

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