• Title/Summary/Keyword: microstructure effect

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The Effect of Uni-nanoadditive Manufactured Using RF Plasma Processing on Core-shell Structure in MLCC

  • Song, Soon-Mo;Kim, Hyo-Sub;Park, Kum-Jin;Sohn, Sung-Bum;Kim, Young-Tae;Hur, Kang-Heon
    • Journal of the Korean Ceramic Society
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    • v.46 no.2
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    • pp.131-136
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    • 2009
  • Radio frequency (RF) plasma treatment is studied for the size reduction and the spheroidization of coarse particles to change them into nano-sized powders of spherical shape in MLCC fields. The uni-nanoadditives manufactured by RF plasma processing for high dispersion have been investigated for the effect on core-shell structure in dielectrics of MLCC. Microstructures have been characterized using scanning electron microscope (SEM), transmission electron microscope (TEM) and Electron Probe Micro Analyzer (EPMA). We compared the distribution of core-shell grains between specimens manufactured using uni-nanoadditive and using mixed additive. In addition, the uniformity of rare earth elements in the core-shell structured grains was analyzed. It was shown, from TEM observations, that the sintered specimen manufactured using uni-nanoadditives had more dense small grains with well-developed core-shell structure than the specimen using mixed additives, which had a homogeneous microstructure without abnormal grain growth and shows broad temperature coefficient of capacitance (TCC) curves in all temperature ranges because of well dispersed additives.

Effect Boron and Silicon on Various Properties of Dental Cobalt-Chromium Alloys (치과용 Co-Cr 합금의 제성질에 미치는 Boron과 Silicon의 영향)

  • Jung, Jong-Hyun
    • Journal of Technologic Dentistry
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    • v.14 no.1
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    • pp.119-132
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    • 1992
  • This paper aims to investigate the effect of B and Si upon the mechanical properties, microstructure and corrosion resistance of Co-Cr base alloy. Ten groups of alloy ingot ingot with various contents of B and Si were remelted by high frequency electrical induction furnace and cast into tensile specimen of ADA Specification No. 14 Tensile and hardness test were carried out by Amsler and Rockwell hardness tester(R-30N), respectively. The microstructures of specimen were observed by SEM. The results obtained are summarized as follows : 1. As B content is increased, tensile strength, yield strength and Rockwell hardness number(R-30N) are also increased significantly, while the elongation is decreased significantly. 2. As Si contect os increased, no significant chang in tensile strength is noticed, yield strength is slightly decreased, but Rockwell hardness number(R-30N) is moderately in creased, Elongation marks maxium value with 1% Si content while with more than 1% Si it is decreased. 3. As B content is increased corrosion resistance is decreased and is at best with 1.5% B content. Corrosion resistance is increased with the increase of Si content and the alloys with Si over 3.0% showed corrosion resistance. 4. As B content increased, precipitates are increased in number at grain boundaries. The grain size tends to become coarse with the increase of Si content. 5. Co rich-Cr alloy is present through matrix whereas at the grain boundaries Cr base precipitates are primarily formed.

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Effect of VC Addition on the Microstructure & Mechanical Properties of Ti(CN)-based Cermet (VC 첨가가 Ti(CN)계 써메트의 미세구조 및 기계적 성질에 미치는 영향)

  • 안성용;강신후
    • Journal of the Korean Ceramic Society
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    • v.35 no.12
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    • pp.1316-1322
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    • 1998
  • The amount of VC and C/N ratio in Ti(CN) was varied to investigate the effect of VC addition on the mi-crostructural change in Ti(CN)-Ni system. As the amount of VC addition increases in Ti(C0.7N0.3)-20Ni sys-tem a complete solid solution was observed in Ti(C0.7N0.3)-20Ni-25VC system. It implies that the ratio of the dissolution rates of Ti(C0.7N0.3)to that of VC is nearly 2:1 at the sintering conditions used in this study. It was found from the experiments that the system composed of the Ti(C0.7N0.3) phase exhibits a rimless structure and relatively small amount of solid solution. That is among Ti(C0.7N0.3) phase exhibits a rimless structure and relatively small amount of solid solution. This is among Ti(C1-xNx) phases the dissolution rate of Ti(C0.3N0.7) is the lowest. Also fracture toughness(KIC) of the cermet was measured by indentation method. Attentions were paid to crack propagation path to look for a dominant fracture mode and to cor-relate it with fracture toughness values. The fracture toughness was relatively high with the addition of VC content. But the addition of a large VC content reduced the overall toughness of the cermet. This result is explained with the difference in fracture mode.

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Effect of the Sintering Temperature on Electrical Properties of Porous Barium-strontium Titanate Ceramics

  • Kim, Jun-Gyu;Sim, Jae-Hwang;Cho, Won-Seung
    • Journal of the Korean Ceramic Society
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    • v.40 no.1
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    • pp.5-10
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    • 2003
  • Porous barium-strontium titanate ceramics were fabricated by adding corn- or potato-starch (are referred to as starch). The effect of sintering temperature on the microstructure and electrical properties of the porous ceramics was investigated. The room-temperature electrical resistivity of the barium-strontium titanate ceramics decreased with sintering temperature. The porosity and pore size were decreased and the grain size was increased with increasing the sintering temperature. The porosity and grain size of the barium-strontium titanate ceramics with corn-starch sintered at 1300 and 1450$^{\circ}C$ were 28.5, 22.6% and 3.2, 6.2 $\mu\textrm{m}$, respectively. The average pore sizes of the barium-strontium titanate ceramics with corn-starch sintered at 1300, 1400 and 1450$^{\circ}C$ were 0.5, 0.3 and 0.2 $\mu\textrm{m}$, respectively. The decrease in the room-temperature resistivity with increasing sintering temperature is attributed mainly due to the increase of grain size and the decrease of the electrical barrier height of grain boundaries as well as the partial decrease of porosity.

The Effect of Particle Size Distribution on the Physical and Optical Properties of Cenosphere (세노스피어(Cenosphere)의 입도 분포에 따른 물리적 특성 및 광학적 특성 평가)

  • Lee, Won-Jun;Hwang, Hae-Jin;Han, Kyu-Sung;Hwnag, Kwang-Taek;Cho, Woo-Suk;Kim, Jin-Ho
    • Korean Journal of Materials Research
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    • v.27 no.7
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    • pp.353-358
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    • 2017
  • Recycled cenosphere, which is a hollow shaped particle from fly ash, has become attractive as a building material due to its light weight and excellent heat insulation and soundproof properties. In this paper, we investigated the effect of cenosphere size on the physical and optical properties. High brightness of cenosphere as raw material is required for a wide range of ceramics applications, particularly in fields of building materials and industrial ceramic tiles. Cenospheres were sorted by particle size; the microstructure was analyzed according to the cenosphere size distribution. Cenospheres were generally composed of quartz, mullite, and amorphous phase. Colour measurement corresponding to chemical composition revealed that the contents of iron oxide and carbon in the cenospheres were the major factors determining the brightness of the cenospheres.

Influence on properties of base metal after elimination of lifting-lug member in a dissimilar welding between steel base and steel lifting lug

  • Park, Jeongung;An, Gyubaek;Lee, Haewoo
    • International Journal of Naval Architecture and Ocean Engineering
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    • v.11 no.2
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    • pp.858-864
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    • 2019
  • The increasing demands of lifting lugs can be attributed to the rapid advancement of shipbuilding and offshore-structure production technologies and an exponential increase in the size of the block units of ship structures. Therefore, to ensure safety during the transportation and turnover of large blocks, it is important to determine the structural integrity and position of lifting lugs. However, because the manufacturing cost and availability of lugs are important considerations, low cost and easily obtainable steel compositions of grades different from those of the blocks are often used as alternatives. The purpose of this study is to investigate the effect of a lifting-lug metal on the physical properties of a base metal in a dissimilar welding between the base metal and lifting lug. The effect was evaluated by observing the metal microstructures and determining the hardness and dilution values on the cross-sectional surface of the lifting lug. According to the results of the metal microstructures, impact, hardness, and emission spectrochemical analysis at the surface from where the lug was removed confirmed that the chemical composition of the lifting-lug metal did not influence the physical properties of the base metal.

The Effect of grain size on the damping capacity of Fe-26Mn-2Al alloy (Fe-26Mn-2Al 합금의 진동 감쇠능에 미치는 결정립 크기의 영향)

  • Kang, C.Y.;Eom, J.H.;Kim, H.J.;Sung, J.H.
    • Journal of Power System Engineering
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    • v.11 no.1
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    • pp.115-120
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    • 2007
  • The effect of grain size on the damping capacity of Fe-26Mn-2Al alloy studied in this paper has been investigated after changing the microstructure by cold rolling and changing grain size. Micro structures in Fe-26Mn-2Al at room temperature consist of a large quantity of austenite and a small quantity of ${\varepsilon}\;and\;{\alpha}'$ martensite. And ${\varepsilon}\;and\;{\alpha}'$ martensite was increased by increasing the degree of cold rolling. The content of deformation induced martensite was increased with increasing the degree of cold rolling. Damping capacity was linearly increased with increasing ${\varepsilon}$ martensite content, which suggests that stacking faults and ${\varepsilon}$ martensite variant boundaries are the principle damping sources. With increasing the grain size in Fe-26Mn-2Al alloy, the damping capacity was increased due to increasing the volume fraction of ${\varepsilon}$ martensite by decrement in stability of austenite phase. With decreasing the grain size, the content of deformation induced martensite was decreased and the damping capacity was decreased.

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Effect of Deposition Parameters on the Properties of Pyrolytic Carbon Deposited by Fluidized-Bed Chemical Vapor Deposition (유동층 화학증착법을 이용하여 증착한 열분해 탄소의 특성에 미치는 증착조건의 영향)

  • Park, Jeong-Nam;Kim, Weon-Ju;Park, Jong-Hoon;Cho, Moon-Sung;Lee, Chae-Hyun;Park, Ji-Yeon
    • Korean Journal of Materials Research
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    • v.18 no.8
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    • pp.406-410
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    • 2008
  • The properties of pyrolytic carbon (PyC) deposited from $C_2H_2$ and a mixture of $C_2H_2/C_3H_6$ on $ZrO_2$ particles in a fluidized bed reactor were studied by adjusting the deposition temperature, reactant concentration, and the total gas flow rate. The effect of the deposition parameters on the properties of PyC was investigated by analyzing the microstructure and density change. The density could be varied from $1.0\;g/cm^3$ to $2.2\;g/cm^3$ by controlling the deposition parameters. The density decreased and the deposition rate increased as the deposition temperature and reactant concentration increased. The PyC density was largely dependent on the deposition rate irrespective of the type of the reactant gas used.

The Effect of Sputtering Conditions on Magnetic Properties of CoCrMo/Cr Magnetic Thin Film (CoCrMo/Cr 자성박막의 제조조건이 자기적성질에 미치는 영향)

  • 박정용;남인탁;홍양기
    • Journal of the Korean Magnetics Society
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    • v.3 no.4
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    • pp.320-324
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    • 1993
  • The effect of sputtering conditions on magnetic properties of CoCrMo/Cr magnetic thin film was investigated. Substrate temperature were controlled from R. T to $250^{\circ}C$. The thickness changes of Cr underlayer and CoCrMo magnetic layer were in the range of $1000-2500\AA$ and $300-800\AA$, respectively. Grain size was found to be decreased with increasing magnetic layer thickness(from $500\AA$ to $800\AA$). CoCrMo magnetic layer microstructure showed relatively small dependence on Cr underlayer thickness, substrate temperature. Coercivity increased with increasing Cr underlayer, magnetic layer thickness and substrate temperature. CoCrMo/Cr thin film showed a coercivity of 880 Oe in $700\AA$ magnetic layer thickness and $1000\AA$ Cr underalyer thickness.

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Study on the Effect of Induction Heating with Alloying Elements for the Pre-Heat Treated Steel of 100kgf/$mm^2$ Tensile Strength (100Kgf/$mm^2$급 선조질강의 합금원소에 따른 유도가열효과에 관한 연구)

  • Park, J.T.;Ahn, S.T.;Kwon, D.H.;Seo, J.H.;Kang, N.H.;Youn, D.J.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2009.05a
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    • pp.40-43
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    • 2009
  • This study is for investigating the effect of induction heating with various alloy elements to manufacture the pre-heat treated steels of 100kgf/$mm^2$ for cold heading. For four kinds of steels, the condition of induction heating (especially, induction tempering) were observed, and their microstructure and tensile and compressive properties were investigated. The middle carbon steel and the low carbon Cr-Mo steel are needed the higher Grange-Baughman tempering parameter than that of the low carbon Cr steel to obtain 100kgf/$mm^2$ tensile strength. For accomplishing the pre-heat treated steel of 100kgf/$mm^2$ tensile strength having advanced cold heading. It is needed that the pre-heat treated steel is manufactured by induction quenching and tempering with the low carbon alloy steel to have the high ratio of ferrite and the fine globular cementite simultaneously.

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