• Title/Summary/Keyword: microstructure effect

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Effect of Al-5Ti-B on the Microstructure of Rheology Material (Al-5Ti-B가 레오로지 소재의 미세조직에 미치는 영향)

  • Yang Z.;Seo P. K.;Kang C. G.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2005.05a
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    • pp.299-302
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    • 2005
  • Semisolid A356 slurries were prepared by electromagnetic stirring casting and by inoculation of Al-5Ti-B master alloy. As stirring time and addition of Al-5Ti-B are different, the grain size of the primary phase is different. Through the experiment of rheocast in a Buhler horizontal die casting machine, it was found that the finer the equiaxed primary dendrites, the smoother the die filling and better cast quality. Small equiaxed primary dendrite also results in less liquid segregation on the surface.

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Effect of various cold rolling process on the evolution of texture and recrystallized grain size in AA 5052 sheet (AA 5052 판재의 집합조직 발달과 결정립 크기에 미치는 다양한 냉간압연 공정의 영향)

  • Lee, J.H.;Nah, J.J.;Huh, M.Y.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2008.05a
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    • pp.408-410
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    • 2008
  • The evolution of texture and microstructure during recrystallization was tracked after different cold rolling of aluminum sheets. Texture of the sheet center were differentiated by different strain states due to prior deformation. The evolution of recrystallization texture was studied with the amount of shear applied during cold rolling. The final grain size after recrystallization annealing was varied due to the effective strain during deformation.

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Magnetic Pulsed Compaction of nanostructured Al-Fe-Cr-Ti Powder and wear properties (Al-Fe-Cr-Ti 나노결정 합금분말의 자기펄스 성형 및 마모 특성)

  • Kim, Jun-Ho;Hong, Soon-Jik
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2008.05a
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    • pp.528-530
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    • 2008
  • The effect of consolidation temperature on the microstructure, density and mechanical properties (especially, wear property) of $Al_{92.5}-Fe_{2.5}-Cr_{2.5}-Ti_{2.5}$ alloy fabricated by gas atomization and magnetic pulsed compaction was investigated. All consolidated alloys consisted of homogeneously distributed fine-grained fcc-Al matrix and intermetallic compounds. Relative higher mechanical properties in the MPCed specimen were attributed to the retention of the nanostructure in consolidated bulk without cracks. The as consolidated bulk by magnetic pulsed compaction showed the enhanced wear properties than that of a general consolidation process. In addition, the wear mechanism and fracture mode of MPCed bulk was discussed.

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Nonequilibrium Heat Transfer Characteristics During Ultrafast Pulse Laser Heating of a Silicon Microstructure

  • Lee Seong Hyuk
    • Journal of Mechanical Science and Technology
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    • v.19 no.6
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    • pp.1378-1389
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    • 2005
  • This work provides the fundamental knowledge of energy transport characteristics during very short-pulse laser heating of semiconductors from a microscopic viewpoint. Based on the self-consistent hydrodynamic equations, in-situ interactions between carriers, optical phonons, and acoustic phonons are simulated to figure out energy transport mechanism during ultrafast pulse laser heating of a silicon substrate through the detailed information on the time and spatial evolutions of each temperature for carriers, longitudinal optical (LO) phonons, acoustic phonons. It is found that nonequilibrium between LO phonons and acoustic phonons should be considered for ultrafast pulse laser heating problem, two-peak structures become apparently present for the subpicosecond pulses because of the Auger heating. A substantial increase in carrier temperature is observed for lasers with a few picosecond pulse duration, whereas the temperature rise of acoustic and phonon temperatures is relatively small with decreasing laser pulse widths. A slight lagging behavior is observed due to the differences in relaxation times and heat capacities between two different phonons. Moreover, the laser fluence has a significant effect on the decaying rate of the Auger recombination.

Effect of Heattreatment condition on structure and properties of TiAl alloys (열처리 조건에 따른 TiAl화합물의 미세조직과 기계적 성질에 관하여)

  • Park, J.J.;Lee, C.H.;Choe, J.I.
    • Journal of the Korean Society for Heat Treatment
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    • v.8 no.1
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    • pp.84-88
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    • 1995
  • Various heat-treatments were conducted to Ti-48.1at%Al and Ti-48.3at%Al-1.2at%Mn alloys casted by plasma arc melting system. Mechanical properties, microstructure and high temperature oxidizing behaviors of as-casted and heat-treatment alloys were investigated. Ti-48.1Al and Ti-48.3Al-1.2Mn alloys were decreased in strength according to increased of heattreatment temperature. Oxidizing weight gain of Ti-48.1Al alloy which conducted at $1273^{\circ}K$ was linearly increased. In case of adding Mn to alloy, there was no rapid increase of oxidizing weight gain during early time.

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Shape Control of Automotive Flexible Plate in Press Quenching (프레스 퀜칭 공정에 의한 자동차 Flexible Plate의 형상 제어 연구)

  • Park, I.H.;Jeong, W.C.
    • Journal of the Korean Society for Heat Treatment
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    • v.21 no.4
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    • pp.189-198
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    • 2008
  • The production of automotive chassis parts requiring both high hardness and good shape-holdability is better realized by using press quenching technology, comprising the austenitizaton and the subsequent press quenching in a specially designed stamping tool. The effect of press quenching mold shape on the hardness distribution, bending height, and degree of planeness of automotive flexible plate during press quenching and tempering has been investigated. The preferable shape of the projections of punch and die in contact with the flexible plate was close to oval to improve the flow of cooling oil, leading to the higher hardness. The press quenching mold with three separate parts was more effective to control the dimensional change due to thermal deformation during press quenching. Some decrease in the bending height during tempering may be related to some recovery of the residual stress at $400^{\circ}C$.

The effect of pulse current electrolysis on the composition and themicrostructure of Tin-Zinc electrodeposits (주석-아연 합금도금층의 조성 및 조직에 미치는 파형전류전해의 영향)

  • 예길촌;박성진;김대영
    • Journal of Surface Science and Engineering
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    • v.34 no.4
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    • pp.303-312
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    • 2001
  • Composition and microstructure of the tin-zinc alloys electroplated in gluconate bath were studied according to pulse current parameters. The cathode current efficiency increased with both the mean current density and the off-time decrease. Zinc content of the alloy deposits increased with increasing mean current density, while it decreased noticebly with increasing the off-time from 10-30ms to 100-150ms. The preferred orientation of the alloy deposits changed with the increase of peak current density in the sequence of (220)longrightarrow(220)+(420) or (220)+(420)+(321) mixed structure. The equiaxed grain size of the alloy increased with the increase of off-time and the decrease of mean current density.

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TiN coatings by HCD plasma enhanced reactive ion plating method (HCD플라즈마를 이용한 반응성 이온플레이팅법에 의한 TiN 코팅)

  • 서용운;황기웅
    • Journal of Surface Science and Engineering
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    • v.25 no.3
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    • pp.133-143
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    • 1992
  • Titanium nitride(TiN) films have been prepared by HCD plasma enhanced reactive ion plating. Density and temperature of the plasma generated by the HCD were investigated. It was shown that parameters such as the substrate bias voltage(0 350V) and N2 flow rate(10 180SCCM) influenced the growth, the growth, the microstructure and the color tone of the film mostly. In order to study the interface region, surface analysis by AES combined with sputter depth profiling was performed. Microhardness of the coated TiN films were measured by micro Vickers hardness tester. Also, the effect of coating parameters on composition, coating surface and fracture morphology, grain size and growth rate were examined.

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The effect of pulse parameters on the composition and the structure of Palladium-Nickel alloy electrodeposits (팔라디움-니켈 합금전착층의 조성 및 조직에 미치는 파형전류인자의 영향)

  • 예길촌;오유청
    • Journal of Surface Science and Engineering
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    • v.27 no.5
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    • pp.285-291
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    • 1994
  • The effects of pulse current parameters on the composition and the microstructure of Pd-Ni alloy electrodeposits were studied. The cathode current efficiency of p.c. electrolysis conditions decreased with increasing both mean and peak current density and was lower than those under D.C. electrolysis condition. Palladium content of Pd-Ni alloy increased with increasing both peak current density and on-time, while it decreased with increasing mean current density and duty cycle. The preferred orientation of Pd-Ni alloys changed with increasing mean current density in the sequence of (111)+(110).(100) or (110)longrightarrow(111)longrightarrow(100) or random distribution of crystal structure. The surface morphology of Pd-Ni alloy changed mainly according to the mean current density and was related to the preferred orientation.

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Effect of anodic potentials for fabricating co-doped TiO2 on the photocatalytic activity

  • Lee, Seunghyun;Han, Jae Ho;Oh, Han-Jun;Chi, Choong-Soo
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2012.05a
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    • pp.295-295
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    • 2012
  • The $TiO_2$ films were prepared in the $H_2SO_4$ solution containing $NH_4F$ at different anodic voltages, to compare the photocatalytic performances of titania for purification of waste water. The microstructure was characterized by a Field-emission scanning electron microscopy (FE-SEM) and X-ray diffractometry (XRD). Chemical bonding states and co-doped elements of F and N were analyzed using surface X-ray photoelectron spectroscopy (XPS). The photocatalytic activity of the co-doped $TiO_2$ films was analyzed by the degradation of aniline blue solution. From the result of diffuse reflectance absorption spectroscopy(DRS), it is indicated that the absorption edge of the F-N-codoped $TiO_2$ films shifted toward visible light area, and the photocatalytic reaction of $TiO_2$ was improved by doping an appropriate contents of F and N.

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