• Title/Summary/Keyword: microscopic characteristics

Search Result 672, Processing Time 0.027 seconds

Synthesis, Spectral Characterization, Electron Microscopic Study and Influence on the Thermal Stability of Phosphorus-containing Dendrimer with a 4,4'-Sulphonyldiphenol at the Core

  • Dadapeer, Echchukattula;Rasheed, Syed;Raju, Chamarthi Naga
    • Bulletin of the Korean Chemical Society
    • /
    • v.32 no.2
    • /
    • pp.498-502
    • /
    • 2011
  • The divergent synthesis of novel phosphorus-containing dendrimer with 4,4'-sulphonyldiphenol at the core has been accomplished involving simple condensation reactions using $P(O)Cl_3$, $P(S)Cl_3$, 3-amino-phenol, 3-hydroxy-benzaldehyde, and 2-butyn 1, 4-diol. The final compound was a Schiff's base macromolecule possessing 4 imine bonds, 8 acetylenic bonds and 8 OH groups at the periphery. The structures of intermediate compounds were confirmed by IR, NMR ($^1H$, $^{13}C$ and $^{31}P$), LC-Mass and C, H, N analysis. The structure of the final dendrimer (5) was confirmed by IR, NMR ($^1H$, $^{13}C$ and $^{31}P$), MALDI-TOF-MS, and C, H, N analysis. The surface morphological characteristics of the final dendrimer were understood by Scanning Electronic Microscopic study (SEM). The thermal stability of the final dendrimer was studied by TGA/DTA analysis.

Anatomical and Microscopic Studies on Acanthopanax gracilistylus, A. koreanum and A. sieboldianus (세주오가피, 섬오가피 및 당오가피의 외부형태 및 내부형태학적 연구)

  • Moon, Jung Hyun;Yook, Chang Soo;Jang, Young Pyo
    • Korean Journal of Pharmacognosy
    • /
    • v.43 no.4
    • /
    • pp.268-273
    • /
    • 2012
  • Acanthopanax species are well known medicinal plants in Korea for their adaptogenic efficacy. Regarding to the botanical classification of Acanthopanax koreanum, an indigenous species in Jeju island of Korea, it has been classified as different species of Acanthopanax genus. However, the morphological characteristics of A. koreanum are very similar with other Acanthopanax species, especially with A. gracilistylus. In order to provide further classification information among these botanically related species, microscopic and morphological studies on these Acanthopanax species were performed. In this result, it has been found that A. koreanum is similar to A. gracilistylus in terms of anatomical observation and was distinguished from A. sieboldianus by their morphological and anatomical differences.

Computer Vision System for Analysis of Geometrical Characteristics of Agricultural Products and Microscopic Particles(II) -Algorithms for Geometrical Feature Analysis- (농산물 및 미립자의 기하학적 특성 분석을 위한 컴퓨터 시각 시스템(II) -기하학적 특성 분석 알고리즘-)

  • Lee, J.W.;Noh, S.H.
    • Journal of Biosystems Engineering
    • /
    • v.17 no.2
    • /
    • pp.143-155
    • /
    • 1992
  • The aim of this study is to develop a general purpose algorithm for analyzing geometrical features of agricultural products and microscopic particles regardless of their numbers, shapes and positions with a computer vision system. Primarily, boundary informations of an image were obtained by Scan Line Coding and Scan & Chain Coding methods and then with these informations, geometrical features such as area, perimeter, lengths, widths, centroid, major and minor axes, equivalent circle diameter, number of individual objects, etc, were analyzed. The algorithms developed in this study was evaluated with test images consisting of a number of randomly generated ellipsoids or a few synthesized diagrams having different features. The result was successful in terms of accuracy.

  • PDF

Dynamic fracture instability in brittle materials: Insights from DEM simulations

  • Kou, Miaomiao;Han, Dongchen;Xiao, Congcong;Wang, Yunteng
    • Structural Engineering and Mechanics
    • /
    • v.71 no.1
    • /
    • pp.65-75
    • /
    • 2019
  • In this article, the dynamic fracture instability characteristics, including dynamic crack propagation and crack branching, in PMMA brittle solids under dynamic loading are investigated using the discrete element method (DEM) simulations. The microscopic parameters in DEM are first calibrated using the comparison with the previous experimental results not only in the field of qualitative analysis, but also in the field of quantitative analysis. The calibrating process illustrates that the selected microscopic parameters in DEM are suitable to effectively and accurately simulate dynamic fracture process in PMMA brittle solids subjected to dynamic loads. The typical dynamic fracture behaviors of solids under dynamic loading are then reproduced by DEM. Compared with the previous experimental and numerical results, the present numerical results are in good agreement with the existing ones not only in the field of qualitative analysis, but also in the field of quantitative analysis. Furthermore, effects of dynamic loading magnitude, offset distance of the initial crack and initial crack length on dynamic fracture behaviors are numerically discussed.

A Scanning Electron Microscopic Study on Korean Rhus Lacquer Coats (한국산(韓國産) 옻칠도막(漆塗膜)에 관한 주사전자현미경적(走査電子顯微鏡的) 고찰(考察))

  • Lee, Phil-Woo;Kim, Hyun-Joong
    • Journal of the Korean Wood Science and Technology
    • /
    • v.15 no.3
    • /
    • pp.24-33
    • /
    • 1987
  • This study was executed to investigate scanning electron microscopic characteristics of Korean Rhus lacquer coats. With the unrefined coat, distilled water, sodium hydroxide, acetic acid, ethyl alcohol, cold-check test, and accelerated weathering were performed after refining treatment. These treated lacquer coats were discussed through observation by scanning electron microscope and the obtained results were summarized as follows: 1. Compared with unrefined coat, the refined coat of Korean Rhus lacquer showed more even surface with regular distribution of dispression. 2. Korean Rhus lacquer coat heated at $120^{\circ}C$ for 3 hours revealed no observable difference irrespective of refining and unrefining. 3. Korean Rhus lacquer coat treated by distilled water, sodium hydroxide, acetic acid. ethyl alcohol, cold-check test. and ultraviolet radiation showed significant characteristics compared with untreated coat. Especially. large deformation and checkings were observed by cold-check test and ultraviolet radiation respectively. 4. The Korean Rhus lacquer coat radiated by ultraviolet ray showed 0.11 duller and 1.41 brighter than non-radiated coat through color difference calculator.

  • PDF

AE Characteristics on Microscopic Failure Behavior of Carbon/Epoxy Comosite Prepared by Cocure and Precure Process (Cocure/Precure 경화공정에 의해 제조된 Carbon/Epoxy 복합재료의 미시적 파손거동에 대한 AE 특성)

  • Lee, Jin-Gyeong;Lee, Jun-Hyeon;Lee, Min-Rae;Choe, Heung-Seop
    • Transactions of the Korean Society of Mechanical Engineers A
    • /
    • v.24 no.10 s.181
    • /
    • pp.2520-2528
    • /
    • 2000
  • Mechanical and physical properties of composite materials make a great difference due to their cure process condition. In order to clarify the effect of cure process condition on the microscopic damage behavior and failure mechanism of Carbon/Epoxy composites, three point bend test has been performed. For this purpose, two kinds of specimens with single adhesive and multiple adhesive layers were prepared. For single adhesive layer, four different types of specimen were used, that is, non-sanding, sanding, cocured, laminated specimens. Three different types of specimen were also used for the multiple adhesive layer, non-sanding, sanding, cocured specimens. Acoustic emission technique has also been employed to monitor the damage progresses associated with each micro-failure mechanism. The characteristics of AE parameters associated with micro-failure mechanism of each specimen were discussed.

Comparison of Overall Characteristics between an Air-Assisted Fuel Injector and a High-Pressure Swirl Injector- Part II: Microscopic Spray Characteristics (공기보조 분사기와 고압 선회식 분사기의 특성 비교 - Part II: 미시적 분무특성)

  • 장창수;최상민
    • Transactions of the Korean Society of Automotive Engineers
    • /
    • v.8 no.5
    • /
    • pp.28-35
    • /
    • 2000
  • As a second part of the comparison study, microscopic features of an air-assisted fuel injector(AAFI) and a high-pressure swirl injector (HPSI) were characterized. They consist of the internal spray structure in terms of fuel mass and drop diameter, the overall atomization performance with respect to operating parameters and the drop size distribution. Large droplets are concentrated in around the head part of a spray field of the HPSI, while in the case of the AAFI, they were distributed in the tail part. Although the AAFI showed the better atomization performance, the feasible ranges of operating parameters such as injection and ambient pressure were found to be wider in the HPSI. Drop size distribution of the AAFI sprays was more dispersed than that of the HPSI. Drop size distribution of the AAFI sprays was more dispersed than that of the HPSI. However, at the well-atomized condition, it appeared to be very uniform.

  • PDF

Comparison of Skin Condition Before and After Use of Scrub Cosmetics and Microscopic Characteristics of Microbeads (스크럽 화장품의 사용 전과 후의 피부상태 비교와 이에 첨가된 마이크로비드의 현미경적 특성)

  • Kim, Hoon;Chang, Byung-Soo
    • Journal of Convergence for Information Technology
    • /
    • v.9 no.6
    • /
    • pp.211-217
    • /
    • 2019
  • In this study, the change of skin condition was analyzed by skin analysis equipment using scrub cosmetics, and the morphological characteristics of microbead were observed by dermascope and scanning electron microscope. In the dermascope observation, during the process of cleansing, the microbeads attached to the skin existed in close contact with each other or dispersed. The skin after scrubbing was clean and smooth and the fine wrinkles between epidermal keratinocytes were reduced. In the scanning electron microscopic observation, the microbead surface did not have severe bending or rough surface. The skin moisture and oil content were higher than the scrub skin before the scrub, and there was no significant difference in the pH.

Fourteen Unrecorded Species of Agaricales Underw. (Agaricomycetes, Basidiomycota) from the Republic of Korea

  • Shinnam Yoo;Yoonhee Cho;Ji Seon Kim;Minkyeong Kim;Young Woon Lim
    • Mycobiology
    • /
    • v.50 no.4
    • /
    • pp.219-230
    • /
    • 2022
  • Agaricales species form pileate-stipitate fruiting bodies and play important roles in maintaining the terrestrial ecosystem as decomposers, symbionts, and pathogens. Approximately 23,000 Agaricales species have been known worldwide, and 937 species have been recorded in the Republic of Korea. However, most of them were identified solely based on morphological characteristics that often led to misidentifications. The specimens collected from 2018 to 2020 in the Republic of Korea were identified based on phylogenetic analysis of the internal transcribed spacer (ITS) sequences. Their identities were confirmed by microscopic characteristics. As a result, 14 Agaricales species were discovered for the first time in the Republic of Korea. They belonged to nine genera: Agaricus, Calocybe, Cortinarius, Hygrocybe, Inocybe, Lepista, Leucoagaricus, Marasmius, and Psathyrella. Detailed macroscopic and microscopic descriptions were provided to help distinguish these species. The morphological and molecular data provided in this study will serve as reliable references for the identification of Agaricales species.

Analysis of Roadside Soil Characteristics and Tire Wear Particles(TWPs) According to Traffic Volume (교통량별 가로변 토양특성 및 타이어 마모 입자(TWPs) 분석)

  • Sun Yeong Lee;Jin Hee Ju;Yong Han Yoon
    • Journal of Environmental Science International
    • /
    • v.32 no.9
    • /
    • pp.627-634
    • /
    • 2023
  • Tire wear particles(TWPs), regarded as a microplastic, is generated in significant quantities each year and exist in various spaces and have a negative impact on the surrounding environment. Particularly, roadside environments fall within the direct influence of TWPs, necessitating proactive investigation for contamination management and response. Therefore, this study aimed to investigate the soil acidity and electrical conductivity(EC) and TWPs in the roadside soil of six sites based on traffic volume. The analysis revealed that the soil in all sites exhibited subacidity, and there were no significant differences in EC. Microscopic and FT-IR analysis revealed the presence of microscopic particles in soil samples that exhibited common visual characteristics of TWPs. In the road with the highest traffic volume, 48,300 TWPs were detected per unit area. Furthermore, a proportional relationship between traffic volume and TWPs particles was established. However, influences other than traffic volume on TWPs particle count within the soil were observed. Therefore, for the management of TWPs contaminated roadside soil, a proactive response is necessary in areas with high traffic volumes. However, in order to effectively address the factors contributing to the generation and dispersion of TWPs, further research is required with a multidimensional approach.