• Title/Summary/Keyword: micro-particle

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The Statistical Hypothesis Verification to Influence of Addition of Metakaolin and Silica Fume on Compressive Strength and Chloride Ion Penetration of High Strength Concrete (메타카올린 및 실리카퓸의 혼입이 고강도 콘크리트의 압축강도와 염소이온 투과에 미치는 영향에 관한 통계적 가설검증)

  • Min, Jeong Wook
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.15 no.1
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    • pp.215-225
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    • 2011
  • Metakaolin is a dehydroxylated form of the clay mineral kaolinite. Rocks that are rich in kaolinite are known as china clay or kaolin, traditionally used in the manufacture of porcelain. The particle size of metakaolin is smaller than cement particles, but not as fine as silica fume. This paper investigates the effect of the concrete containing metakaolin as a mineral admixture on the compressive strength and resistance properties to chloride ion penetration. In this study, the experiment was carried out to investigate and analyze the influence of replacement ratio of metakaolin and micro silica fume on the compressive strength and chlorine ion penetration resistance of concrete. All levels were water/binder ratio 30%, replacement ratio of metakaolin and silica fume were 0, 5, 10, 15, 20% respectively. The compressive strength of concrete using metakaolin tends to increase, as the replacement ratio increases but the chlorine ion penetration resistance was not so as lager as silica fume concrete. Therefore, the optimum mixing ratio of metakaoline to satisfy a properties of compressive strength and chlorine ion penetration resistance was was approximately10%.

Improvement of Solubility of Atorvastatin Calcium Using Self-Microemulsion Drug Delivery System(SMEDDS) (자가미세유화를 통한 아토르바스타틴 칼슘의 난용성 개선)

  • Lee, Jun-Hee;Choi, Myoung-Kyu;Kim, Yun-Tae;Kim, Myoung-Jin;Oh, Jae-Min;Park, Jung-Soo;Mo, Jong-Hyun;Kim, Moon-Suk;Khang, Gil-Son;Lee, Hai-Bang
    • Journal of Pharmaceutical Investigation
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    • v.37 no.6
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    • pp.339-347
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    • 2007
  • SMEDDS is mixture of oils, surfactants, and cosurfactants, which are emulsified in aqueous media under conditions of gentle agitation and digestive motility that would be encountered in the gastro-intestinal(GI) tract. The main purpose of this work is to prepare self-microemulsifying drug delivery system(SMEDDS) for oral bioavailability enhancement of a poorly water soluble drug, atorvastatin calcium. Solubility of atorvastatin calcium was determined in various vehicles. Pseudo-ternary phase diagrams were constructed to identity the efficient self-emulsification region and particle size distributions of the resultant micro emulsions were determined using a laser diffraction sizer. Optimized formulations for in vitro dissolution and bioavailability assessment were $Capryol^{(R)}$ 90(50%), Tetraglycol(16%), and $Cremophor^{(R)}$ EL(32%). The release rate of atorvastatin from SMEDDS was significantly higher than the conventional tablet ($Lipitor^{(R)}$), 2-fold. Our studies illustrated the potential use of SMEDDS for the delivery of hydrophobic compounds, such as atorvastatin calcium by the oral route.

Electrical and Mechanical Properties of Inkjet-Printed Ag films (잉크젯 인쇄 Ag 배선의 전기적, 기계적 특성에 관한 연구)

  • Kim, In-Young;Song, Young-Ah;Jung, Jea-Woo
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2007.06a
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    • pp.550-550
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    • 2007
  • Inkjet printed silver films were fabricated using nano particles with the size of ~ 20 nm. We can obtain very good conducting silver films with the resistivity of $7.3\;{\mu}{\Omega}{\cdot}cm$ even though they were sintered at the very low temperature of $200^{\circ}C$. The electrical and mechanical properties of inkjet printed silver lines were measured with the sintering time and analyzed with the micro-structural development. The measured resistivity of inkjet printed Ag films were $57.4\;{\sim}\;7.3\;{\mu}{\Omega}{\cdot}cm$. And their hardness and Young's modulus were 0.98 ~ 1.72 GPa and 32 ~ 71 GPa, respectively.

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Micellar Enhanced Ceramic Microfiltration for Removal of Aqueous Ferrous Ion: Effect of Surfactant Concentration and $N_2$-back-flushing (용존 철(II) 제거를 위한 미셀형성 세라믹 정밀여과: 계면활성제 농도 및 질소 역세척의 영향)

  • Park, Jin-Yong;Kang, Sung-Gyu
    • Membrane Journal
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    • v.19 no.2
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    • pp.136-144
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    • 2009
  • In this study, sodium dedocyl sulfate (SDS), which was anionic surfactant, was added for forming micelles to remove ferrous ions that could be contained with a small amount in industrial water. Then aggregates were formed by adsorption or binding of ferrous ions on the surface of micelles, and then rejected by ceramic membranes to remove ferrous ions. Ferrous concentration was fixed at 1mM and SDS was changed as $0{\sim}10mM$ to investigate the effect of the anionic surfactant. As a result, rejection rate of ferrous was the highest to 88.97% at 6mM. And we used ELS (Electrophoretic Light Scattering Spectrometer) to investigate particle size distribution of micellar aggregates depending on SDS concentration. Then distribution of large aggregates was the highest at 6mM. And we investigated effects of $N_2$-back-flushing time (BT) during periodic $N_2$-back-flushing on ceramic membranes. Finally optimal $N_2$-BT for NCMT-723l (pore size $0.10{\mu}m$) membrane was 20 sec.

The Influence of Heat Treatment and Ca contents on the Electrochemical Characteristics of Mg-Ca Alloys (Mg-Ca 합금의 전기화학적 특성에 미치는 Ca 첨가량 및 열처리의 영향)

  • Lee, S.H.;Chung, Dong-Seok;Park, B.O.;Kim, Y.G.;Jeong, Ha-Guk;Kim, Hye-Sung
    • Journal of the Korean Society for Heat Treatment
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    • v.17 no.3
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    • pp.173-179
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    • 2004
  • In this study, the influence of heat treatment and Ca contents on the electrochemical behavior was investigated. Mg-Ca alloys, i.e., Mg-0.22wt%Ca, Mg-0.56wt%Ca, Mg-1.31wt%Ca are prepared by ingot metallurgy. As-cast Mg-Ca alloys exhibited better electrochemical properties than pure Mg. Especially, Mg-0.22wt%Ca alloy improves its anode efficiency up to 62% and lowers the OCP up to -1.72VSCE. Microstructure and XRD patterns of Mg-Ca alloys show that additive Ca element is mainly solid-solutioned. While, the others show the microstructure and XRD pattern with large $Mg_2Ca$ at grain boundary. To assess the effect of heat treatment on the as-cast Mg-alloy, the specimens were heat treated at $200^{\circ}C$ for 2 hours under $CO_2$ gas atmosphere. Although corrosion properties of Mg-Ca alloys are somewhat deteriorated by heat treatment at $200^{\circ}C$ Mg-0.22wt%Ca alloy with uniformly distributed nano-sized $Mg_2Ca$ phase in ${\alpha}$-Mg matrix show still better corrosion properties than pure Mg specimen.

Mechanical properties and microstructures of stabilised dredged expansive soil from coal mine

  • Chompoorat, Thanakorn;Likitlersuang, Suched;Sitthiawiruth, Suwijuck;Komolvilas, Veerayut;Jamsawang, Pitthaya;Jongpradist, Pornkasem
    • Geomechanics and Engineering
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    • v.25 no.2
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    • pp.143-157
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    • 2021
  • Expansive soil is the most predominant geologic hazard which shows a large amount of shrinkage and swelling with changes in their moisture content. This study investigates the macro-mechanical and micro-structural behaviours of dredged natural expansive clay from coal mining treated with ordinary Portland cement or hydrated lime addition. The stabilised expansive soil aims for possible reuse as pavement materials. Mechanical testing determined geotechnical engineering properties, including free swelling potential, California bearing ratio, unconfined compressive strength, resilient modulus, and shear wave velocity. The microstructures of treated soils are observed by scanning electron microscopy, x-ray diffraction, and energy dispersive spectroscopy to understand the behaviour of the expansive clay blended with cement and lime. Test results confirmed that cement and lime are effective agents for improving the swelling behaviour and other engineering properties of natural expansive clay. In general, chemical treatments reduce the swelling and increase the strength and modulus of expansive clay, subjected to chemical content and curing time. Scanning electron microscopy analysis can observe the increase in formation of particle clusters with curing period, and x-ray diffraction patterns display hydration and pozzolanic products from chemical particles. The correlations of mechanical properties and microstructures for chemical stabilised expansive clay are recommended.

Thermophoretic Control of Particle Transport in a Microfluidic Channel (미세유체 채널 내에서 열영동에 의한 입자이동 제어)

  • So, Ju-Hee;Koo, Hyung-Jun
    • Korean Chemical Engineering Research
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    • v.57 no.5
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    • pp.730-734
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    • 2019
  • Thermophoresis is a transport phenomenon of particles driven by a temperature gradient of a medium. In this paper, we discuss the thermophoresis of particles in microfluidic channels. In a non-fluidic, stagnant channel, the thermophoretic transport of micro-particles was found to be larger in proportion to the voltage applied to the platinum wire heat source installed in the channel. The variation of the temperature around the platinum wire depending on the voltage was estimated, by using the Callendar-van Dusen equation. The thermophoretic behavior of nano-particles in the same system was observed, which is similar to that of the microparticles. Finally, we fabricated a Y-shaped microfluidic channel with a platinum wire heat source installed in the channel, to realize the thermophoretic phenomenon of the particles in the suspension flowing through the channel. It is shown that the flow of the suspension can be controlled based on the thermophoretic principle.

Performance Evaluation of Combined Sewer Overflow Treatment using Filtration Pilot Device (파일럿 여과장치를 이용한 합류식하수관 월류수 처리성능 평가)

  • Lee, Jun Ho;Shin, Young Gyun
    • Journal of Korean Society on Water Environment
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    • v.35 no.5
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    • pp.409-417
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    • 2019
  • In this study, a $480m^3/day$ pilot device was constructed through laboratory experiments based on the Ministry of Environment manual. The purpose of this study was to analyze the characteristics of CSO treatment and backwashing characteristics by applying the pilot device to the field. The purpose of this study was to acquire the basic data necessary for the design and operation management of the real scale filtration type non-point pollution control system. The filtration was conducted while maintaining the linear velocity of 20m/hour. The CSO treatment efficiencies of the pilot devices were 0.4-76.1%(mean 49.0 %), SS 51.4-91.6%(mean 77.8%), COD 22.2-59.4% (mean 38.3%) and TP 14.5-52.6%(mean 38.1%),respectively. The correlation coefficient between SS and the turbidity of influent water was 0.90, higher than that of CSO. To operate the treatment system effectively, the turbidity can be easily measured in real time as the monitoring item is the most appropriate because SS is the main target substance of the non-point source. As a result of analyzing the adsorbent treatment characteristics of PP filter material applied to this pilot device, the average particle diameter range of influent was $4.6-40.1{\mu}m$(mean $21.2{\mu}m$) and the treated water was $0.9-24.5{\mu}m$(mean $6.4{\mu}m$), respectively. Particles of approximately 10m or less are leached out, and so it is necessary to compensate for the raw water containing micro particulate matter.

Cations of Soil Minerals and Carbon Stabilization of Three Land Use Types in Gambari Forest Reserve, Nigeria

  • Falade, Oladele Fisayo;Rufai, Samsideen Olabiyi
    • Journal of Forest and Environmental Science
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    • v.37 no.2
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    • pp.116-127
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    • 2021
  • Predicting carbon distribution of soil aggregates is difficult due to complexity in organo-mineral formation. This limits global warming mitigation through soil carbon sequestration. Therefore, knowledge of land use effect on carbon stabilization requires quantification of soil mineral cations. The study was conducted to quantify carbon and base cations on soil mineral fractions in Natural Forest, Plantation Forest and Farm Land. Five 0.09 ha were demarcated alternately along 500 m long transect with an interval of 50 m in Natural Forest (NF), Plantation Forest (PF) and Farm Land (FL). Soil samples were collected with soil cores at 0-15, 15-30 and 30-45 cm depths in each plot. Soil core samples were oven-dried at 105℃ and soil bulk densities were computed. Sample (100 g) of each soil core was separated into >2.0, 2.0-1.0, 1.0-0.5, 0.5-0.05 and <0.05 mm aggregates using dry sieve procedure and proportion determined. Carbon concentration of soil aggregates was determined using Loss-on-ignition method. Mineral fractions of soil depths were obtained using dispersion, sequential extraction and sedimentation methods of composite soil samples and sieved into <0.05 and >0.05 mm fractions. Cation exchange capacity of two mineral fractions was measured using spectrophotometry method. Data collected were analysed using descriptive and ANOVA at α0.05. Silt and sand particle size decreased while clay increased with increase in soil depth in NF and PF. Subsoil depth contained highest carbon stock in the PF. Carbon concentration increased with decrease in aggregate size in soil depths of NF and FL. Micro- (1-0.5, 0.5-0.05 and <0.05 mm) and macro-aggregates (>2.0 and 2-1.0 mm) were saturated with soil carbon in NF and FL, respectively. Cation exchange capacity of <0.05 mm was higher than >0.05 mm in soil depths of PF and FL. Fine silt (<0.05 mm) determine the cation exchange capacity in soil depths. Land use and mineral size influence the carbon and cation exchange capacity of Gambari Forest Reserve.

OGLE-2017-BLG-1049: ANOTHER GIANT PLANET MICROLENSING EVENT

  • Kim, Yun Hak;Chung, Sun-Ju;Udalski, A.;Bond, Ian A.;Jung, Youn Kil;Gould, Andrew;Albrow, Michael D.;Han, Cheongho;Hwang, Kyu-Ha;Ryu, Yoon-Hyun;Shin, In-Gu;Shvartzvald, Yossi;Yee, Jennifer C.;Zang, Weicheng;Cha, Sang-Mok;Kim, Dong-Jin;Kim, Hyoun-Woo;Kim, Seung-Lee;Lee, Chung-Uk;Lee, Dong-Joo
    • Journal of The Korean Astronomical Society
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    • v.53 no.6
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    • pp.161-168
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    • 2020
  • We report the discovery of a giant exoplanet in the microlensing event OGLE-2017-BLG-1049, with a planet-host star mass ratio of q = 9.53 ± 0.39 × 10-3 and a caustic crossing feature in Korea Microlensing Telescope Network (KMTNet) observations. The caustic crossing feature yields an angular Einstein radius of θE = 0.52 ± 0.11 mas. However, the microlens parallax is not measured because the time scale of the event, tE ≃ 29 days, is too short. Thus, we perform a Bayesian analysis to estimate physical quantities of the lens system. We find that the lens system has a star with mass Mh = 0.55+0.36-0.29 M⊙ hosting a giant planet with Mp = 5.53+3.62-2.87 MJup, at a distance of DL = 5.67+1.11-1.52 kpc. The projected star-planet separation is a⊥ = 3.92+1.10-1.32 au. This means that the planet is located beyond the snow line of the host. The relative lens-source proper motion is μrel ~ 7 mas yr-1, thus the lens and source will be separated from each other within 10 years. After this, it will be possible to measure the flux of the host star with 30 meter class telescopes and to determine its mass.