• Title/Summary/Keyword: metallurgical technology

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Spherodization of Granuled Cr2O3 Fine Ceramic Powder by Plasma Spray (플라즈마 분사 처리에 의한 Cr2O3 조립분말의 구상화에 대한 연구)

  • Lee, Dong Won;Lee, Hak Sung;Yu, Ji-Hun;Wang, Jei-Pil
    • Resources Recycling
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    • v.25 no.6
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    • pp.92-97
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    • 2016
  • Spray dried $Cr_2O_3$ powder having an agglomerated structure of particles was twice treated into a plasma flame to increase its apparent density. The powder subjected to the first densification treatment did not show the entirely melted state keeping inner particle hollows, and it was fully melted after the second processing only. The powder size as a result of the second treatment decreased, and the apparent density as well as flowability were increased due to melting and surface smoothing effects. But a part of particles after the second densified treatment showed the hollow structure, especially those which were above $30{\mu}m$ in size. This densification behavior of the powder has been qualitatively discussed in terms of the thermal conductivity and inner gas pressure within aggregates exposed to the plasma flame.

Characteristics of Excimer Laser-Annealed Polycrystalline Silicon on Polymer layers (폴리머 위에 엑시머 레이저 방법으로 결정화된 다결정 실리콘의 특성)

  • Kim, Kyoung-Bo;Lee, Jongpil;Kim, Moojin;Min, Youngsil
    • Journal of Convergence for Information Technology
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    • v.9 no.3
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    • pp.75-81
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    • 2019
  • In this work, we investigated a low temperature polycrystalline silicon (LTPS) thin film transistors fabrication process on polymer layers. Dehydrogenation and activation processes were performed by a furnace annealing at a temperature of $430^{\circ}C$ for 2 hr. The crystallization of amorphous silicon films was formed by excimer laser annealing (ELA) method. The p-type device performance, fabricated by polycrystalline silicon (poly-Si) films, shows a very good performance with field effect mobility of $77cm^2/V{\cdot}s$ and on/off ratio current ratio > $10^7$. We believe that the poly-Si formed by a LTPS process may be well suited for fabrication of poly-Si TFTs for bendable panel displays such as AMOLED that require circuit integration.

Design and Implementation of OPC-Based Intelligent Precision Servo Control Power Forming Press System (OPC 기반의 지능형 정밀 서보제어 분말성형 프레스 시스템의 설계 및 구현)

  • Yoo, Nam-Hyun
    • The Journal of the Korea institute of electronic communication sciences
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    • v.13 no.6
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    • pp.1243-1248
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    • 2018
  • Metal Powder Metallurgy is a manufacturing technology that makes unique model parts or a certain type of product by using a hardening phenomenon when a powder of metal or metal oxide is put it into a mold and compression-molded by a press and then heated and sintered at a high temperature. Powder metallurgical press equipment is mainly used to make the parts of automobile, electronic parts and so on, and most of them are manufactured using precise servo motor. The intelligent precision servo control powder molding press system which is designed and implemented in this paper has advantages of lowering the price and maintaining the precision by using the mechanical camshaft for the upper ram part and precisely controlling the lower ram part using the high precision servo system. In addition, OPC-based monitoring and process data collection systems are designed and implemented to provide scalability that can be applied to smart manufacturing management systems that utilize Big Data in the future.

Effect of Perovskite Surface Treatment Using Oxygen Atmospheric Pressure Plasma (산소분위기의 상압플라즈마를 이용한 페로브스카이트 표면 처리 효과)

  • Kim, Kyoung-Bo;Lee, Jongpil;Kim, Moojin
    • Journal of Convergence for Information Technology
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    • v.11 no.6
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    • pp.146-153
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    • 2021
  • Recently, research on perovskite semiconductor materials has been performed, and the evaluation of properties using surface treatment for this material is the basis for subsequent studies. We studied the results of surface treatment of perovskite thin films exposed to air for about 6 months by generating oxygen plasma with an atmospheric pressure plasma equipment. The reason for exposure for 6 months is that the perovskite thin film is made of organic and inorganic substances, so when exposed to air, the surface changes through reaction with oxygen or water vapor. Therefore, this change is to investigate whether it is possible to restore the original film. The surface shape and the ratio of elements were analyzed by varying the process time from 1 s to 1200 s in an oxygen plasma atmosphere. It was found that the crystal grains change over a process time of 5 s or more. In order to maintain the properties of the deposited film, it is the optimal process condition between 2 s and 5 s.

Characteristics by deposition and heat treatment of Cr and Al thin film on stainless steel (금속 기판위에 Cr과 Al 증착 및 열처리 융합 기술에 의한 표면 형상 변화)

  • Kim, Kyoung-Bo;Lee, Jongpil;Kim, Moojin
    • Journal of Convergence for Information Technology
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    • v.11 no.3
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    • pp.167-173
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    • 2021
  • There is an increasing interest in manufacturing various electronic devices on a bendable substrate. In this paper, we observed a surface morphology by annealing for 20 minutes at temperatures of 150 ℃, 350 ℃, and 550 ℃, respectively, with samples coated by chromium and aluminum. Data on surfaces are investigated using high-resolution SEM and AFM that can measure roughness up to nm. There is no difference from the sample without heat treatment up to 350 ℃, but the change of crystal grains can be observed at 550 ℃. In the future, for application to the flexible optoelectronic field, additional characteristics such as electrical conductivity and reflectivity will be analyzed and optical devices will be manufactured. In conclusion, we will explore the possibility of applying metal materials to flexible electronic devices.

Influence of Droplet Size and Oil Viscosity on the Descending Velocity of Droplets Using Water Model With and Without Stirring (교반 유무에 따른 수모델을 사용한 액적의 하강 속도에 대한 액적 크기 및 오일 점도의 영향)

  • Hyeok-In Kwon;Alberto Conejo;Sung Yong Jung;Sun-Joong Kim
    • Resources Recycling
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    • v.32 no.2
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    • pp.33-42
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    • 2023
  • Metal emulsions have been studied for several decades as a method of increasing the efficiency of the steelmaking process. This study was performed using a water model, observable at room temperature, to compensate for the disadvantages of the high-temperature experiment, the results of which are difficult to observe visually. As a substitute for metal-in-slag emulsions, experiments were conducted by dropping distilled water into silicone oil and comparing the results with the results of a calculation by momentum balance equations. The descending velocity of the water droplet decreased as the diameter of the droplet and viscosity of the fluid (silicon oil) increased. To simulate the descending velocity of a water droplet in silicon oil under stirring conditions, the flow rate of the fluid (silicon oil) was measured by particle image velocimetry (PIV) methods. The calculation of the descending velocity of the water droplet was in good agreement with the measured values, with and without stirring a viscous silicone oil.

Effects of Extrusion Ratio and Extrusion Temperature on Microstructure and Tensile Properties of SEN6 Magnesium Alloy (SEN6 마그네슘합금의 미세조직과 인장 특성에 미치는 압출비와 압출 온도의 영향)

  • H. J. Kim;J. Y. Lee;S. C. Jin;S. H. Park
    • Transactions of Materials Processing
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    • v.33 no.3
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    • pp.178-184
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    • 2024
  • In this study, we investigated the effects of extrusion ratio and extrusion temperature on the microstructure and tensile properties of extruded Mg-6Al-0.3Mn-0.3Ca-0.2Y (SEN6) alloy. As the extrusion ratio and temperature increase, dynamic recrystallization during extrusion is promoted, leading to the formation of a fully recrystallized microstructure with increased grain size. Additionally, the increases in extrusion ratio and temperature lead to texture strengthening, exhibiting a higher maximum texture intensity. The extruded materials contain three types of secondary phases, i.e., Al8Mn4Y, Al2Y, and Al2Ca, with irregular or polygonal shapes. The quantity, size, distribution, and area fraction of the second-phase particles are nearly identical between the two materials. Despite its larger grain size, the tensile yield strength of the material extruded at 450 ℃ and an extrusion ratio of 25 (450-25) is higher than that of the material extruded at 325 ℃ and an extrusion ratio of 10 (325-10), which is mainly attributed to the stronger texture hardening effect of the former. The ultimate tensile strength is similar in the two materials, owing to the higher work hardening rate in the 325-10 extrudate. Despite differences in grain size and recrystallization fraction, numerous twins are formed throughout the specimen during tensile deformation in both materials; consequently, the two materials exhibit nearly the same tensile elongation.

Band-Gap Energy and Thermoelectric Properties of 90% $Bi_2Te_3-10% Bi_2Se_3$ Single Crystals (90% $Bi_2Te_3-10% Bi_2Se_3$ 단결정의 밴드갭 에너지와 열전특성)

  • Ha, Heon-Pil;Hyeon, Do-Bin;Hwang, Jong-Seung;O, Tae-Seong
    • Korean Journal of Materials Research
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    • v.9 no.4
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    • pp.349-354
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    • 1999
  • The temperature dependences of the Hall coefficient, carrier mobility, electrical resistivity, Seebeck coefficient, thermal conductivity, and figure-of-merit of the undoped and $CdI_2$-doped 90% $Bi_2Te_3-10% Bi_2Se_3$, single crystals, grown by the Bridgman method, have been characterized at temperatures ranging from 77K to 600K. The saturated carrier concentration and degenerate temperature of the undoped 90% $Bi_2Te_3-10% Bi_2Se_3$ single crystal are $5.85\times10_{18}cm^{-3}$ and 127K, respectively. The scattering parameter of the 90% $Bi_2Te_3-10% Bi_2Se_3$ single crystal is determined to b -0.23, and the electron mobility to hole mobility ratio ($\mu_e/\mu_h)$ is 1.45. The bandgap energy at 0K of the 90% <$Bi_2Te_3-10% Bi_2Se_3$ single crystal is 0.200 eV. Adding $CdI_2$as a donor dopant, a maximum figure-of-merit of $3.2\times10^{-3}/K$$CdI_2$-doped specimen.

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A Study on the Mechanical Properties of Single and Multiple layer Thin Film of YSZ Electrolyte Produced by E-beam Coating for Solid Oxide Fuel Cells (전자빔 코팅에 의해 제조된 고체산화물 연료전지용 YSZ 전해질 단층 및 다층박막의 기계적 특성 연구)

  • Im, Hae-Sang;Kim, Hui-Jae;Park, Jong-Wan
    • Korean Journal of Materials Research
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    • v.9 no.8
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    • pp.792-797
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    • 1999
  • The 8mol.%Y$_2$$O_3$-$ZrO_2$mainly employed as an electrolyte of solid oxide fuel cells(SOFCs) shows excellent electrical properties but has a weakness in the mechanical properties. Since the electrolyte of SOFCs requires both good electrical and mechanical properties, this study was conducted to meet both requirements. The electrolyte thin films were produced on the LSM(cathode material) substrate of a cell and Si wafer. Four electrolyte film types of single layer and the multiple layer, consisting of 3-YSZ(3mol.%$Y_2$$O_3$) with excellent mechanical properties and 8-YSZ with the excellent electric conduction, were produced by electron beam coating technology. Ther crystal structure and the mechanical properties were also analysed. As the results of the study, the 3-YSZ thin film turned out to be in the tetragonal, partially monoclinic phase, while the 8-YSZ thin film showed the cubic phase. The residual stress in the multiple layer was lower than that of the single layer. The microhardness of the multiple layer was similar to that of the existing 8-YSZ single layer both before and after annealing treatment.

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Metallurgical Investigation of the Iron Objects from Suchon-ri Site in Gongju (공주 수촌리유적 출토 철제유물의 금속학적 분석)

  • Cho, Hyun Kyung;Cho, Nam Chul;Lee, Hun
    • Journal of Conservation Science
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    • v.30 no.3
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    • pp.317-327
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    • 2014
  • Iron objects excavated from the sites of Mahan and Baekje are dominated by swords, spearheads and arrowheads. Spearheads usually have a function of weapon and swords with ring pommel are considered fancy articles because of ornament in ring pommel. In Gongju Suchon-ri site, the central type and the local type of the Baekje tombs co-exist together. The sword with ring pommel, the long sword and spearheads were excavated. They are investigated metallurgically and we focused of their functions and manufacturing techniques. Solid carburizing technology and quenching of heat treatment applied the sword with ring pommel was presumed as fancy article in the late 4th century while these techniques didn't apply spearhead from same tomb. This informed that the central government of Baekje had high technology on iron manufacture in 4th century. In case of local gentry, they didn't apply this high technology to mass-produced spearheads, even though they had it. Thus, it is able to say the sword with ring pommel was applied techniques of the central government and spearheads, the weapons were applied techniques of local societies.