• Title/Summary/Keyword: material tests

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Effect of Vapor Deposition on the Interdiffusion Behavior between the Metallic Fuel and Clad Material (금속연료-피복재 상호확산 거동에 미치는 기상증착법의 영향)

  • Kim, Jun Hwan;Lee, Byoung Oon;Lee, Chan Bock;Jee, Seung Hyun;Yoon, Young Soo
    • Korean Journal of Metals and Materials
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    • v.49 no.7
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    • pp.549-556
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    • 2011
  • This study aimed to evaluate the performance of diffusion barriers in order to prevent fuel-cladding chemical interaction (FCCI) between the metallic fuels and the cladding materials, a potential hazard for nuclear fuel in sodium-cooled fast reactors. In order to prevent FCCI, Zr or V metal is deposited on the ferritic-martensitic stainless steel surface by physical vapor deposition with a thickness up to $5{\mu}m$. The diffusion couple tests using uranium alloy (U-10Zr) and a rare earth metal such as Ce-La alloy and Nd were performed at temperatures between 660~800$^{\circ}C$. Microstructural analysis using SEM was carried out over the coupled specimen. The results show that significant interdiffusion and an associated eutectic reaction ocurred in the specimen without a diffusion barrier. However, with the exception of the local dissolution of the Zr layer in the Ce-La alloy, the specimens deposited with Zr and V exhibited superior eutectic resistance to the uranium alloy and rare earth metal.

The Mechanical Properties and Biocompatibility of Functionally Graded Coatings(FGC) of Hydroxyapatite(HA) and Metallic Powders - Functionally Gradient Coatings of Thermal Spray in Air- (Hydroxyapatite (HA)와 금속 분말 경사 코팅의 기계적 특성 및 생체 적합성 - 대기 열용사 경사코팅 -)

  • Kim, Eun-Hye;Kim, Yu-Chan;Han, Seung-hee;Yang, Seok-Jo;Park, Jin-Woo;Seok, Hyun-Kwang
    • Korean Journal of Metals and Materials
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    • v.47 no.1
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    • pp.13-20
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    • 2009
  • This work presents functionally graded coatings (FGC) of hydroxyapatite (HA) and metallic powders on Ti-6Al-4V implants using plasma spray coating method. HA has been the most frequently used coating material due to its excellent compatibility with human bones. However, because of the abrupt changes in thermomechanical properties between HA and the metallic implant across an interface, and residual stress induced on cooling from coating temperture to room temperature, debonding at the interface occurs in use sometimes. In this work, FGC of HA and Ti or Ti-alloy powders is made to mitigate the abrupt property changes at the interface and the effect of FGC on residual stress release is investigated by evaluating the mechanical bond strength between the implant and the HA coating layers. Thermal annealing is done after coating in order to crystallize the HA coating layer which tends to have amorphous structure during thermal spray coating. The effects of types and compositional ratio of metallic powders in FGC and annealing conditions on the bond strength are also evaluated by strength tests and the microstructure analysis of coating layers and interfaces. Finally, biocompatibility of the coating layers are tested under ISO 10993-5.

Viologen Based All-in-one Flexible Electrochromic Devices (바이올로진 기반의 일체형 유연 전기변색소자)

  • Park, Bo-Seong;Kim, Hyun-Jeong;Shin, Hyeonho;Park, Seongmin;Lee, Jaeun;Jeon, Sunggun;Nah, Yoon-Chae
    • Korean Journal of Materials Research
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    • v.31 no.3
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    • pp.132-138
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    • 2021
  • Electrochromic devices (ECDs) have been drawing great attention due to their high color contrast, low power consumption, and memory effect, and can be used in smart windows, automatic dimming mirrors, and information display devices. As with other electronic devices such as LEDs (light emitting diodes), solar cells, and transistors, the mechanical flexibility of ECDs is one of the most important issue for their potential applications. In this paper, we report on flexible ECDs (f-ECDs) fabricated using an all-in-one EC gel, which is a mixture of electrolyte and EC material. The f-ECDs are compared with rigid ECDs (r-ECDs) on ITO glass substrate in terms of color contrast, coloration efficiency, and switching speed. It is confirmed that the f-ECDs embedding all-in-one gel show strong blue absorption and have competitive EC performance. Repetitive bending tests show a degradation of electrochromic performance, which must be improved using an optimized device fabrication process.

Design Evaluation of the Post-installed Anchor considering Effective Embedded Depth and Concrete Strength (유효 묻힘 깊이와 콘크리트 강도를 고려한 후설치 앵커의 설계식 평가)

  • Hur, Moo-Won;Chae, Kyoung-Hun;Won, Jae-Sik;Park, Tae-Won
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.25 no.3
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    • pp.13-20
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    • 2021
  • Post-installed anchor is a structural material that connects structural and non-structural members to existing concrete members. However, there are cases where rebar interception and construction error occur at the site. In that case, measures are needed to prevent performance degradation of the rear-installation anchors. In this study, in order to evaluate the performance of torsional control expandable post-installed anchors for compressive strength and effective depth of the reference concrete was tested. The results of the most commonly used tests of M10 and M20 showed that had variable coefficients within 15%, satisfying the reliability presented in KCI(2017). It was also confirmed that the depth of the buried and the strength of concrete affect the strength of the pavement. Based on the results of the existing similar studies and the results of this study, the design equation of the post-installed anchor was proposed and the results were compared with the existing design.

Utilization of Ready-mixed Concrete Recycling Water Mixed with Hot-rolled Slag Containing C12A7 and Application Characteristics of Cement Mortar (C12A7을 함유한 열연슬래그를 혼입한 레미콘 회수수 활용 및 시멘트 모르타르의 적용 특성)

  • Kim, Young-Yeop;Lee, Han-Seung
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.9 no.1
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    • pp.92-99
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    • 2021
  • CaO-based by-products composed of CaO, SO3, Al2O3, etc. are generally used as raw materials for CaO compounds. When applied to the recovered water of ready-mixed concrete, the hydration reaction of the powder material is accelerated and concrete performance can be improved. In this study, activated sludge was prepared to apply to the recovered water of ready-mixed concrete by mixing CaO-based hot-rolled slag(C12A7) in the recycling water of ready-m ixed concrete. Cem ent paste setting time and mortar compressive strength performance tests confirmed the effect on the hydration reaction. Therefore, the possibility of concrete application using activated sludge was confirmed.

Anti-inflammatory and Anti-itching Effects of Herbal Medicine Complex Extracts(NI-01) (한약복합추출물(NI-01)의 항염증 및 소양감 억제 효과)

  • Kim, Hyun-A;Kim, Suk-Kyung;Kim, Bae-Hwan
    • Journal of Physiology & Pathology in Korean Medicine
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    • v.34 no.6
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    • pp.341-347
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    • 2020
  • The purpose of this study was to investigate the possibility of herbal medicine complex extract (NI-01), which were prepared from 6 natural materials (Cinnamomum cassia Blume, Lonicerae Flos, Paeonia suffruticosa Andrews, Arctium lappa Linne, Schzandra chinesis Bailon, Elsholtzia ciliata Hylander), as a functional material for inhibition of atopic dermatitis. anti-oxidative activity was confirmed by measuring DPPH electron donating ability and ABTS+ radical scavenging ability. Cytotoxicity and NO inhibition were measured using RAW 264.7 cells to confirm anti-inflammatory efficacy. The test substance was orally administered to the pruritus-induced ICR mice to confirm the inhibition of pruritus. The bovine cornea opacity and permeability (BCOP) assay was performed to confirm safety for irritation. NI-01 showed high antioxidant activity in DPPH and ABTS+ methods. In the anti-inflammatory effect tests with RAW 264.7 cells, NO production was inhibited at NI-01 concentrations of 50 (14.9%) and 100 (4.2%) ㎍/mL, which indicated that the anti-inflammatory effect was increased in a concentration-dependent manner. NI-01 also showed anti-itching effect after inducing of itching by compound 48/80 in ICR mice. NI-01 was proved to be a non-irritant substance in BCOP assay. The results of this study suggested that the herbal medicine combined extract (NI-01) has high antioxidant, anti-inflammatory and anti-itching effects, and safety for irritation. Therefore, herbal medicine complex extract (NI-01) is thought to be highly applicable for the inhibitory ingredients of the atopic dermatitis.

Characteristics of Concrete Using Ready-Mixed Concrete Recycled Water Mixed with Industrial By-Product Desulfurization Gypsum (산업부산물 탈황석고 혼입 레디믹스트콘크리트 회수수를 이용한 콘크리트의 특성)

  • Kim, Young-Yeop;Lee, Han-Seung
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.8 no.4
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    • pp.395-403
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    • 2020
  • CaO-based by-product, which consist of CaO, SO3, Al2O3 and so on, has being used to raw materials of CaO compound. When It was applied to recycling water of remicon, concrete performance can be enhanced because hydration reaction of powder material is accelerated. In this study, activated-sludge, which was putted desulfurization gypsum of CaO-based in recycling water, was manufactured to verify effect of them, and then they was investigated by characteristics of redy-mixde concrete. As a result of concrete tests, it was confirmed that there is no problem of strength or drying shrinkage while ensuring workability. Therefore, the possibility of specific application using activated sludge was confirmed.

Experimental research on the effect of water-rock interaction in filling media of fault structure

  • Faxu, Dong;Zhang, Peng;Sun, Wenbin;Zhou, Shaoliang;Kong, Lingjun
    • Geomechanics and Engineering
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    • v.24 no.5
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    • pp.471-478
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    • 2021
  • Water damage is one of the five disasters that affect the safety of coal mine production. The erosion of rocks by water is a very important link in the process of water inrush induced by fault activation. Through the observation and experiment of fault filling samples, according to the existing rock classification standards, fault sediments are divided into breccia, dynamic metamorphic schist and mudstone. Similar materials are developed with the characteristics of particle size distribution, cementation strength and water rationality, and then relevant tests and analyses are carried out. The experimental results show that the water-rock interaction mainly reduces the compressive strength, mechanical strength, cohesion and friction Angle of similar materials, and cracks or deformations are easy to occur under uniaxial load, which may be an important process of water inrush induced by fault activation. Mechanical experiment of similar material specimen can not only save time and cost of large scale experiment, but also master the direction and method of the experiment. The research provides a new idea for the failure process of rock structure in fault activation water inrush.

A Study of Germination Characteristics of Native Plants to be Utilized in DMZ Barren Land (불모지 내 활용 가능한 자생식물의 발아특성 연구)

  • Kim, Dong-Hak;Kim, Sang-Jun;Yu, Seung-Bong;Bak, Gippeum
    • Journal of the Korean Society of Environmental Restoration Technology
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    • v.24 no.4
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    • pp.1-14
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    • 2021
  • This study suggested suitable soil textures that is proper to propagate native plants to manage and restore barren land in DMZ. Germination tests were conducted for 16 native herbaceous plants growing in the DMZ border area in accordance with FAO-BI (Biodiversity International) standards, and the germination rate and T50 in vitro were investigated. In order to examine the germination characteristics according to the soil textures, we used gravel, bed and mixed soil and investigated the germination characteristics under ordinary room temperature conditions in the greenhouse. As a result, it was observed that the germination rate in the greenhouse was significantly decreased compared to the germination rate in vitro of the species advertised due to soil textures. T50 between the in vitro and each soil texture showed significant differences whereas T50 between soil textures alone did not in all species advertised. The germination rate in vitro of Aster koraiensis, Dendranthema zawadskii var. latilobum, Hosta clausa, and Hosta minor there was no significant difference compared to ordinary room temperature conditions. In addition, as the germination rate is demonstrated more than 70%, which is relatively higher than other species advertised, it is considered to have strong environmentally adaptable. On the other hand, considering that the 6 species of Leontopodium coreanum, Plantago major, Potentilla chinensis, Sedum kamtschaticum, Sedum latiovalifolium, and Veronica kiusiana demonstrated less than 50% of germination rate in vitro, it is expected to be difficult to propagate without pre-treatment. In order to use these 6 species as restoration material plants, it needs to be considered to pre-treat to improve germination rate, or to enhance the vitality of seeds by improving the seed gathering period and storage method.

Antinociceptive, anti-inflammatory, and cytotoxic properties of Origanum vulgare essential oil, rich with β-caryophyllene and β-caryophyllene oxide

  • Moghrovyan, Armenuhi;Parseghyan, Lilya;Sevoyan, Gohar;Darbinyan, Anna;Sahakyan, Naira;Gaboyan, Monica;Karabekian, Zaruhi;Voskanyan, Armen
    • The Korean Journal of Pain
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    • v.35 no.2
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    • pp.140-151
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    • 2022
  • Background: Essential oils are of great interest for their analgesic and anti-inflammatory properties. We aimed to study the content of the essential oil of the Origanum vulgare of the Armenian highlands (OVA) in different periods of vegetation and to investigate its antinociceptive and anti-inflammatory effects in mice (in vivo) and cytotoxic action in cultured cells (in vitro). OVA essential oil was extracted from fresh plant material by hydro-distillation. Methods: For OVA essential oil contents determination the gas chromatography-mass spectrometry method was used. Formalin and hot plate tests and analysis of cell viability using the methyl-thiazolyl-tetrazolium (MTT) assay were used. Results: The maximal content of β-caryophyllene and β-caryophyllene oxide in OVA essential oil was revealed in the period of blossoming (8.18% and 13.36%, correspondently). In the formalin test, 4% OVA essential oil solution (3.5 mg/mouse) exerts significant antinociceptive and anti-inflammatory effects (P = 0.003). MTT assay shows approximately 60% cytotoxicity in HeLa and Vero cells for 2.0 µL/mL OVA essential oil in media. Conclusions: The wild oregano herb of Armenian highlands, harvested in the blossoming period, may be considered as a valuable source for developing pain-relieving preparations.