• Title/Summary/Keyword: material tests

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Corrosion Behavior of Pyro-Carbon in Hot Lithium Molten Salt Under an Oxidation Atmosphere (산화성 고온 리튬용융염계 분위기에서 Pyro-Carbon의 부식거동)

  • Lim, Jong-Ho;Choi, Jeong-Mook
    • Korean Journal of Materials Research
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    • v.23 no.2
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    • pp.123-127
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    • 2013
  • The electrolytic reduction of a spent oxide fuel involves liberation of the oxygen in a molten LiCl electrolyte, which is a chemically aggressive environment that is too crosive for typical structural materials. Therefore, it is essential to choose the optimum material for the process equipment for handling a molten salt. In this study, the corrosion behavior of pyro-carbon made by CVD was investigated in a molten LiCl-$Li_2O$ salt under an oxidation atmosphere at $650^{\circ}C$ and $750^{\circ}C$ for 72 hours. Pyro-carbon showed no chemical reactions with the molten salt because of its low wettability between pyro-carbon and the molten salt. As a result of XRD analysis, pyro-carbon exposed to the molten salt showed pure graphite after corrosion tests. As a result of TGA, whereas the coated layer by CVD showed high anti-oxidation, the non-coated layer showed relatively low anti-oxidation. The stable phases in the reactions were $C_{(S)}$, $Li_2CO_{3(S)}$, $LiCl_{(l)}$, $Li_2O$ at $650^{\circ}C$ and $C_{(S)}$, $LiCl_{(l)}$, $Li_2O_{(S)}$ at $750^{\circ}C$. $Li_2CO_{(S)}$ was decomposed at $750^{\circ}C$ into $Li_2O_{(S)}$ and $CO_{2(g)}$.

Evaluation of the Temperature Dependent Flow Stress Model for Thermoplastic Fiber Metal Laminates (열가소성 섬유금속적층판의 온도를 고려한 유동응력 예측에 대한 연구)

  • Park, E.T.;Lee, B.E.;Kang, D.S.;Kim, J.;Kang, B.S.;Song, W.J.
    • Transactions of Materials Processing
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    • v.24 no.1
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    • pp.52-61
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    • 2015
  • Evaluation of the elevated temperature flow stress for thermoplastic fiber metal laminates(TFMLs) sheet, comprised of two aluminum sheets in the exterior layers and a self-reinforced polypropylene(SRPP) in the interior layer, was conducted. The flow stress as a function of temperature should be evaluated prior to the actual forming of these materials. The flow stress can be obtained experimentally by uniaxial tensile tests or analytically by deriving a flow stress model. However, the flow stress curve of TFMLs cannot be predicted properly by existing flow stress models because the deformation with temperature of these types of materials is different from that of a generic pure metallic material. Therefore, the flow stress model, which includes the effect of the temperature, should be carefully identified. In the current study, the flow stress of TFMLs were first predicted by using existing flow stress models such as Hollomon, Ludwik, and Johnson-Cook models. It is noted that these existing models could not effectively predict the flow stress. Flow stress models such as the modified Hollomon and modified Ludwik model were proposed with respect to temperatures of $23^{\circ}C$, $60^{\circ}C$, $90^{\circ}C$, $120^{\circ}C$. Then the stress-strain curves, which were predicted using the proposed flow stress models, were compared to the stress-strain curves obtained from experiments. It is confirmed that the proposed flow stress models can predict properly the temperature dependent flow stress of TFMLs.

A Study of Fire Extinguishment Characteristic for the Real Scale Deap-Seated Fire (실규모 심부화재 소화특성에 관한 연구)

  • Kim, Nam-Kyun;Rie, Dong-Ho
    • Fire Science and Engineering
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    • v.29 no.2
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    • pp.13-19
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    • 2015
  • Real scale fire tests was carried out for extinguishing performance evaluation of the wetting agent. The experiment was conducted in accordance with a Class A fire extinguishing test methods specified in the 'Type Approval of the Manual System Fire Extinguisher and Technical Standards of Test'. In addition, the subjects of this experiment were the wood flour and rice husk. Fire-fighting water, the three kinds of wetting agents used in the country and this study was used, was undertaken to determine a clear discrimination of the water and wetting agent. In the experimental results, it was confirmed that the internal temperature is maintained long time in the case of water. The internal temperature were rapidly lowered in the experiment of wetting agents. Therefore, the discrimination of extinguishing ability was confirmed by the temperature distribution in accordance with time. Based on the results of this experiment, this study is expected to be used as a underlying material on presenting a method of optimized performance evaluation of wetting extinguishing agent.

Study on the Thermal Protective Performance Measurements of Fire Fighter's Protective Clothing for Low Level Radiant Heat Exposures (저열유속 조건의 복사열 노출에 따른 소방보호복의 열보호성능 측정에 관한 연구)

  • Lee, Jun-Kyoung;Bang, Young-Jun;Bang, Chang-Hoon;Kwon, Jung-Suk
    • Fire Science and Engineering
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    • v.28 no.2
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    • pp.1-8
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    • 2014
  • Despite advancements in the development of synthetic fibers and materials that provide better insulation, fire burn injuries remain a significant issue. To ensure adequate protection, clothing and equipment must be selected on the basis of performance. There are different standards like ISO standards applicable to each of the various types of clothing used by fire fighters. But, in most cases, the tests are performed in the conditions of high heat flux exposure, the clothing material can be destroyed easily. Thus the effective way to investigate the protective performance for the low (radiant) heat flux conditions should be needed. Therefore improved RPP (Radiant Protective Performance) test method based on the onset of pain burn injury was suggested. Experiments were performed to verify the proposed method with current protective clothing for fire fighters and the transient heat transfer characteristics were identified, also. Moreover, several protective performance indices were acquired from experimental results to analyze their relations.

Tensile Behavior of Ultra-High Performance Concrete According to Combination of Fibers (섬유 조합에 따른 초고성능 콘크리트의 인장거동)

  • Choi, Jung-Il;Koh, Kyung-Taek;Lee, Bang-Yeon
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.19 no.4
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    • pp.49-56
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    • 2015
  • Ultra-High Strength Concrete(UHPC) has ultra-high material performance including high strength and high flowability. On the other hand it is less ductile than high ductile fiber reinforced cementitious composite. This study investigated the effect of combination of steel fiber and micro fiber on the tensile behavior of UHPC. Four types of UHPC containing combination of steel fiber, polyethylene(PE), polyvinyl alcohol(PVA), and basalt fiber were designed. And then uniaxial tension tests were performed to evaluate the tensile behavior of UHPC according to combination of fibers. And density was measured to evaluate whether micro fiber induces unintentional high pore or not. From the test results, it was exhibited that PE fiber with high strength is effective to improve the tensile behavior of UHPC and basalt fiber is effective to increase the cracking and tensile strength of UHPC. Furthermore, it was also verified that micro fiber does not make high pore.

Surface Tribology of Total Ankle Joint Replacement (인공발목관절의 표면 마모 특성)

  • Jeong, Yong-Hoon;Jung, Tae-Gon;Yang, Jae-Woong;Park, Kwang-Min;Lee, Su-Won
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2016.11a
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    • pp.117-117
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    • 2016
  • Total ankle replacement (TAR) is a visible option in the surgical treatment of degenerative or inflammatory diseases of ankle joint. it is attributed to the current TAR which has improvements in surgical technique, uncemented implant fixation and minimally constrained articulation. In the clinical result, they can show promised surgical result when compared to earlier attempts in TAR. However, TAR is still not as successful as total knee replacement (TKR) or total hip replacement (THR), it needs to be note that there are limitations in concerning of long term performance of TAR, the high failure rate still associated with wear of the PE (polyethylene) component that has related with their material property and surface roughness. The aim of this study was to introduce the tribology characteristics of total ankle joint prosthesis with one of TDR model which was fabricated to try multi-axis wear test as a region of motion in ankle joint. The wear specimen of TDR was prepared with Ti-6Al-4V alloy and UHMWPE (ultra-high molecular weight polyethylene) for tibia-talus and bearing component, respectively. A wear test was carried out using a Force 5 (AMTI, Massachusetts, US) wear simulator which can be allowed to move in three axis to flexion-extension ($+3^{\circ}{\sim}-6^{\circ}$), internal-external axial rotation (${\pm}5^{\circ}$), as well as sinusoidal compressive load (1.6 kN, R=10). All tests were performed following standard ISO 14243, wear rate was calculated with weight loss of UHMWPE bearing while the specimen has tested at certain cycles. As based on the preliminary results, wear rate of UHMWPE bearing was $7.9{\times}10^{-6}mg/cycles$ ($R^2=0.86$), calculated loss weight until $10^7cycles$ was 79 mg, respectively.

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A Study on the Properties of Anticorrosive for RC Structure (콘크리트구조물 보수용 방식피복재의 특성)

  • Moon, Han-Young;Shin, Dong-Gu;Kwon, Yong-Jin;Oh, Sang-Kun
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.9 no.1
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    • pp.251-258
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    • 2005
  • Up until now, most protection design has been concerned primarily with concrete's exterior protection from corrosion, its waterproof ability and its reparability. However, there are many cases in which service life of the concrete is shortened because suitability of the type of concrete surface has not been thoroughly investigated in the development process. According1y, this paper presents the development and test of the material for its reparability and its protection against corrosion in the case of wet surfaces (i.e. water supply facilities, sewage systems, and port facilities) in this country. From the test, both A type and B type are excellent for durability in watertightness, chemical resistance and abrasion. Test results of adhesive strength over $15kgf/cm^2$ under both wet and dry conditions, curing conditions and various temperatures conditions were also achieved in field tests.

Re-distribution of Welding Residual Stress Due to Tensile Pre-load and Its Effects on Fatigue Strength in Padding Plate Weldment (Padding plate 용접구조의 인장 정하중 이력에 의한 용접잔류응력 변화 및 피로강도에의 영향)

  • S.W. Kang;Y.W. Kim;W.S. Kim;D.H. Kim
    • Journal of the Society of Naval Architects of Korea
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    • v.38 no.4
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    • pp.75-82
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    • 2001
  • Static loadings on ship structure induced either by water pressure before service such as a tank test and ballasting or by cargo pressure during first laden voyage cause relatively much greater stress than dynamic loadings induced by wave. With these static pre-loadings, the initial residual stresses around welded joint, where fatigue strength is concerned(in most cases, where stress concentration occurs) are expected to be shaken-down in a great extent by the elasto-plastic deformation behavior of material. Therefore, it is more resonable to assess the fatigue strength of ship structure with S-N data which have taken into account the effect of shaken-down residual stresses(re-distributed stresses) on the fatigue strength. In this research work, the re-distribution of residual stresses by the tensile pre-loading is measured using an ordinary sectioning method for specimens of padding plate weldment. Fatigue tests are performed also to evaluate the fatigue strength of the both as-welded and pre-loaded specimens.

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Destructive testing of adhesively bonded joints under static tensile loading

  • Ochsner, A.;Gegner, J.
    • Journal of Adhesion and Interface
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    • v.5 no.2
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    • pp.22-36
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    • 2004
  • Several in-situ testing methods of adhesively bonded joints under static short-time tensile loading are critically analyzed in terms of experimental procedure and data evaluation. Due to its rather homogeneous stress state across the glue line, the tensile-shear test with thick single-lap specimens, according to ISO 11003-2, has become the most important test process for the determination of realistic materials parameters. This basic method, which was improved in both, the experimental part by stepped adherends and easily attachable extensometers and the evaluation procedure by numeric substrate deformation correction and test simulation based on the finite element method (FEM), is therefore demonstrated by application to several kinds of adhesives and metallic adherends. Multi-axial load decreases the strength of a joint. This effect, which is illustrated by an experimental comparison, impedes the derivation of realistic mechanical characteristics from measured force-displacement curves. It is shown by numeric modeling that tensile-shear tests with thin plate substrates according to ISO 4587, which are widely used for quick industrial quality assurance, reveal an inhomogeneous stress state, especially because of relatively large adherend deformation. Complete experimental determination of the elastic properties of bonded joints requires independent measurement of at least two characteristics. As the thick-adherend tensile-shear test directly yields the shear modulus, the tensile butt-joint test according to ISO 6922 represents the most obvious complement of the test programme. Thus, validity of analytical correction formulae proposed in literature for the derivation of realistic materials characteristics is verified by numeric simulation. Moreover, the influence of the substrate deformation is examined and a FEM correction method introduced.

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Study on the Determination of Fatigue Damage Parameter for Rubber Component under Multiaxial Loading (다축하중이 작용하는 방진고무부품 피로손상 파라미터 결정에 관한 연구)

  • Moon, Seong-In;Woo, Chang-Su;Kim, Wan-Doo
    • Elastomers and Composites
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    • v.47 no.3
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    • pp.194-200
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    • 2012
  • Rubber components have been widely used in automotive industry as anti-vibration components for many years. These subjected to fluctuating loads, often fail due to the nucleation and growth of defects or cracks. To prevent such failures, it is necessary to understand the fatigue failure mechanism for rubber materials and to evaluate the fatigue life for rubber components. The objective of this study is to develop the durability analysis process for vulcanized rubber components, which is applicable to predict fatigue life at initial product design step. The determination method of nonlinear material constants for FE analysis was proposed. In order to investigate the applicability of the commonly used damage parameters, fatigue tests and corresponding finite element analyses were carried out and strain energy density was proposed as the fatigue damage parameter for rubber components. The fatigue analysis for automotive rubber components was performed and the durability analysis process was reviewed.