• Title/Summary/Keyword: mass microscope

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The research on static and dynamic mechanical properties of concrete under the environment of sulfate ion and chlorine ion

  • Nie, Liangxue;Xu, Jinyu;Bai, Erlei
    • Computers and Concrete
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    • v.20 no.2
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    • pp.205-214
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    • 2017
  • The Hydraulically driven test system and ${\Phi}100mm$ split Hopkinson pressure bar(SHPB) test device were employed to research the quasi-static and dynamic mechanical properties of concrete specimens which has been immersed for 60 days in sodium sulfate (group S1) and sodium chloride (group S2) solution, the evolution of their mass during corrosive period was explored at the same time, and the mechanism of performances lost was analyzed from the microscopic level by using scanning electron microscope. Results of the experimental indicated that: their law of mass both presents the trend of continuous rising during corrosive period, and it increases rapidly on the early days, the mass growth of group S1 and group S2 in first 7 days are 76.78% and 82.82% of their total increment respectively; during the corrosive period, the quasi-static compressive strength of specimens in two groups are significantly decreased, both of which present the trend of increase first and then decrease, the maximum growth rate of group S1 and group S2 are 7.52% and 12.71% respectively, but they are only 76.23% and 82.84% of specimens which under normal environment (group N) on day 60; after immersed for 60 days, there were different decrease to dynamic compressive strength and specific energy absorption, and so as their strain rate sensitivities. So the high salinity environment has a significant effect of weaken the quasi-static and dynamic mechanical performance of concrete.

Effects of Humidity and Velocity on Frost Distribution Characteristics of Humid Air Flow on Cold Surfaces (차가운 표면위에서의 습공기 유동의 습도 및 속도가 착상분포 특성에 미치는 영향)

  • Kwon Jeong-Tae;Rew Keun-Ho;Lim Hyo-Jae;Han Ji-Won;Kwon Young Chul
    • Journal of Energy Engineering
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    • v.14 no.4 s.44
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    • pp.213-218
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    • 2005
  • In order to understand the heat and mass transfer characteristics of humid airflow in frosting conditions, a flat plate of aluminum with cooling modules located in the central part of the plate was used. A microscope system (resolution of 0.05 mm) was used for the measurement of local thickness of frost at seven points along the plate in the flow direction. For the total mass of frost at each test operation, an electronic balance (resolution of 1 mg) was used. The local frost thickness distributions far various test conditions were presented along with the frost mass data measured at the given operating times. The effect of humidity and velocity of humid air on frosting were analyzed.

Detection of Resonance Frequency of Micro Mechanical Devices Using Optical Method and Their Application for Mass Detection (광학적 방법을 통한 마이크로 역학 소자의 공진주파수 측정법과 이를 이용한 마이크로 캔티레버 공진기의 질량 변화 연구)

  • Kim, Hak-Seong;Lee, Sang-Wook
    • Journal of the Korean Vacuum Society
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    • v.21 no.1
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    • pp.36-40
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    • 2012
  • We have developed the detection method of the resonance frequency of micro/nano mechanical resonator using optical method. The optical interferometery method enabled us to detect the displacement change of resonators within several nm scale. The micro mechanical resonator was produced by attaching a micro mechanical cantilever to a piezo ceramic. The mass of cantilever was increased by evaporating Au using electron beam evaporator and the mass variation was estimated by detecting the resonance frequency changes.

AN EXPERIMENTAL STUDY ON MISTLETOE EXTRACT-INDUCED APOPTOSIS IN ORAL SQUAMOUS CELL CARCINOMA (구강편평세포암종에서 미슬토 추출물의 Apoptosis 유도 효과에 대한 실험적 연구)

  • Heo, Gyun-Haeng;Lee, Jae-Hoon;Kim, Chul-Hwan
    • Journal of the Korean Association of Oral and Maxillofacial Surgeons
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    • v.31 no.1
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    • pp.13-23
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    • 2005
  • This study was performed to investigate mistletoe extract-induced apoptosis in oral squamous cell carcinoma. In vivo study, HN22 cells were xenografted in nude mice. After tumor was experimentally induced, mistletoe extract was directly injected on the tumor mass. The specimens were evaluated using light and transmission electron microscopes. In vitro study, HN22 cells were cultured and exposed to mistletoe extract. The cells were evaluated using transmissin electron microscope. To evaluate apoptotic cells, flow cytometric analysis was done. The results were obtained as follows: 1. Light microscopic view of tumor mass showed necrosis at 2-4 weeks. 2. Transmission electron micrographs of tumor mass showed apoptosis and necrosis. 3. In TEM view of cell lines, necrosis and apoptosis were shown with mistletoe extract at $300{\mu}g/ml$, apoptosis was shown with mistletoe extract at $100{\mu}g/ml$. 4. In flow cytometric analysis, early and late apoptosis was shown when using caspase-3Ab and annexin-V, but no significant change was noted when using mebstain and Apo2.7 Ab. In this study, mistletoe extract induced necrosis and apoptosis in the tumor mass was induced by HN22 cells, early and late apoptosis in vitro study. Mistletoe extract was likely to induce cell death in oral squamous cell carcinoma through apoptosis.

A Study on Etching of Si3N4 Thin Film and the Exhausted Gas Using C3F6 Gas for LCD Process (LCD 공정용 C3F6 가스를 이용한 Si3N4 박막 식각공정 및 배출가스에 관한 연구)

  • Jeon, S.C.;Kong, D.Y.;Pyo, D.S.;Choi, H.Y.;Cho, C.S.;Kim, B.H.;Lee, J.H.
    • Journal of the Korean Vacuum Society
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    • v.21 no.4
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    • pp.199-204
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    • 2012
  • $SF_6$ gas is widely used for dry etching process of semiconductor and display fabrication process. But $SF_6$ gas is considered for typical greenhouse gas for global warming. So it is necessary to research relating to $SF_6$ alternatives reducing greenhouse effect in semiconductor and display. $C_3F_6$ gas is one of the promising candidates for it. We studied about etch characteristics by performing Reactive Ion Etching process of dry etching and reduced gas element exhausted on etching process using absorbent Zeolite 5A. $Si_3N_4$ thin film was deposited to 500 nm with Plasma Enhanced Chemical Vapor Deposition and we performed Reactive Ion Etching process after patterning through photolithography process. It was observed that the etch rate and the etched surface of $Si_3N_4$ thin film with Scanning Electron Microscope pictures. And we measured and compared the exhausted gas before and after the absorbent using Gas Chromatograph-Mass Spectrophotometry.

Construction and a Chronological Examination of the Fabrics in the Buddhist (불복장 직물의 구조특성 및 연대규명)

  • Kim, Sun-Kyung;Cho, Hyo-Sook
    • Journal of the Korean Society of Costume
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    • v.55 no.8 s.99
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    • pp.73-84
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    • 2005
  • Collections in the buddhist statue owned by Dr. Jong-Hm Baik(白宗欽) included 3 ancient documents and 2 wooden cylinders that showed a clear historical order. The temple and buddhist statue that these objects were belonged to were not known, however, according to the document, it could be inferred as Chunsukwaneumsang(천수관음상) created in 1322 and reformed in 1614 from the list of donator for the statue. Inside a wooden cylinder, a bundle of ivory, yellow, green, orange, and dark brown fabrics that were folded up and tided up with 5 different colored thread strands and aromatic trees and rice plant was placed on the bottom. All the fabrics were silk. Three thread strands were silk. The white and blue strands were cotton fibers as a result of analysis of IR spectrum and the microscope. According to a radioactive carbon isotope dating by accelerator mass spectroscopy, years before present was 160$\pm$40, and cablibrated ages were 1680-1890 (79.3$\%$), 1910-1960(16.1$\%$) in 95.4$\%$ probability. Accordingly, the fabrics in the buddhist statue proved to be reformed in 1614 not the original ones in 1322.

A Case of Neurilemmoma of the Trachea (기관에 발생한 신경초종 1례)

  • Lee, Keum-Hyung;Kang, Jun-Myung;Park, Young-Hak;Ju, Young-Ha
    • Korean Journal of Bronchoesophagology
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    • v.5 no.2
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    • pp.198-201
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    • 1999
  • Benign tracheal tumors are less common than malignant tumors, but they are relatively more important because they are operable and curable. Neurilemmoma is originated from Schwann cells of nerve sheath, which are characterized by benign, solitary, and encapsulated mass. Tracheal neurilemmomas are extremely rare and reported only 21 cases in the world literature. Recently, we experienced a case of neurilemmoma which arose from the trachea of a 48-year-old female patient who complained of progressive dyspnea. The tumor mass was removed successfully through bronchoscopic and tracheal fissure approach. The final pathological diagnosis viewed under a microscope after H&E stain was a neurilemmoma in which Antoni type A and type B both existed.

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Explosive mass-removal processes during high power nanosecond Nd-YAG laser ablation of silicon (나노초 야그 레이저 어블레이션에 의한 실리콘의 폭발적 제거 현상)

  • Jeong, S.H.;Yoo, J.H.;Grief, R.;Russo, R.E.
    • Proceedings of the KSME Conference
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    • 2000.11a
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    • pp.736-742
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    • 2000
  • Mass removed from crystalline silicon samples during high power single-pulse laser ablation was studied by measuring the resulting crater morphology with a white light interferometric microscope. The volume and depth of the craters show a strong nonlinear change as the laser irradiance increases across a threshold value, that is, approximately $2.2{\times}10^{10}\;W/cm^2$. Time-resolved shadowgraph images of the ablation plume show the ejection of large particulates from the sample for laser irradiance above the threshold, with a time delay of about 300-400 nsec. The thickness of superheated liquid layer near the critical temperature was numerically estimated, considering the transformation of liquid metal into liquid dielectric near the critical state (i.e., induced transparency). The estimated thickness of the superheated layer at a delay time of 200 nsec agreed with the measured crater depths, suggesting that induced transparency promotes the formation of a deep superheated liquid layer which leads to an explosive boiling responsible for the sudden increase of crater volume and depth.

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Basic Research on the Quantitative Estimation of Yellow Sand (黃砂의 量的推定을 위한 基礎硏究)

  • 김동술
    • Journal of Korean Society for Atmospheric Environment
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    • v.6 no.1
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    • pp.11-21
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    • 1990
  • To quantitatively estimate the effect of yellow sand(loess) fromt he Northern China, various soil sources having similar chemical compositions to yellow sands should be separated and identified. After that, mass contribution for yellow sand can be calculated. The study showed that it was impossible to solve this problem by the traditional bulk analyses. However, particle-by-particle analysis by a CCSEM (computer controlled scanning electron microscope) gave enormous potentials to solve it. To perform this study, seven soil source data analyzed by CCSEM were obtained from Texas, U.S.A. Initially, each soil date was classified into two groups, coarse and fine particle groups since the particle number distribution showed a minimum occurring at 5.2$\mu$m of aerodynamic diameter. Particles in each group were then classified into one of the 283 homogeneous particle classes by the universal classification rule which had been built by an expert system in the early study. Further, mass fractions and their uncertainties for each class in each source were calculated by the Jackknife method, and then source profile matrix for the 7 soil sources was created. To use the profile matrix in the study of source contribution, it is necessary to test the degree of collinearity among sources. The profiles were tested by the singular value decomposition method. As a result, each soil source characterized by artificially created variables was totally independent each other and is ready to use in source contribution studies as a receptor model.

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Microstructure Properties of High Strength Concrete Utilizing EVA with Micro Particles (EVA 마이크로 입자를 활용한 고강도 콘크리트의 미세구조특성)

  • Kim, Young-Ik;Sung, Chan-Yong
    • Proceedings of the Korean Society of Agricultural Engineers Conference
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    • 2005.10a
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    • pp.97-101
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    • 2005
  • High strength concretes utilizing EVA with micro particles were prepared by varying polymer/binder mass ratio and curing conditions with a constant water/binder mass ratio of 0.3. The EVA modified concretes on the compressive and flexural strength, microstructure, ultrapulse modulus in curing condition(dry and water curing) were studied. Also, scanning electron microscope analysis(SEM) was performed to reveal the presence of polymer film and cement hydrates in the concrete. The compressive strength of the EVA modified concretes cured at water conditions ere higher than that of the EVA modified concretes cured at dry conditions. But, the flexural strength of the specimens cured at dry conditions were higher than that of the specimens cured at water conditions. Due to the interaction of the cement hydrates and polymer film, an interpenetrating network originated in which the aggregates were embedded. The curing of the polymer modified concrete involves two step of cement hydrates and polymer modification, and cement hydrates was promoted in water conditions and polymer film formation take place when water evaporates and was thereby was favored in dry conditions. By SEM analysis, influences of polymer modification was strengthening of the transition zone between the aggregate and the paste, and the porosity of transition zone decreases. By spring analysis, it could known that polymer film affects in porosity decrease and strengthening of transition zone.

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