• 제목/요약/키워드: mass microscope

검색결과 210건 처리시간 0.029초

NANO-STRUCTURAL AND NANO-CHEMICAL ANALYSIS OF NI-BASE ALLOY/LOW ALLOY STEEL DISSIMILAR METAL WELD INTERFACES

  • Choi, Kyoung-Joon;Shin, Sang-Hun;Kim, Jong-Jin;Jung, Ju-Ang;Kim, Ji-Hyun
    • Nuclear Engineering and Technology
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    • 제44권5호
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    • pp.491-500
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    • 2012
  • The dissimilar metal joints welded between Ni-based alloy, Alloy 690 and low alloy steel, A533 Gr. B with Alloy 152 filler metal were characterized by using optical microscope, scanning electron microscope, transmission electron microscope, secondary ion mass spectrometry and 3-dimensional atom probe tomography. It was found that in the weld root region, the weld was divided into several regions including unmixed zone in Ni-base alloy, fusion boundary, and heat-affected zone in the low alloy steel. The result of nanostructural and nanochemical analyses in this study showed the non-homogeneous distribution of elements with higher Fe but lower Mn, Ni and Cr in A533 Gr. B compared with Alloy 152, and the precipitation of carbides near the fusion boundary.

기상합성법을 이용한 탄소나노튜브의 대량합성 (Mass production of carbon nanotubes using Vapor Phase Growth)

  • 류승철;이태재;이철진
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2001년도 하계학술대회 논문집
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    • pp.123-126
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    • 2001
  • Multiwalled carbon nanotubes were massively produced by the catalytic reaction of C$_2$H$_2$ - Fe(CO)$\sub$5/ mixture at 750 - 950$^{\circ}C$ in a quartz tube reactor and over quartz substrates. Well-aligned MWNT array grows perpendicular to the quartz tube reactor and the quartz substrates at an average of 60 nm in diameter and up to several thousands of micrometers in length. This method does not require any pretreatment of substrates and CNTs are grown at atmospheric pressure. It could be suitable for mass production of multiwalled nanotubes. Scanning electron microscope and transmission electron microscope images of the nanotubes deposited on the substrates allowed us to monitor the quality of MWNTs grown under different operating conditions.

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A Case of Engorged Female Hard Tick in the External Auditory Canal of an Infant

  • Sung, Woo-Jung;Kim, Yee-Hyuk
    • Parasites, Hosts and Diseases
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    • 제55권5호
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    • pp.565-568
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    • 2017
  • An oval-shaped mass with a smooth surface was found in the ear canal of a 22-month-old male infant. Although the mass appeared to be almost entirely blocking the ear canal, it was successfully removed under a surgical microscope without general anesthesia at the outpatient department. Under an optical microscope with hematoxylin and eosin staining, the specimen was observed to have a cuticle with a serrated surface and a pore canal, as well as parts of the capitulum, salivary glands, muscles, midgut, and the legs. The specimen was identified as a hard tick of the family Ixodidae, based on gross and histological findings. This paper is the first report in Korea on the diagnosis and treatment of a tick bite in the ear canal.

Characterizations of Two-step Matrix Application Procedures for Imaging Mass Spectrometry

  • Shimma, Shuichi
    • Mass Spectrometry Letters
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    • 제6권1호
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    • pp.21-25
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    • 2015
  • In this paper, I describe the importance of matrix spraying conditions in imaging mass spectrometry (IMS) to obtain successful imaging results. My developed matrix application methodology, which is a "two-step matrix application" sequentially combined with matrix sublimation and spraying matrix solution can provide high reproducibility and high ion yield compared with a conventional direct spraying method. However, insufficient IMS results were obtained occasionally despite the two-step method. Therefore, I wanted to characterize the methodology to continuously provide high quality data. According to my results, the sublimation time was not a strict parameter, and the most important step was the first spraying condition. This means that the extraction conditions from the tissue section and co-crystallization of the matrix were the most important factors.

음향현미경을 이용한 layer의 두께측정에 관한 연구 (A study on the measurement of layer thickness using acoustic microscope.)

  • 고대식;김흥기;전계석
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 1988년도 전기.전자공학 학술대회 논문집
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    • pp.43-46
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    • 1988
  • In this paper, a methodology for determination of the thickness of layer on a substrate using reflection acoustic microscope has been presented. It has been shown that the amplitude and the phase of reflection coefficient of the layer-substrate composite has been used for measurement of layer thickness, acoustic velosity, mass density of the layer material. The reflection acoustic microscope operating at a frequency of 15 MHz has been used for the experiment and the measured acoustic impedance value for aluminum sample has agreed with the published data, and the measured layer thickness for silver-glass composite has agreed with that measured using micrometer.

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은 박막이 코팅된 표면에서 물질전이층의 형성 및 그 트라이볼로지적 역할에 관한 연구 (A Study on the Formation and the Tribological Role of Mass Transfers Layers at Rubbing Silver-coated Surface)

  • 공호성;양승호;윤의성;김대은
    • Tribology and Lubricants
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    • 제18권6호
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    • pp.377-383
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    • 2002
  • The tribological role of mass transfer layer was studied with silver coatings under various ranges of load and sliding speed. Silver coating was performed with a functionally gradient coating method. Tests were per-formed in dry sliding conditions, using a ball-on-disk contact configuration, at the load of 0.0196-17.64 N and the sliding speed of 20-1,000 mm/s in ambient air. Optical microscope and EPMA analyses showed that contact surfaces were covered with the mass transfer layers of agglomerated wear particles depending upon the contact conditions, and they greatly influenced the tribological characteristics of the surfaces. However, the formation of mass transfer layer was suppressed as the sliding speed increased, and above a critical sliding speed, no mass transfer layer was able to form. For building up a general framework of triboiogical behavior of the coated silver films, all test data were summarized on a map whose axes are contact pressure and sliding speed.

심장내 발생한 원발성 지방종 1례 보고 (Primary Lipoma of the Heart -A Case Report-)

  • 정일영
    • Journal of Chest Surgery
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    • 제27권4호
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    • pp.310-312
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    • 1994
  • Primary cardiac lipoma is an extremely rare condition. We reports a case of primary lipoma located mainly in the right atrium of the heart in a 58-year-old male patient. The initial presenting symptoms were dyspnea followed by rapidly progress!ve congestive heart failure. Echocardiogram revealed huge mass on right atrium with stalk arising from septum. Under cardiopulmonary bypass the mass was removed and revealed characteristic findings of lipoma on microscope. The patient was recovered without any problem. We would like to describe this case of rare tumor with the review of literatures.

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하동일산청지역(河東一山淸地域)의 아노르도사이트의 성인(成因)에 관(關)하여 (On the Origin of Anorthosite in the Area of Hadong, Sancheong, Gyeongsang-namdo, Korea)

  • 손치무;정지곤
    • 자원환경지질
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    • 제5권1호
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    • pp.1-20
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    • 1972
  • A large anorthositic mass outcropped as mushroom-like body extending up to 46km which occurs in the Hadong kaoline district of southern Korea. The anorthositic mass is in contact with the metamorphic, plutonic and sedimentary rocks. The metamorphic rocks are of granitic gneiss and banded gneiss, etc; the plutonic rocks are of gabbroic and dioritic rocks, schistose granite, syenite, diorite and granite. The sedimentary rocks include siltstone and pebbly sandstone of Lower Gyeongsang System, Cretaceous in age. The anorthositic mass shows a gradational contact with the metamorphic and sedimentary rocks, and is cut by the plutonic rocks except gabbroic and dioritic rocks. The anorthositic mass is leucocratic in the central portion of the mass, and, in turn, grades to rock phases in which ma/ic minerals are irregularly scattered, then to the well-lineated rock and finally to the banded gneiss. Lineation of the anorthositic mass is accordant with that of the surrounding banded gneiss, and the lineation continues toward the gneiss. In some places, the rock phases in which mafics are scattered is gradational with adjacent sedimentary rocks. The anorthositic mass in contact with gabbroic and dioritic rocks shows spotted features. Various replacement features seen under the microscope and paragenetic sequence of the mineral components in the anorthositic rocks cannot be considered as the origin of magmatic crystallization. From the field and microscopic observations, it is concluded that the anorthositic mass was formed from replacement of the metamorphic rocks and plutonic rocks by the anorthositic magma.

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Inhibition of Klebsiella pneumoniae ATCC 13883 Cells by Hexane Extract of Halimeda discoidea (Decaisne) and the Identification of Its Potential Bioactive Compounds

  • Supardy, Nor Afifah;Ibrahim, Darah;Sulaiman, Shaida Fariza;Zakaria, Nurul Aili
    • Journal of Microbiology and Biotechnology
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    • 제22권6호
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    • pp.872-881
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    • 2012
  • The inhibitory effect of the Klebsiella pneumoniae ATCC 13883 strain caused by the hexane extract of Halimeda discoidea (Nor Afifah et al., 2010) was further evaluated by means of the microscopy view and its growth curves. The morphological changes of the K. pneumoniae ATCC 13883 cells were observed under the scanning electron microscope (SEM) and transmission electron microscope (TEM) after they were treated at minimum inhibitory concentration (MIC; 0.50 mg/ml) (Nor Afifah et al., 2010) for 12, 24, and 36 h. The results showed the severity of the morphological deteriorations experienced by the treated cells. The killing curve assay was performed for 48 h at three different extract concentrations (1/2 MIC, MIC, and 2 MIC). An increase in the extract concentration of up to 2 MIC value did significantly reduce the number of cells by approximately 1.9 $log_{10}$, as compared with the control. Identification of the potential compounds of the extract responsible for the antibacterial activity was carried out through the gas chromatography-mass spectrum (GC-MS) analysis of the active subfraction, and the compound E-15-heptadecenal was identified and suggested as the most potential antibacterial compound of this extract. The subsequent cellular degenerations showed by the data might well explain the inhibitory mechanisms of the suggested antibacterial compound. All of these inhibitory effects have further proven the presence of an antibacterial compound within H. discoidea that can inhibit the growth of K. pneumoniae ATCC 13883.

A Case of Brachial Plexus Schwannoma

  • Kim, Young-Woo;Ahn, Sung-Ki;Song, Joon-Ho
    • Journal of Korean Neurosurgical Society
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    • 제39권5호
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    • pp.396-399
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    • 2006
  • Brachial plexus schwannoma is rare. A case of a 28-year old woman who complained of a palpable mass in the right axilla is presented. She had previous incisional biopsy on the axillary mass. Brachial plexus magnetic resonance imaging revealed a well circumscribed contrast enhancing mass on the right distal cord of the brachial plexus. EMG revealed normal. Tumor resection was performed with the transaxillary approach. Though dense granulation tissue obscured normal brachial plexus nerve anatomy, using the surgical microscope and nerve stimulator, grossly total tumor resection was performed. She is free of any neurologic symptom at three months postoperatively.