• Journal of the Korean Ceramic Society
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• v.34 no.6
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• pp.601-610
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• 1997

In cofiring of multilayered alumina with tungsten, the change of camber with lamination condition was experimented and the effect of sintering shrinkage of alumina and tungsten was investigated. From the exact measurement of sintering shrinkage of tungsten thick film, as lamination pressure increased, the sintering shrinkage of alumina decreased but that of tungsten thick film was not changed. So it was though that the main factor which induced the sintering shrinkage difference between ceramics and metal with lamination condition was the change of sintering shrinkage of ceramics. In case of high lamination pressure, high green sheet density, the cofired specimen showed low camber due to low shrinkage difference between alumina and tungsten and there was a linear relation between camber and shrinkage difference. It was found that this shrinkage difference could change the thickness of tungsten film and the microstructure within via hole during cofiring.

• Journal of the Korean Ceramic Society
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• v.19 no.3
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• pp.241-249
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• 1982

Two dinnerware porcelain bodies involving partial replacement of feldspar and kaoline by about 35wt% domestic GYUNGJU-pottery stone were developed and their properties such as shrinkage, porosity, firing range, linear thermal expansion, pyroplastic deformation, degree of whiteness and mechanical strength were compared with those of a traditional clay-flint-feldspar body. The experimental results showed that one of the clay-flint-feldspar-pottery stone body with 1% ZnO addition had the firing range of 115$0^{\circ}C$~121$0^{\circ}C$, whereas the traditional body had the firing range of 12$25^{\circ}C$~129$0^{\circ}C$. The linear drying shrinkage and linear dry-to-fired shrinkage of all bodies were 2.5~4.5% and 15~18%, respectively. And the major crystalline phases of sintered bodies were $\alpha$-quartz and secondary mullite surrounded by glassy phases. The modulus of rutpture of sintered bodies was ranged from 860 to 870kg/$\textrm{cm}^2$, and the microhardness of sintered bodies was 680 kg/$\textrm{cm}^2$.

• Journal of the Korea Institute of Building Construction
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• v.4 no.2
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• pp.81-88
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• 2004

The purpose of this study is to investigate the chemical shrinkage and autogenous shrinkage of high strength cement paste and silica fume and fly ash and sand to cement ratio by the method of volumetric tests, and also investigate the autogenous shrinkage of high measurement method, and compare the results of volumetric test and linear length measurement test. A series of cement paste which have W/C ratio of 25%, 35%, 45% respectively were planed to study the effect of the W/C ratio to the shrinkages, and a series of cement paste which were replaced the cement by the silica fume and fly ash with 5%, 10%, 15% as the mass of cement respectively were planed to investigate the effects of poazolana to the shrinkages. A series of mortar which have a C/S ratio of 1:1, 1:1.5, 1:2 respectively were planed to investigate the shrinkage resistant effect of aggregate.

• Restorative Dentistry and Endodontics
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• v.27 no.5
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• pp.488-492
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• 2002

The purpose of this study was to evaluate the effectiveness of plasma arc curing (PAC) unit for composite and compomer curing. To compare its effectiveness with conventional quartz tungsten halogen (QTH) light curing unit, the polymerization shrinkage rates and amounts of three composites (Z100, Z250, Synergy Duo Shade) and one compomer, that had been light cured by PAC unit or QTH unit, was compared using a custome made linometer. The measurement of polymerization shrinkage was peformed after polymerization with either QTH unit or PAC unit. In case of curing with the PAC unit, the composite was light cured with Apollo 95E for 6s, the power density of which was recorded as 1350 mW/$\textrm{cm}^2$ by Coltolux Light Meter. For light curing with QTH unit, the composite was light cured for 30s with the XL2500, the power density of which was recorded as 800 mW/$\textrm{cm}^2$ by Coltolux Light Meter. The amount of linear polymerization shrinkage was recorded in the computer every 0.5s for 60s. Ten measurements were made for each material. The amount of linear polymerization shrinkage for each material in 10s and 60s which were cured with PAC or QTH unit were compared with t test. The amount of polymerization shrinkage in the tested materials were compared with 1way ANOVA with Duncan's multiple range test. As for the amounts of polymerization shrinkage in 60s, there was no difference between PAC unit and QTH unit in Z250 and Synergy Duo Shade. In Z100 and Dyract AP, it was lower when it was cured with PAC unit than when it was cured with QTH unit (p<0.05). As for the amounts of polymerization shrinkage in 10s, there was no difference between PAC unit and QTH unit in Z100 and Dyract AP. The amounts of polymerization shrinkage was significantly higher when it was cured with PAC unit in Z250 and Synergy Duo Shade (p<0.05). The amounts of polymerization shrinkage in the tested materials when they were cured with QTH unit were Z250 (6.6um) < Z100 (9.3um), Dyract AP (9.7um) < Synergy Duo Shade (11.2um) (p<0.05). The amount of polymerization shrinkage when the materials were cured with PAC unit were Dyract AP (5.6um) < Z100 (8.1um), Z250(7.0um) < Synergy Duo Shade (11.2um) (p<0.05).

• Journal of the Korean Wood Science and Technology
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• v.33 no.3 s.131
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• pp.38-44
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• 2005

This research investigated the variation of density, the weight loss, dimensional shrinkage and heat conduction by the heating rate and keeping time at maximum temperature of woodceramics, when sawdust boards made from thinned logs of Pinus densiflora, Larix kaemferi and Pinus koraiensis were impregnated with phenol-formaldehyde resin, and then were formed by heating rate ($2^{\circ}C/min{\sim}6^{\circ}C/min$) and keeping time at maximum temperature (1~5 h). As the heating rate increased, the density and thickness shrinkage decreased, but weight loss and linear shrinkage increased. The more the keeping time at maximum temperature, the greater the linear shrinkage and thickness shrinkage. The heating conduction was superior at the heating rate is $2^{\circ}C/min$ and the keeping time at maximum temperature of 2 hs.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2000.05a
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• pp.808-811
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• 2000

The product of stereolithography is consist of gathering the single strand. Therefore the accuracy of the shape is related to the linear shrinkage of the single strand. The resin temperature change affect on curing properties. This article will propose the interaction between material temperature and shape accuracy by resin temperature control. The main concern of this article is related to the improvement of end product's shape accuracy by the persuit for the filles curing criterion.

• Korean Journal of Materials Research
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• v.33 no.12
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• pp.537-549
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• 2023

The sintering shrinkage behaviors of low temperature cofired ceramics (LTCC) and resistors were compared using commercial LTCC and thick-film resistor pastes, and factors influencing the camber of cofired resistor/LTCC bi-layers were also investigated. The onset of sintering shrinkage of the resistor occurred earlier than that of LTCC in all resistors, but the end of sintering shrinkage of the resistor occurred earlier or later than that of LTCC depending on the composition of the resistor. The sintering shrinkage end temperature and the sintering shrinkage temperature interval of the resistor increased as the RuO₂/glass volume ratio of the resistor increased. The camber of cofired resistor/LTCC bi-layers was obtained using three different methods, all of which showed nearly identical trends. The camber of cofired resistor/LTCC bi-layers was not affected by either the difference in linear shrinkage strain after sintering between LTCC and resistors or the similarity of sintering shrinkage temperature ranges of LTCC and resistors. However, it was strongly affected by the RuO₂/glass volume ratio of the resistor. The content of Ag and Pd had no effect on the sintering shrinkage end temperature or sintering shrinkage temperature interval of the resistor, or on the camber of cofired resistor/LTCC bi-layers.

• Restorative Dentistry and Endodontics
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• v.19 no.1
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• pp.135-147
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• 1994

This study was conducted to evaluate whether the fatigue toughness of visible light cured composite resins could be improved and how much percentage of polymerzation shrinkage could be affected by additional heat treatment. 7 materials were investigated for this study: P-50, Lite-fil CR inlay, Pekafil, Clearfil CR inlay, Clearfil photo posterior, Z -100 and Progress. Diametral tensile strengths and linear shrinkages of composite resins were taken under visible light cured and additional post-cure heated condition and compared each other. A fatigue toughness of above materials was evaluated by measuring diametral tensile strength after they were repeatedly loaded with 120kgf/$cm^2$ up to 3000 cycles. The results obtained were as follows : 1. When composite resins were cured just by visible light, Lite fil CR inlay, Z -100 and Progress showed respectively higher diametral tensile strength than the other materials. Clearfil CR inlay, Clearfil photo posterior and Progress exhibited strong fatigue toughness compared to P-50 and Pekafil. 2. Post-cure heat treated composite resins had higher diametral tensile strengths than visible light cured composite resins at fatigue toughness test as well as no fatigue toughness test. 3. When Composite resins were additionally polymerized by post-cure heat treatment, P-50 showed weak fatigue toughness, on the contrary, Clearfil CR inlay, Z-100, Progress showed strong one. 4. When composite resins were cured just by visible light, percentage of polymerization linear shrinkage was the lowerest in Clearfil CR inlay, followed by, in ascending order, Clearfil photo posterior, Lite-fil CR inlay, Progress, Pekafil, P-50, and Z-100. In the case of post- cure heat treated composite resins, percentage of linear shrinkage was the lowest in Clearfil photo posterior, followed by, in ascending order, Lite-til CR inlay, Clearfil CR inlay, Progress, P-50, Pekafil and Z-100. 5. Percentage of polymerization linear shrinkage was greater in the post-cure heat treated composite resins than in the visible light cured composite resins and linear shrinkage increased significantly in Pekafil, Clearfil CR inlay, and Clearfil photo posterior between at the visible light cured and at the post-cure heat treated condition. The above results is saying that additional post-cure heat treatment on the composite resins for posterior restoration is able to affect on improvement of strength and fatigue toughness and lead to increase polymerization of composite resins.

• Restorative Dentistry and Endodontics
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• v.28 no.4
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• pp.354-359
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• 2003

This study evaluated the effectiveness of the light emitting diode(LED) units for composite curing. To compare its effectiveness with conventional quartz tungsten halogen (QTH) light curing unit. the microhardness of 2mm composite. Z250, which had been light cured by the LEDs (Ultralume LED2, FreeLight, Developing product Dl) or QTH (XL 3000) were compared on the upper and lower surface. One way ANOVA with Tukey and Paired t-test was used at 95% levels of confidence. In addition. the amount of linear polymerization shrinkage was compared between composites which were light cured by QTH or LEDs using a custom-made linometer in 10s and 60s of light curing, and the amount of linear polymerization shrinkage was compared by one way ANOVA with Tukey. The amount of polymerization shrinkage at 10s was XL3000 > Ultralume 2. 40. 60 > FreeLight, D1 (P<0.05) The amount of polymerization shrinkage at 60s was XL3000 > Ultralume 2, 60> Ultralume 2.40 > FreeLight, D1 (P<0.05) The microhardness on the upper and lower surface was as follows ; (equation omitted) It was concluded that the LEDs produced lower polymerization shrinkage in 10s and 60s compared with QTH unit. In addition. the microhardness of samples which had been cured with LEDs was lower on the lower surfaces than the upper surfaces whereas there was no difference in QTH cured samples.

• Journal of the Korean Ceramic Society
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• v.16 no.1
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• pp.31-37
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• 1979

The middle point of composition within the system $MgO-Al_2O_3-SiO_2$ has been studied for applicability as ceramics dielectrics. A Kyul Sung Tale of high purity, magnesia clinker of Sam-wha chemical company, C.P. aluminium oxide, calcium carbonate, red lead, barium carbonate which was made into frit were used the raw materials. A number of steatite ceramics were prepared under carefully controlled condition and the water absorption, linear shrinkage, power factor, dielectric constant and dielectric loss were measured at elevated temperature. When we used magnesia clinker as flux, the quantity of this flux was 0.05mole, sintering temperature was continued for 2 hrs. at 1, 27$0^{\circ}C$. From this conditions, we could get the data whose power factor was 0.142%, water absorption was zero, linear shrinkage was 8.76%, dielectric constant was 5.63, dielectric loss was 0.00799. When we used red lead as flux, the quantity of this flux was 0.033mole and 0.066mole, sintering temperature was continued for 2hrs. at 1, 26$0^{\circ}C$. From this conditions, we could get the data whose water absorption was zero, linear shrinkage was 8.03%, and 8.48%, power factor was 0.136% and 0.062%, dielectric loss was 0.0072 and 0.0037. When we used barium carbonate made into frit as flux, the quantity of this flux was 0.02mole, sintering temperature was continued for 2hrs. at 1, 27$0^{\circ}C$. From this conditions, we could get the data whose water absoption was zero, linear shrinkage was 8.44%, power factor was 0.138%, dielectric constant was 5.69, dielectric loss was 0.0074.