• Title/Summary/Keyword: iso4

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GC/MS-SIM for the Determination of Alkylphenols, Chlorophenols and Bisphenol A in Paper Materials

  • Kim, Hyub
    • Proceedings of the Korea Society of Environmental Toocicology Conference
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    • 2003.05a
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    • pp.145-145
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    • 2003
  • A method for the determination of alkylphenols, chlorophenols and bisphenol A in paper materials using GC/MS-SIM has been developed. Eleven endocrine disrupting chemicals (EDCs) of phenols in paper samples were extracted with acetonitrile. Also, solid-phase extraction (SPE) with XAD-4 and subsequent conversion to isobutoxycarbonyl derivatives or tert.-butyldimethylsilyl derivatives for sensitive analysis with the selected ion-monitoring (SIM) mode. The recoveries were 82.4∼108.8 % by area ratio of pheranthrene-d$\sub$10/ vs bisphenol A d$\sub$l6/. (isoBOC derivatization and TBDMS derivatization) The SIM responses were linear with the correlation coefficient varying 0.9717∼0.9995 (isoBOC derivatization), and 0.9842∼0.9980 (TBDMS derivatization). The range of concentrations was respectively, 0.95∼l.44 ng/g in 2,4-dichlorophenol, 1.01∼1.17 ng/g in t-butylphenol, 2.17∼5.84 ng/g in pentachlorophenol, 12.68∼14.88 ng/g in nonylphenol and 30.84∼153.72 ng/g in bisphenol A.

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Liquid Adsorption Characteristics on Surface-treated Natural Zeolite (표면처리된 천연 제올라이트의 액체흡착 특성)

  • 이재영;이홍기;이주성;심미자;김상욱
    • Journal of the Korean institute of surface engineering
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    • v.26 no.6
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    • pp.285-290
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    • 1993
  • A series of samples were prepared by treating natural zeolite from Kampo area with HCl and NaOH. And, the adsorption characteristics of some liquid samples were investigated by the Diamond-Kinter method. The adsorption amount of all liquid investigated was more effective in acid treatment than in alkali treatment. In the case of n-, iso-C3H7OH, thed adsorption amount of n-form which has smaller molecular size was larger. Similar tenedncy was observed in n-, iso-C4H9OH, but the amount was lower than n-, iso-C3H7OH. In CHCl3 and CCl4, that of CHCl, which is smaller molecular size and has polarity, was far lager. From the view of the molecular size, adsorption amount of C6H5CH3 and p-C6H4(CH3)2 showed the characteristics of surface activity rather than chemical treatment.

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Quality Characteristics in Mash of Takju Prepared by Using Different Nuruk during Fermentation (누룩 종류를 달리하여 담금한 탁주 발효과정중 술덧의 품질특성)

  • Han, Eun-Hey;Lee, Taik-Soo;Noh, Bong-Soo;Lee, Dong-Sun
    • Korean Journal of Food Science and Technology
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    • v.29 no.3
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    • pp.555-562
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    • 1997
  • The characteristics of mash qualities of takju prepared by using different nuruk (Korean-style bran koji) such as Mucor racemosus nuruk, Rhizopus japonicus nuruk, Aspergillus oryzae nuruk, Aspergillus kawachii nuruk and traditional nuruk were investigated during fermentation. At the begining of fermentation, ethanol content was in the range of $2.0{\sim}3.0%$. However, it increased to $8.2{\sim}12.6%$ after 16 days of fermentation. Takju made from Rhizopus japonicus nuruk showed higher ethanol content than treated otherwise. pH of takju made from Rhizopus japonicus nuruk showed higher value the others. Total acids were $0.15{\sim}0.20%$ at the begining of fermentation, and it increased to $0.086{\sim}1.57%$ after 16 days of fermentation. Total sugar were $16.64{\sim}17.62%$ at the begining of fermentation, but decreased to below 7.00% after 16 days of fermentation. Rhizopus japonicus nuruk showed the lowest level of total sugar content. Except ethanol, iso-amyl alcohol and iso-butyl alcohol were major part of minor alcohol in the mash of takju. Higher concentration of iso-amyl alcohol, iso-butyl alcohol and n-propyl alcohol were found in the mash of Rhizopus japonicus nuruk whereas the level of phenylethyl alcohol was high in the mash of traditional nuruk. Fusel oil was $0.002{\sim}0.411\;mg/mL$ during fermentation.

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The Fundamental Study on the Development of Leisure Boat's Drop Test Management System based on ISO 12215-5 (ISO 12215-5에 기반 한 레저선박 낙하시험 평가시스템 개발을 위한 기초연구)

  • Kang, Nam-Seon;Park, Chung-Hwan
    • Journal of the Korean Society of Marine Environment & Safety
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    • v.18 no.4
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    • pp.365-370
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    • 2012
  • International Organization for Standardization has recently published ISO 12215-5 which is the small craft-hull construction and scantling. According to ISO 12215-5 AnnexB, the scantling determination can be accomplished by drop test for craft with a length $L_H$ of 2.5m up to 6m and single-skin construction. The current method, however, of visual test has the issue where it is difficult to make an objective evaluation of ship body strength. In this study, in order to develop an evaluation system that can make a quantitative evaluation of the drop test of leisure boats, the domestic/foreign regulations on drop test of leisure boats are analyzed and the drop test evaluation system is designed, and the system applicability is reviewed through 5-meter level aluminum ship, and the issues incurred by the state of the ship and the posture while dropping were checked.

Evaluation of volatile organic compounds emitted from door-trim armrest using micro chamber and 20 L static chamber (마이크로 챔버와 20 L static chamber를 이용한 도어트림 암레스트로부터 방출되는 휘발성 유기화합물 평가)

  • Lee, Ik-Hee;Yoo, Ji-Ho;Kim, Man-Goo
    • Analytical Science and Technology
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    • v.24 no.4
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    • pp.290-297
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    • 2011
  • In present, evaluation method for car cabin air quality has been developed in ISO, China, Japan. Also The management standard for new produced car has been applied since 1, July, 2010. To manage car cabin air quality, It is important to evaluate VOC emitted from interior material. In this study, complete component of door trim armrest was evaluated in accordance with ISO 12219-5, cut component was evaluated in accordance with ISO 12219-3. The vapour gas was collected with stainless tube packed with Tenax TA and analyzed with TD-GC/MS. It was confirmed that emission rate of each compounds was difficult in each evaluation method. As a result, to evaluating each components composing door trim armrest, main sources of emitting VOCs in door trim armrest were PP substrate and adhesive.

Design of an NMOS Current-Mirror Type Bridge Rectifier for driving RFID chips (RFID 칩 구동을 위한 NMOS 전류미러형 브리지 정류기의 설계)

  • Park, Kwang-Min;Hur, Myung-Joon
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.9 no.2
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    • pp.333-338
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    • 2008
  • In this paper, a new NMOS current-mirror type bridge rectifier for driving RFID chips, whose minimum input voltage required to obtain the effective DC output voltage is low enough and whose power dissipation can be reduced than that of conventional one, is proposed. The designed rectifier is able to supply high enough and well-rectified DC voltages to drive RFID transponder chips for the frequency range of 13.56 MHz HF(for ISO 18000-3), 915 MHz UHF(fur ISO 18000-6), and 2.45 GHz microwave(for ISO 18000-4). Output characteristics of the proposed rectifier are analyzed with the high frequency equivalent circuit. And the circuitry method for effective reducing of the gate leakage current due to the increasing of operating frequency is also proposed theoretically. Using this method, the power consumption of $100\;{\mu}W$ and the DC output voltage of 2.13V for 3V peak-to-peak input voltage and $45\;K{\Omega}$ load resistance are obtained. Compared to conventional one, the proposed rectifier operates in more stable and shows superior characteristics in UHF and microwave frequencies.

Development of the SQL/MM Standard for Metadata Registries (메타데이터 레지스트리를 위한 SQL/MM 표준 개발)

  • Jeong, Dong-Won;Jeong, Hye-Jin;Kim, Jang-Won;Jeon, Keun-Hwan;Shin, Shin-Ae
    • Journal of the Korea Society of Computer and Information
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    • v.15 no.9
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    • pp.9-18
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    • 2010
  • Standards for various multimedia and application fields have been developed, and the standardization for the multimedia and applications have been making as ISO/IEC 13249 packages by ISO/IEC JTC 1/SC 32/WG 4. This paper describes SQL/MM part 8, which is currently being standardized for providing consistent access support to metadata registries. Systems for ISO/IEC 11179 - metadata registries, the international standard, have been realized and utilized in various fields. However, there is no standardized query processing to share and exchange information between the systems, and thus it causes many problems. Therefore, SQL/MM part 8 described in this paper resolves these problems as well as makes users easily understand it.

Improving Inspection Systems for Radio Stations: An Emphasis on the ISO 2859-1 Sampling Method (무선국 검사제도 개선방안에 관한 연구: ISO 2859-1 샘플링 검사기법을 중심으로)

  • Hyojung Kim;Yuri Kim;Sina Park;Seunghwan Jung;Seongjoon Kim
    • Journal of Korean Society for Quality Management
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    • v.51 no.4
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    • pp.515-530
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    • 2023
  • Purpose : This research aims to develop a data-driven inspection policy for radio stations utilizing the KS Q ISO 2859-1 sampling method, addressing potential regulatory relaxations and impending management challenges. Methods : Using radio station inspection big data from the past six years, we established a simulation model to evaluate the current policy. A new inspection sampling policy framework was designed based on the KS Q ISO 2859-1 method. The study compares the performance of the current and proposed inspection systems, offering insights for an improved inspection strategy. Results : This study introduced a simulation model for inspection system based on the KS Q ISO 2859-1 sampling method. Through various experimental designs, key performance indicators such as non-detection rate and sample proportion were derived, providing foundational data for the new inspection policy. Conclusion : Using big data from radio station inspections, we evaluated current inspection systems and quantitatively compared a new system across diverse scenarios. Our simulation model effectively verified the feasibility and efficiency of the proposed framework. For practical implementation, essential factors such as lot size, inspection cycle, and AQL standards need precise definition and consideration. Enhancing radio station inspections requires a policy-driven approach that factors in socio-economic impacts and solicits feedback from industry participants. Future study should also explore various perspectives related to legislative, institutional, and operational aspects of inspection organizations.

Field Tests for Accuracy of GNSS-RTK Surveys by ISO 17123-8 Standard (ISO 17123-8 표준에 의한 GNSS-RTK 수신기 정확도 평가)

  • Lee, Hungkyu
    • Journal of the Korean Society of Surveying, Geodesy, Photogrammetry and Cartography
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    • v.40 no.4
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    • pp.333-342
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    • 2022
  • This paper has theoretically and practically reviewed the ISO (International Standard Organization) 17123-8 standard not only to raise the appropriateness for introducing performance criteria of GNSS (Global Navigation Satellite Systems) surveying equipment based on RTK (Real-Time Kinematic) accuracy but also to derive its proper test procedure by introducing the international standard. Field experiments have been performed to appreciate the GNSS-RTK accuracy of five selected receivers via the full testing procedure of the ISO standard, which statistically compares the so-called experimental standard deviations with themselves and with the reference accuracy. A series of statistical tests have revealed that the RTK accuracy of the same class receivers is not identical, whereas that of the different classes can be equivalent. Such a result evidences the urgency of adopting an RTK accuracy-based specification of the GNSS equipment to the performance standard, currently referenced to the static observation technique only. It is believed that this transition helps the maximization of a new generation of cost-effective receivers to legal surveying applications. Finally, this study proposes the ISO full test, comparing an experimental standard deviation with its referenced value, for a potential field verification procedure of the new performance standard.

CC 3.0의 변화 내용 분석

  • 강연희;김정대;최상수;이강수
    • Review of KIISC
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    • v.15 no.4
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    • pp.80-96
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    • 2005
  • ISO/IEC ISO/IEC 15408인 CC(Common Criteria)는 전세계 정보보호 학계와 산업 분야에서 정보보호 기능과 보증에 대한 표준적 개념, 평가 및 분류체계로 자리매김했다. 현재의 공식적인 버전은 CC 2.2이지만, 2004년 3월에 CC 2.4(초안)가 발표된 후, 공식버전이 되기도 전인 2005년 7월에 CC 3.0 (초안, 수정 2판)이 발표되었다. CC 3.0은$50\%$이상 대폭 변화되었으며 지난 10년간 경험했던 CC의 문제점을 해결하려한 흔적이 역역하다. 본 논문에서는 CC 3.0의 변화를 CC 2.4와 함께 조사 및 분석하였고 변화에 따른 문제점과 대책을 제시한다.