• Title/Summary/Keyword: infiltration method

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Fabrication of Ceramic 3D Integration Technology for Ink-jet Printing (Ink-jet Printing을 이용한 3D-Integration 구현)

  • Hwang, Myung-Sung;Kim, Ji-Hoon;Kim, Hyo-Tae;Yoon, Young-Joon;Kim, Jong-Hee;Moon, Joo-Ho
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2010.06a
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    • pp.332-332
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    • 2010
  • We have successfully demonstrated the inkjet printing method to create $Al_2O_3$ films withouWe have successfully demonstrated the inkjet printing method to create $Al_2O_3$ films without a high temperature sintering process. In order to remove the coffee ring effect in the ink drop, we have introduced a co-solvent system in order to create Marangoni flow in the ink drop, which leads to the dense packing of ceramic powders on the substrate during inkjet process. The packing density of the Inkjet-printed $Al_2O_3$ films is around 60% (max. 70%) which is very high compared to the value obtained from the same material films by other conventional methods such as film casting, dip coating process, etc. The voids inside the films (which are around 40% of the entire film volume) are filled with the polymer resin (Cyanate ester) by the infiltration process. This resin infiltration is also implemented by the inkjet printing process right after the Ah03 film ink-jetting process. The microstructures of the printed $Al_2O_3$ films are investigated by Scanning Electron Microscope (SEM) to understand the degree of packing density in the printed films. The inkjet-printed $Al_2O_3$ films have been characterized to investigate its thickness and roughness. Quality factor of the printed $Al_2O_3$ film is also measured to be over 300 at 1MHz.

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Fabrication of SiC Converted Graphite by Chemical Vapor Reaction Method(II) (화학적 기상 반응법에 의한 탄화규소 피복 흑연의 제조(II))

  • 윤영훈;최성철
    • Journal of the Korean Ceramic Society
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    • v.36 no.1
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    • pp.21-29
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    • 1999
  • The effects of density and pore size distribution of substrate in preparing SiC conversiton layer on graphite substrate were investigated. The chemical reaction for formation of SiC conversion layer was occurred at substrate surface or below surface through SiC gas infiltration. It was supposed that the pore size distribution required for the sufficient SiO gas infiltration and the continuous chemical reaction during conversion process was in the range of 1.0∼10.0$\mu\textrm{m}$. In the stress analysis of SiC layer with finite element method (FEM), the residual stress distribution due to thermal mismatch was shown. However, the compressive stress was measured in SiC layer by X-ray diffraction, it was presumed that the residual stress distribution of SiC layer was mainly influenced by the constraining effect of interlayer between SiC layer and graphite substrate, and the densification behaviro and the grain growth in SiC conversion layer.

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Creep Properties of Squeeze Infiltrated AS52 Mg/Al18B4O33w Composite (용탕가압침투 AS52 Mg/Al18B4O33w 복합재료의 크리프 특성)

  • Choi, Kye-Won;Park, Yong-Ha;Park, Bong-Gyu;Park, Yong-Ho;Park, Ik-Min;Cho, Kyung-Mox
    • Korean Journal of Metals and Materials
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    • v.46 no.7
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    • pp.412-419
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    • 2008
  • Creep behavior of the squeeze infiltrated AS52 Mg matrix composites reinforced with 15 vol% of aluminum borate whiskers($Al_{18}B_4O_{33}w$) fabricated squeeze infiltration method was investigated. Microstructure of the composites was observed as uniformly distributed reinforcement in the matrix without any particular defects of casting pores etc.. Creep test was carried out at the temperature of 150 and $200^{\circ}C$ under the applied stress range of 60~120 MPa. The creep resistance of the composite was significantly improved comparing with the unreinforced AS52 Mg alloy. The creep behavior of composites might be interpreted with the substructure invariant model successfully for the composite. Threshold stress of the composite exist for the creep deformation of the composite. The analysis of the creep behavior of the composite with threshold stress indicated that creep deformation was controlled by the lattice diffusion process of AS52 Mg matrix at given effective stresses and temperatures. Activation energy was also calculated to check lattice diffusion controlled creep behavior of the composite.

Experimental Study of Direct Metal Prototyping Prcess (금속재료를 이용한 직접식 3차원 형상제조공정의 실험적 연구)

  • 신민철;손현기;양동열
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 1994.10a
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    • pp.169-175
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    • 1994
  • This study attempts to develop a process which can produce three-dimensional shapes of metals directly from CAD data. Prototypes made from metals, can not only be used to test the mecchanical properties of the product, but also potentially become the actual die or product itself. The test-device of the process has been designed and manufactured. The laser scanning method using a scanning path schedule composed of circle and arc elements, scanning speed variation method and dwell method have been developed, which resist warping phenomenon and increase the adhesiveness between the layers. For the production of prototypes with pure iron powder, the optimal values of the principal process parameters have been determined, through which cross-shaped and twisted clover-shaped prototypes have been fabricated. In order to improve the strength of the prototype, the experimental studies of solid-phase sintering, and copper infiltration have been done.

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A Study on Sealant Evaluation and Effectiveness of Saw and Seal Method for Reducing Reflection Cracking (반사균열 저감을 위한 Saw and Seal 공법의 줄눈재 평가 및 효과에 관한 연구)

  • Seo, Yong-Hwan;Suh, Young-Chan;Bae, Jong-Oh;Chon, Beom-Jun
    • International Journal of Highway Engineering
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    • v.14 no.4
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    • pp.73-81
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    • 2012
  • PURPOSES : The purpose of this study is to select the proper sealing method and to see the performance of the saw and seal method for concrete rehabilitation based on accelerated pavement testings and lab tests. METHODS : Two accelerated pavement testings were conducted. One is to select proper sealing method of the asphalt joints and the other is to see the performance of the saw and seal method. Lab tests were conducted to select proper sealing method and a test section was constructed to see the field performance. RESULTS : The result of the first accelerated pavement testing indicated that the adhesive preformed sealants showed good performance when asphalt layer was rutted and in terms preventing from water infiltration. The second acceleration test indicated that the saw and seal method using the adhesive preformed sealant showed much better performance than the control. In the lab test bitumen, rubber and epoxy showed good performance as the adhesive. CONCLUSIONS : Saw and Seal method using the adhesive preformed sealant would markedly reduce the joint damage on the asphalt overlay.

Estiamtion of Groundwater Recharge Rate Using the NRCS-CN and the Baseflow Separation Methods (NRCS-CN방법과 기저유출 분리법을 이용한 지하수함양률 산정)

  • Bae Sang-Keun;Kim Yong-Ho
    • Journal of Environmental Science International
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    • v.15 no.3
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    • pp.253-260
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    • 2006
  • Groundwater recharge from precipitation is affected by the infiltration from ground surface and the movement of soil water. Groundwater recharge is directly related to the groundwater amount and flow in aquifers, and baseflow to rivers. Determining groundwater recharge rate for a given watershed is a prerequisite to estimate sustainable groundwater resources. The estimation of groundwater recharge rate were carried out for three subwatersheds in the Wicheon watershed and two subwatersheds in the Pyungchang River basin and for the period 1990-2000, using the NRCS-CN method and the baseflow separation method. The recharge rate estimates were compared to each other. The result of estimation by the NRCS-CN method shows the average annual recharge rate 15.4-17.0% in the Wicheon watershed and 26.4-26.8% in the Pyungchang River basin. The average annual recharge rates calculated by the baseflow separation method ranged 15.1-21.1% in the W icheon watershed, and 25.2-33.4% in the Pyungchang River basin. The average annual recharge rates calculated by the NRCS-CN method is less variable than the baseflow separation method. However, the average annual recharge rates obtained from the two methods are not very different, except NO. 6 subwatershed in Pyungchang River basin.

Comparisons of RDII Predictions Using the RTK-based and Regression Methods (RTK 방법 및 회귀분석 방법을 이용한 RDII 예측 결과 비교)

  • Kim, Jungruyl;Lee, Jaehyun;Oh, Jeill
    • Journal of Korean Society of Water and Wastewater
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    • v.30 no.2
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    • pp.179-185
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    • 2016
  • In this study, the RDII predictions were compared using two methodologies, i.e., the RTK-based and regression methods. Long-term (1/1/2011~12/31/2011) monitoring data, which consists of 10-min interval streamflow and the amount of precipitation, were collected at the domestic study area (1.36 km2 located in H county), and used for the construction of the RDII prediction models. The RTK method employs super position of tri-triangles, and each triangle (called, unit hydrograph) is defined by three parameters (i.e., R, T and K) determined/optimized using Genetic Algorithm (GA). In regression method, the MovingAverage (MA) filtering was used for data processing. Accuracies of RDII predictions from these two approaches were evaluated by comparing the root mean square error (RMSE) values from each model, in which the values were calculated to 320.613 (RTK method) and 420.653 (regression method), respectively. As a results, the RTK method was found to be more suitable for RDII prediction during extreme rainfall event, than the regression method.

EXPERIMENTAL STUDY ON EFFECTS OF PULP CAPPING AGENTS THAT ARE USED IN VITAL PULPOTOMY TO PULP TISSUE (생활치수절단술에 사용되는 복탁제가 치수에 미치는 영향에 관한 실험적 연구)

  • Cha, Moon-Ho
    • The Journal of the Korean dental association
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    • v.9 no.4
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    • pp.157-160
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    • 1971
  • To compare the effects of various pulp capping agents that are usually applied to human pulp tissue, adult dogs were bred for a certain period and each capping agent was applied experimentally to pulp tissue after vital pulpotomy. Histological observations are as follows. 1) In comparison between methods of vital pulpotomy, one and two appointment method, different courses of healing were observed. In one appointment method, the granulation tissue formation at the amputation sur face of pulp tissue had a tendency to be transformed to scar tissue formation. In two appointment method, more transformation than that of one appointment method from scar tissue to dentin matrix formation were observed. 2) Histologic changes that have appeared in pulp tissue are a) fixation at outer layer b) degeneration at middle layer c) hyperemia and round cell infiltration at inner layer 3) With use of formocresol mixed zinc oxide powder in two appointment method complete formation of dentin matrix were observed. 4) Among the methods and aagents described above formocresol mixed zinc oxide powder in two appointment method appeared to be relatively effective.

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Mechanical Properties of SiC Particulate Reinforced Mg Matrix Composites Fabricated by Melt Stirring Method (용탕교반법에 의한 SiC 입자강화 Mg기 복합재료의 기계적 특성)

  • Lim, Suk-Won;Choh, Takao;Park, Young-Jin
    • Journal of Korea Foundry Society
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    • v.13 no.5
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    • pp.441-449
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    • 1993
  • SiC particulate reinforced magnesium matrix composites were fabricated by melt stirring method. The effet of several factors on mechanical properties and the efficiency of melt stirring method from the viewpoint of these properties were investigated. The tensile strength increased and the elongation decreased with decrease of the particle size or the increase of the paticulate volume fraction for pure magnesium matrix and Mg-5%Zn alloy matrix composites. A longer stirring time improved the tensile strength of these composites. The tensile strength of Mg-5%Ca alloy matrix composites which shows no uniform paticulate distribution was a little lower than that of matrix alloy. Rapid solidification rate is preferred for the improved tensile strength of these composites. The pure magnesium matrix and Mg-5%Zn alloy matrix composites have tensile strength of about 400MPa. This value agrees with the tensile strength of some magnesium matrix composites fabricated by liquid infiltration method or powder metallurgy method at the same volume fraction of reinforcements of whisker or particle. Therefore, the melt stirring method which has the advantages of simple process is considered to be efficient in fabricating magnesium matrix composites.

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Heavy Rain and Flood Prevention in Urban (뉴스초점: 집중호우와 도시지역 홍수방어)

  • Jeong, Sun-Gil
    • Journal of the Korean Professional Engineers Association
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    • v.43 no.6
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    • pp.31-34
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    • 2010
  • Recently, due to localized heavy rain and flash floods in urban areas is becoming more frequent flood damage. To prevent flood inundation damage, to formulate the diverse directions in connection with the drainage system of buildings, roads, sewerage, pump stations, detention (retention) pond, and streams is very important. In addition, it is important for the uniform design criteria, the consistent of hydrologic and hydraulic analysis method, and a flood disaster mitigation systems connected with structural and nonstructural measures. To accomplish this, the method such as installation of storage facilities, infiltration facilities, and underground water tank, the optimal size of the design gutter and grate of the road, ensure the capacity of pumping stations, and the installation of a flood control channel into the deep underground requires comprehensive measures dimension in urban areas.

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