• Title/Summary/Keyword: hot pressing condition

Search Result 45, Processing Time 0.019 seconds

A Performance characteristics of Pt/C Electrode prepared by Hot Pressing Method (Hot Pressing법에 의해 제조된 Pt/C 전극의 성능특성)

  • 김진수;서동우;설용건;이태희
    • Journal of Energy Engineering
    • /
    • v.1 no.1
    • /
    • pp.58-65
    • /
    • 1992
  • Pt loaded porous carbon Pt/C electrode was prepared by hot pressing process to enhance the electrode performance in PAFC (phosphoric acid fuel cell). By changing the hot pressing conditions and PTFE contents, Pt/C electrodes were prepared and the electrochemical characteristics of oxygen reduction and unit-cell performance were evaluated. The optimum condition of hot press to make electrode is 360$^{\circ}C$ and 10 kg/$\textrm{cm}^2$. Maximum performance was obtained at 30 wt% PTFE content in the catalyst layer with 80% utilization of platinum clusters. Unit-cell performance of hot pressed Pt/C electrode was 200 mA/$\textrm{cm}^2$ at 700 ㎷ and stable performance was maintained more than 200 hr.

  • PDF

Effects of Additives and Hot-Pressing Conditions on the Surface and Performance of MEAs for PEMFCs (첨가제를 이용한 촉매슬러리 조성 안정화 및 열-압착 공정 최적화 통한 PEMFC용 MEA 개발)

  • Jang, Hyun-Sook;Cho, Eun-Ae
    • Transactions of the Korean hydrogen and new energy society
    • /
    • v.21 no.5
    • /
    • pp.398-404
    • /
    • 2010
  • Process conditions for MEA fabrications have significant effects on properties and performance of the MEAs for PEMFCs. In this study, effects of additives on the surface properties of the MEA was investigated to improve homogeneity of the coated catalyst layer. Another parameter that affects on characteristics of the MEAs is hot-pressing condition. Hot pressing condition was optimized by using DOE (design of experiment) method.

Effects of Hot Pressing Condition on the Properties of SiCf/SiC Composites (SiCf/SiC 복합체의 특성에 미치는 열간가압소결 조건의 영향)

  • Noviyanto, Alfian;Yoon, Dang-Hyok
    • Journal of the Korean Ceramic Society
    • /
    • v.48 no.5
    • /
    • pp.335-341
    • /
    • 2011
  • Continuous SiC fiber-reinforced SiC-matrix composites ($SiC_f$/SiC) had been fabricated by electrophoretic infiltration combined with ultrasonication. Nano-sized ${\beta}$-SiC added with 12 wt% of $Al_2O_3-Y_2O_3$ additive and Tyranno$^{TM}$-SA3 fabric were used as a matrix phase and fiber reinforcement, respectively. After hot pressing at 5 different conditions, the density, microstructure and mechanical properties of $SiC_f$/SiC were characterized. Hot pressing at relatively severe conditions, such as $1750^{\circ}C$ for 1 and 2 h, resulted in a brittle fracture behavior due to the strong fiber-matrix interface in spite of their high flexural strength. On the other hand, toughened $SiC_f$/SiC composite could be achieved by hot pressing at milder condition because of the formation of weak interface in spite of the decreased flexural strength. These results proposed the importance of weak fiber-matrix interface in the fabrication of ductile $SiC_f$/SiC composite.

Studies on Wood-based Composite Panel with Waste Tire - Properties of Composite Boards in Relation to Hot Pressing Conditions - (폐타이어를 이용한 목질계 복합판넬의 연구 - 열압조건에 의한 재질특성 -)

  • Lee, Weon-Hee;Park, Sang-Jin
    • Journal of the Korean Wood Science and Technology
    • /
    • v.25 no.4
    • /
    • pp.29-38
    • /
    • 1997
  • The effect and control of wood property of reconstituted composite panels for improved board properties by wood-waste materials and development of combination method for heterogeneous materials have been of interest to the wood science researchers. The purpose of this study is to consider the properties in relation to hot pressing conditions and to develope the optimum hot pressing condition with waste wood and waste tire for the manufacturing of composite boards. The study of composite boards for recycling of wood and waste tire is nothing up to the present. Physical and mechanical properties such as specific gravity, moisture content, swelling coefficient, modulus of rupture and modulus of elasticity in bending test were studied. The condition of 3-stage press time for the lowest moisture content of composite board was $4{\rightarrow}3{\rightarrow}3$ minutes. Specific gravity of composite panels was affected mainly by the amount of rubber chip. Because of the low rigidity and high elasticity in rubber chip, it is considered the composite panel was adequate material in the place of compression load, but not bending load. Therefore, it was concluded that a use of rubber-based wood composite panel is proper to the interior materials such as floor a room than exterior materials. From the test results, the most optimum hot pressing conditions were $4{\rightarrow}3{\rightarrow}3$ minutes for 3-stage press time and $45{\rightarrow}20{\rightarrow}5kg/cm^2$ for 3-stage press pressure. The rubber-based wood composite panel was very excellent in elasticity by combination of rubber chip in comparison with existing other wood-based materials. Therefore, it was considered that rubber-based wood composites can be applicable to every interior materials such as floor a room and will be expected to effective reuse and recycle of waste tires and wood-waste materials, and will be contribute to protection of environment pollution in earth.

  • PDF

Effect of Hot-Pressing Time and Temperature on Properties of Bamboo Zephyr Boards (대나무 Zephyr 보드의 제조에 있어서 열압시간과 열압온도가 보드성능에 미치는 영향)

  • Jung, Ki-Ho;Kim, Yu-Jung;Roh, Jeang-Kwan;Park, Sang-Jin
    • Journal of the Korean Wood Science and Technology
    • /
    • v.31 no.2
    • /
    • pp.77-83
    • /
    • 2003
  • In this research, in order to investigate the effect of hot-pressing condition, properties of bamboo zephyr boards (target density 0.7 g/cm3, 400×400×12 mm) produced by different hot-pressing time and temperature were compared through Korean Standard(KS) F 3104 and F 3113, and the results were summarized as follows: All of the boards had comparatively high values in bending properties (MOR, MOE) irrespective of hot-pressing condition, and the boards hot-pressed by 160℃ and 12 min showed the highest strength in parallel direction of board-surface to span. Internal bond (IB) strength of the boards generally increased with the increase of hot pressing temperature. Boards produced by hot pressing temperature and time of 160℃ and 12 min and 180℃ and 10 min exhibited relatively higher wet-bending strength. Thickness swelling (TS) of all the boards showed good dimensional stability of 6% or less.

Thermoelectric Properties of Skutterudite CoSb3 Fabricated by Mechanical Alloying Process (기계적 합금화에 의해 제조된 Skutterudite CoSb3의 열전특성)

  • Choi Moon-Kwan;Cho Hyoung-Won;Ur Soon-Chul;Kim Il-Ho
    • Korean Journal of Materials Research
    • /
    • v.14 no.11
    • /
    • pp.802-806
    • /
    • 2004
  • Skutterudite $CoSb_3$ powders were produced by mechanical alloying (MA) of elemental powders using a nominal stoichiometric composition. Annealing of MA powders under specific condition led to a complete phase transformation to a semiconducting ${\delta}-CoSb_3$. Single phase $CoSb_3$ was successfully produced by vacuum hot pressing using MA powders without subsequent annealing. Phase transformations during mechanical alloying and hot pressing were systematically investigated using XRD and SEM. Thermoelectric properties as a function of temperature were evaluated for the hot pressed specimens and compared with results of analogous studies.

Fabrication of $Si_3N_4-SiC$ Nanocomposites by Hot Pressing (Hot Pressing에 의한 $Si_3N_4-SiC$ 나노복합체의 제조)

  • 김성현;김인술;박홍채;오기동
    • Journal of the Korean Ceramic Society
    • /
    • v.31 no.9
    • /
    • pp.1021-1029
    • /
    • 1994
  • SiC ultrafine particles of 1, 10, 20 and 30 vol% were dispersed in $\alpha$-Si3N4 matrix and hot-pressed under the condition of 30 MPa at 1800 and 190$0^{\circ}C$ respectively. Physical, mechanical properties and microstructures of sintered Si3N4-SiC nanocomposites were investigated. Flexural strength and density of Si3N4-10 vol% SiC nanocomposites hot-pressed at 190$0^{\circ}C$ represented the 1002 MPa and 97.9%T.D respectively, and it was confirmed as a remarkable improvement of 67% compared to Si3N4 monolith. Fracture toughness was shown as 7.2 MPa.m1/2 when the same composition was hot pressed at 180$0^{\circ}C$. This effect was supposed to be due to the improvement of microstructure by the adequate suppression of the excessive growth of Si3N4 grain with SiC nano-particles.

  • PDF

Effect of Post-processing on Mechanical Properties of 3D Printed Carbon Chopped Fiber Reinforced Composites (3D 프린팅 된 탄소 단섬유강화 복합재료의 후처리 효과가 재료의 기계적 성능에 미치는 영향)

  • Jia-le, Che;Seung-Hwan, Chang
    • Composites Research
    • /
    • v.35 no.6
    • /
    • pp.463-468
    • /
    • 2022
  • The high porosity of the infill pattern of carbon chopped fiber-reinforced Nylon composite structures fabricated by the fused filament fabrication (FFF) type 3D printers determines the mechanical performance of the printed structures. This study experimentally evaluated the mechanical performance of Onyx composite specimens fabricated with a rectangular infill structure under the hot-pressing condition to improve the mechanical properties by reducing the porosity of the infill pattern of the printed structure, and evaluated the best mechanical performance. The hot-pressing conditions (145℃, 4 MPa, 12 min) that induce the most appropriate mechanical properties were found. As a result of microscopic observation, it was confirmed that the infill porosity of the composite specimens subjected to post hot-pressing treatment was effectively reduced. In order to confirm the mechanical performance of the post-treated specimen, a tensile test and a three-point bending test were performed with a control specimen without post-treatment and a specimen printed with the same density and dimensions after post-treatment to evaluate the mechanical properties. As a result of comparison, it was confirmed that the mechanical properties were effectively improved when the post-treatment of hot-pressing was performed.

Development of New Micro Pattern Fabrication Process by U sing Isostatic Pressing (정수압을 이용한 미세 패턴 전사 신공정 개발)

  • Seol, J.W.;Joo, B.Y.;Rhim, S.H.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
    • /
    • 2009.10a
    • /
    • pp.267-270
    • /
    • 2009
  • In the present investigation, we are newly developing a new forming process which can fabricate micro patterns on large-area polymeric substrates for high speed mass production. The key idea of the new process is to pressurize multiple vacuum-packed substrate-mold stacks above the glass transition temperature ($T_g$) of the polymeric substrates. The new process is thought to be promising micro-pattern fabrication technique in three aspects; firstly, isostatic pressing ensures the uniform micro-pattern replicating condition regardless of the substrate area. Secondly, the control of forming condition such as temperature and pressure can realize well-defined process condition exploited in the conventional hot embossing research field. Thirdly, multiple substrates can be patterned at the same time. A prototype forming machine for the new process was developed with the design consideration realizing the present idea. With a developed machine, micro prismatic array patterns with 50 um in size were successfully made on the $380{\times}300{\times}6\;mm$ PMMA plate.

  • PDF

Machinability and Strength of AlN-BN Ceramics (AlN-BN계 세라믹스의 기계가공성과 강도)

  • 감직상;하정수;정덕수;한경섭
    • Journal of the Korean Ceramic Society
    • /
    • v.31 no.2
    • /
    • pp.177-184
    • /
    • 1994
  • AlN-BN ceramics with BN contents in the range of 10 to 40 wt% were prepared by hot pressing using no additive, or 3 wt%, Y2O3 or CaO, which are common densification aids for AlN. And their machinability, bend strength, and microstructures were investigated. Both the main and radial cutting forces decreased with increasing BN content in all three kinds of samples. For the BN contents of 30 wt% or above, the cutting forces were lower than that of a mild steel tested at a same condition. Especially in the case of main forces, the values were less than a quarter of that of a mild steel, indicating excellent machinability. Bend strength (when the tensile surfaces of specimens were perpendicular to the hot pressing direction) also decreased with BN content mainly due to the much lower Young's modulus of BN compared to AlN. With the composition of 30 wt% BN at which the AlN-BN ceramics started to show better machinability than a mild steel, the bend strength was 150 to 160 MPa, which is greater than that of machinable glass-ceramics of a mica system. With tensile surfaces parallel to the hot pressing direction, however, the bend strength obtained for the samples processed with the sintering acids showed low values (about 40 MPa), since most BN particles had such orientation that their cleavage planes (i.e., basal planes) were perpendicular to the pressing direction.

  • PDF