• 에너지공학
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• 제1권1호
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• pp.58-65
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• 1992

인산형 연료전지의 전극성능의 향상을 위해 Hot Pressing공정을 사용하여 Pt이 담지된 다공성 탄소전극(Pt/C)을 제조하였다. Hot pressing의 조건, 촉매층에서의 PTEE 함량을 변화시켜 제조한 Pt/C 전극의 전기화학적 산소환원특성 및 인산형 단위전지 성능특성을 비교하였다. 실험결과 Hot Pressing의 최적조건은 36$0^{\circ}C$, 10kg/$\textrm{cm}^2$이었다. 최대성능은 촉매층에 30wt%의 PTFE 함량을 가진 전극에서 얻어졌으며, 이때 백금의 이용율은 80%이었다. 단위전지의 성능측정 결과, hot pressing한 전극의 성능은 700㎷에서 200mA/$\textrm{cm}^2$이었으며 200시간동안 안정적인 성능이 유지되었다.

• 한국수소및신에너지학회논문집
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• 제21권5호
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• pp.398-404
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• 2010

Process conditions for MEA fabrications have significant effects on properties and performance of the MEAs for PEMFCs. In this study, effects of additives on the surface properties of the MEA was investigated to improve homogeneity of the coated catalyst layer. Another parameter that affects on characteristics of the MEAs is hot-pressing condition. Hot pressing condition was optimized by using DOE (design of experiment) method.

• 한국세라믹학회지
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• 제48권5호
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• pp.335-341
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• 2011

Continuous SiC fiber-reinforced SiC-matrix composites ($SiC_f$/SiC) had been fabricated by electrophoretic infiltration combined with ultrasonication. Nano-sized ${\beta}$-SiC added with 12 wt% of $Al_2O_3-Y_2O_3$ additive and Tyranno$^{TM}$-SA3 fabric were used as a matrix phase and fiber reinforcement, respectively. After hot pressing at 5 different conditions, the density, microstructure and mechanical properties of $SiC_f$/SiC were characterized. Hot pressing at relatively severe conditions, such as $1750^{\circ}C$ for 1 and 2 h, resulted in a brittle fracture behavior due to the strong fiber-matrix interface in spite of their high flexural strength. On the other hand, toughened $SiC_f$/SiC composite could be achieved by hot pressing at milder condition because of the formation of weak interface in spite of the decreased flexural strength. These results proposed the importance of weak fiber-matrix interface in the fabrication of ductile $SiC_f$/SiC composite.

• Journal of the Korean Wood Science and Technology
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• 제25권4호
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• pp.29-38
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• 1997

The effect and control of wood property of reconstituted composite panels for improved board properties by wood-waste materials and development of combination method for heterogeneous materials have been of interest to the wood science researchers. The purpose of this study is to consider the properties in relation to hot pressing conditions and to develope the optimum hot pressing condition with waste wood and waste tire for the manufacturing of composite boards. The study of composite boards for recycling of wood and waste tire is nothing up to the present. Physical and mechanical properties such as specific gravity, moisture content, swelling coefficient, modulus of rupture and modulus of elasticity in bending test were studied. The condition of 3-stage press time for the lowest moisture content of composite board was $4{\rightarrow}3{\rightarrow}3$ minutes. Specific gravity of composite panels was affected mainly by the amount of rubber chip. Because of the low rigidity and high elasticity in rubber chip, it is considered the composite panel was adequate material in the place of compression load, but not bending load. Therefore, it was concluded that a use of rubber-based wood composite panel is proper to the interior materials such as floor a room than exterior materials. From the test results, the most optimum hot pressing conditions were $4{\rightarrow}3{\rightarrow}3$ minutes for 3-stage press time and $45{\rightarrow}20{\rightarrow}5kg/cm^2$ for 3-stage press pressure. The rubber-based wood composite panel was very excellent in elasticity by combination of rubber chip in comparison with existing other wood-based materials. Therefore, it was considered that rubber-based wood composites can be applicable to every interior materials such as floor a room and will be expected to effective reuse and recycle of waste tires and wood-waste materials, and will be contribute to protection of environment pollution in earth.

• Journal of the Korean Wood Science and Technology
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• 제31권2호
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• pp.77-83
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• 2003

본 연구에서는 대나무 Zephyr 보드에 있어서 열압조건이 보드의 성능에 미치는 영향을 조사하기 위하여 다양한 열압시간과 열압온도를 적용하여 보드(목표밀도 0.7 g/cm³, 400×400×12 mm)를 제조하고 그 기본적인 물성을 비교, 검토해 보았다. 제조된 보드는 KS F 3104와 KS F 3113에 준하여 성능평가를 하였으며 그 결과는 다음과 같다. 보드의 상태 휨강도는 열압조건에 관계없이 전반적으로 상당히 높은 값을 나타내었으며 그 중 span에 대한 평행 방향에 있어서는 열판온도 160℃에서 12분 동안 열압하여 제조한 보드가 가장 높은 강도를 보였다. 보드의 박리강도 시험에서는 모든 열압시간에서 열압온도가 높을수록 상대적으로 더 높은 값을 나타내었으며, 그 결과 200℃에서 압체된 보드가 가장 높은 강도를 보였다. 보드의 습윤 휨강도 시험에서는 총 열압시간 12분과 10분일 때 각각 160℃와 180℃의 온도에서 제조된 보드가 상대적으로 높은 강도를 나타내었다. 더욱이, 200℃에서 8분 동안 열압하여 제조한 보드의 경우 상태 휨강도에 거의 육박하는 가장 높은 습윤 휨강도를 보였다. 두께 팽창율 시험에서는 모든 보드에서 전반적으로 6% 미만의 낮은 값을 나타내어 높은 치수안정성을 가지는 것을 알 수 있었다.

• 한국재료학회지
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• 제14권11호
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• pp.802-806
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• 2004

Skutterudite $CoSb_3$ powders were produced by mechanical alloying (MA) of elemental powders using a nominal stoichiometric composition. Annealing of MA powders under specific condition led to a complete phase transformation to a semiconducting ${\delta}-CoSb_3$. Single phase $CoSb_3$ was successfully produced by vacuum hot pressing using MA powders without subsequent annealing. Phase transformations during mechanical alloying and hot pressing were systematically investigated using XRD and SEM. Thermoelectric properties as a function of temperature were evaluated for the hot pressed specimens and compared with results of analogous studies.

• 한국세라믹학회지
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• 제31권9호
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• pp.1021-1029
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• 1994

SiC ultrafine particles of 1, 10, 20 and 30 vol% were dispersed in $\alpha$-Si3N4 matrix and hot-pressed under the condition of 30 MPa at 1800 and 190$0^{\circ}C$ respectively. Physical, mechanical properties and microstructures of sintered Si3N4-SiC nanocomposites were investigated. Flexural strength and density of Si3N4-10 vol% SiC nanocomposites hot-pressed at 190$0^{\circ}C$ represented the 1002 MPa and 97.9%T.D respectively, and it was confirmed as a remarkable improvement of 67% compared to Si3N4 monolith. Fracture toughness was shown as 7.2 MPa.m1/2 when the same composition was hot pressed at 180$0^{\circ}C$. This effect was supposed to be due to the improvement of microstructure by the adequate suppression of the excessive growth of Si3N4 grain with SiC nano-particles.

• Composites Research
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• 제35권6호
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• pp.463-468
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• 2022

상용 FFF (Fused filament fabrication) 3D 프린터로 제조된 탄소 단섬유강화 나일론 복합재료 구조의 내부 채움 패턴(Infill pattern)의 높은 공극률은 프린팅 된 구조의 기계적 성능을 결정한다. 본 연구는 프린팅 된 구조의 내부 채움 패턴의 공극률을 줄여서 기계적 특성을 개선하기 위해 사각형 내부 채움 구조로 제작된 Onyx 복합 재료 시편의 열압밀 조건에 따른 시편의 기계적 성능을 실험적으로 평가하고, 가장 우수한 기계적 물성을 유도하는 열압밀 공정 조건(145℃, 4 MPa, 12 min)을 찾았다. 현미경 관찰결과 열압밀 후처리를 겪은 복합재료 시편의 내부 채움 공극률이 효과적으로 줄어듦을 확인하였다. 후처리된 시편의 기계적 성능을 확인하기 위해, 후처리를 하지 않은 대조군 시편과, 후처리 후 밀도와 치수를 동일하게 설정하여 출력한 시편과 함께 인장시험 및 3점 굽힘시험을 수행하여 기계적 물성을 비교한 결과 열압밀 후처리를 수행한 경우 기계적 물성이 효과적으로 개선되는 것을 확인하였다.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2009년도 추계학술대회 논문집
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• pp.267-270
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• 2009

In the present investigation, we are newly developing a new forming process which can fabricate micro patterns on large-area polymeric substrates for high speed mass production. The key idea of the new process is to pressurize multiple vacuum-packed substrate-mold stacks above the glass transition temperature ($T_g$) of the polymeric substrates. The new process is thought to be promising micro-pattern fabrication technique in three aspects; firstly, isostatic pressing ensures the uniform micro-pattern replicating condition regardless of the substrate area. Secondly, the control of forming condition such as temperature and pressure can realize well-defined process condition exploited in the conventional hot embossing research field. Thirdly, multiple substrates can be patterned at the same time. A prototype forming machine for the new process was developed with the design consideration realizing the present idea. With a developed machine, micro prismatic array patterns with 50 um in size were successfully made on the $380{\times}300{\times}6\;mm$ PMMA plate.

• 한국세라믹학회지
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• 제31권2호
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• pp.177-184
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• 1994

AlN-BN ceramics with BN contents in the range of 10 to 40 wt% were prepared by hot pressing using no additive, or 3 wt%, Y2O3 or CaO, which are common densification aids for AlN. And their machinability, bend strength, and microstructures were investigated. Both the main and radial cutting forces decreased with increasing BN content in all three kinds of samples. For the BN contents of 30 wt% or above, the cutting forces were lower than that of a mild steel tested at a same condition. Especially in the case of main forces, the values were less than a quarter of that of a mild steel, indicating excellent machinability. Bend strength (when the tensile surfaces of specimens were perpendicular to the hot pressing direction) also decreased with BN content mainly due to the much lower Young's modulus of BN compared to AlN. With the composition of 30 wt% BN at which the AlN-BN ceramics started to show better machinability than a mild steel, the bend strength was 150 to 160 MPa, which is greater than that of machinable glass-ceramics of a mica system. With tensile surfaces parallel to the hot pressing direction, however, the bend strength obtained for the samples processed with the sintering acids showed low values (about 40 MPa), since most BN particles had such orientation that their cleavage planes (i.e., basal planes) were perpendicular to the pressing direction.