• Title/Summary/Keyword: heat treatment

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Effect of Heat Treatment on the Bending Strength and Hardness of Wood

  • Won, Kyung-Rok;Kim, Tae-Hong;Hwang, Kyo-Kil;Chong, Song-Ho;Hong, Nam-Euy;Byeon, Hee-Seop
    • Journal of the Korean Wood Science and Technology
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    • v.40 no.5
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    • pp.303-310
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    • 2012
  • Heat treatment improves dimensional stability and sound absorption properties of wood. However, mechanical properties of wood can be deteriorated during the heat treatment. The effect of heat treatment on the bending strength and hardness of wood for Korean paulownia, Pinus densiflora, Lidiodendron tulipifera and Betula costata were measured. The heat treatment temperature has been investigated at $175^{\circ}C$ and $200^{\circ}C$, respectively. The results showed that the weight and density of wood decreased after heat treatment. It was found that the density by heat treatment was lower at $200^{\circ}C$ than that at $175^{\circ}C$. And, MOE increased with the reduced density. On the contrary, MOR and hardness decreased. In all conditions, It was found that there was a high correlation of 1% level between bending modulus of elasticity and modulus of rupture.

Heat Treatment and Characterization of Serpentine for $CO_2$ Sequestration by Mineral Carbonation (이산화탄소 탄산염광물화용 사문석의 열처리 및 특성평가)

  • Choi, Weon-Kyung;Moon, Seung-Hyun;Cho, Tae-Hwan;Lee, Jae-Keun
    • Journal of Hydrogen and New Energy
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    • v.16 no.1
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    • pp.74-81
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    • 2005
  • The heat treatment of serpentines for mineral carbonation was studied systematically. Crystallographic, spectroscopic and thermochemical properties were investigated for serpentines before and after heat treatment. Drastic weight loss due to the removal of hydroxy groupe(-OH) occupied in serpentine crystalline was revealed after heat treatment. In XPS results, MgO was founded at heat treated serpentine powders while Mg(OH) was observed at untreated serpentine powders. Metallic oxides originated from serpentine ingredients were regenerated by heat treatment.

The Effect of Heat Treatment Hold Time for Mechanical Properties of Zinc-Magnesium Alloy (아연-마그네슘 합금의 열처리에 따른 기계적 특성 연구)

  • Hwang, Injoo
    • Journal of the Korean Society for Heat Treatment
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    • v.33 no.3
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    • pp.117-123
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    • 2020
  • Due to high corrosion resistance, Zinc has been widely used in the automobile, shipping or construction industries as a galvanizing material. Zinc is popular as a coating element, but its low mechanical strength impede the expansion of applications as a load-bearing structure. The mechanical strength of Zinc can be increased through zinc based alloy process, but the ductility is significantly reduced. In this study, the mechanical strength and ductility of Zinc-Magnesium alloys with respect to heat treatment hold time was investigated. In order to enhance the mechanical strength of Zinc, a Zinc-Magnesium alloy was fabricated by a melting process. The heat treatment process was performed to improve the ductility of Zinc-Magnesium alloy. The microstructure of the heat-treated alloy specimen was analyzed using SEM. The hardness and compressive strength of the specimen were measured by a micro-hardness tester and a nano-indenter, respectively.

A Study on the Distortion induced by Heat Treatment on Automobile Bevel Gears (단조/절삭 베벨기어의 열처리 변형에 관한 연구)

  • 강우진;김명곤;조종래;이정환;이영선;배원병
    • Transactions of Materials Processing
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    • v.12 no.3
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    • pp.221-227
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    • 2003
  • Heat treatment is widely used in various manufacturing Processes to enhance the quality of a Product such as strength, surface hardness, and service life. In the heat treatment, there is dimensional change or distortion of the product, which critically influences the dimensional accuracy of precision parts. In this study, the distortion of a straight bevel gear induced by heat treatment is investigated in two cases. In the first case, the distortion induced by heat treatment we compared between a forged bevel gear and a machined bevel gear. In the second case, the distortion of an annealed gen is compared with that of a quenched gear. And finite element analysis has been Performed to predict the distortion of a heat-treated and machined bevel gear. The predicted values are compared with the experimental values.

Effect of Dry Heat Treatment of Red Ginseng and Red Ginseng Residue on Mycelial Growth and on Induced Tolerance of Fusarium oxysporum to Mercury Chloride (홍미삼과 홍삼정박의 건열처리가 Fusarium owsporum의 균사 생장과 승홍에 대한 내성에 미치는 영향)

  • Kim, Yeong-Ho;Park, Myeong-Han;Lee, Jong-Won
    • Journal of Ginseng Research
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    • v.16 no.2
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    • pp.99-104
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    • 1992
  • Korean red ginseng and water extract residue of red ginseng roots were treated with dry heat and incorporated in PDA medium to examine the effect of the materials on induced tolerance against mercury chloride and mycelial growth of Fusarium oxysporum. Ginseng residue was not effective in the inducement of tolerance to mercury chloride regardless of dry heat treatment. However, the heat treatment of ginseng and ginseng residues stimulated the mycelial growth of the fungus. The materials responsible for the detoxification appeared to be water-soluble. The stimulation of the fungal mycelial growth on the media by the heat treatment was highest in the water extract of ginseng. Due to the heat treatment, the mycelial growth was also slightly increased in n-hexane and methanol extracts of ginseng, compared with the ginseng fractions without dry heat treatment.

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Characteristics of the Post-Weld Heat Treatment of Chrome Low Alloy Material for a Power Plant Boiler (발전 보일러용 크롬 저합금강의 용접후열처리 특성)

  • Whe, Jae-Hoon;Moon, Seung-Jae;Yoo, Hoseon
    • Plant Journal
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    • v.6 no.4
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    • pp.56-62
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    • 2010
  • This study investigated characteristics of the post-weld heat treatment of SA213-T23, which was developed for water wall of the ultra super critical power boiler. The temperature of post weld heat treatment should be $730^{\circ}C$ or higher to reduce hardness of the deposit metal and heat affected zone. Coincidently, the temperature should remain $760^{\circ}C$ or lower to prevent hardness of the base metal from dropping. Hardness decline of deposit metal was trivial according to time when the holding time of heat treatment at $740^{\circ}C$ of post-weld heat treatment gradually increased from initial 15 minutes.

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Adhesion between Cu-18wt% Cr Alloy Film and Polyimide : Effect of Heat Treatment (Cu-18wt% Cr 합금박막과 폴리이미드사이의 접착력 : 열처리 영향)

  • 임준홍;김영호;한승희
    • Journal of Surface Science and Engineering
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    • v.26 no.6
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    • pp.327-333
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    • 1993
  • The effect of heat treatment on the adhesion between Cu-18wt% Cr film and polyimide has been studied by using T-peel test, AES, and XRD. Cu-18wt% Cr alloy and pure Cu films were sputter deposited onto pol-yimide. Cu was electroplated before and after heat treatment at $400^{\circ}C$ for 0.5 hr and 2 hrs respectively. The adhesion of metal film onto polyimide was considerably good before heat treatment, but heat treatment re-duced the peel adhesion strength in all specimens. The reduction in adhesion in adhesion strength values in the specimens which were plated after heat treatment was mainly due to Cr-O rich pahse formed in the metal/polyimide in-terface. In the specimens which were heat treated after plating, the enhanced ductility in the metal films con-tributes the peel adhesion strength by increasing the amount of deformation in metal strips.

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Effects of Heat Treatment on Surface Properties of Aluminum 6061 Alloy After Anodization (알루미늄 6061 합금 양극산화 후 열처리에 따른 표면 특성 관찰)

  • Seungmin, Lee;Chanyoung, Jeong
    • Corrosion Science and Technology
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    • v.21 no.6
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    • pp.495-502
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    • 2022
  • Anodization is a representative electrochemical surface treatment method that can improve both heat resistance and corrosion resistance by forming an anodization film on the surface of the aluminum. However, these properties can be changed after an additional heat treatment process. In this study, Al 6061 was subjected to an anodization process at 60 V for 1 hour, 5 hours, or 9 hours. An additional heat treatment process was performed at 500 ℃ for 30 minutes. Field emission scanning electron microscopy (FE-SEM) analysis revealed that the thickness of the anodized film was increased in proportion to the anodization time. Both pore size and pore diameter of the anodized film was also increased after anodization. After an additional heat treatment process, there were no significant changes in the thickness, pore size, or pore diameter of the anodized film. Heat resistance was confirmed through thermal analysis and chemical resistance was evaluated with a potentiodynamic polarization test.

Improvement of Physical and Drying Properties of Large Diameter and Long Axis Moso Bamboo (Phyllostachys pubescens) Poles Using Heat Treatment

  • Kyoung-Jung KIM;Young-Jin KIM;Se-Yeong PARK
    • Journal of the Korean Wood Science and Technology
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    • v.51 no.6
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    • pp.447-447
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    • 2023
  • This study aimed to convert underutilized moso bamboo into high-value added products such as fences, interior materials, lighting fixtures, and accessories. Green moso bamboo poles with a diameter of approximately 10 cm and a length of approximately 3.7 m were heat treated at 140℃ using a large-scale kiln. The processing time was meticulously adjusted through various stages, including pretreatment (6-8 hours at 60℃), cooking (8-10 hours at 100℃), steaming (26-30 hours at 120℃), heating (4-6 hours at 140℃), and finally, cooling (below 80℃). A meticulously designed heat treatment process has enabled efficient mass production of moso bamboo poles with improved qualities, including minimal splitting, moisture levels below 3%, and a specific gravity of 1.05. The focus of this study was to present the physical and drying properties, such as color, dimensional change, specific gravity, moisture content, and splitting, observed during the heat treatment process.

Improvement of the Biocompatibility of Chitosan Dermal Scaffold by Rigorous Dry Heat Treatment

  • Kim, Chun-Ho;Park, Hyun-Sook;Gin, Yong-Jae;Son, Young-Sook;Lim, Sae-Hwan;Park, Young-Ju;Park, Ki-Sook;Park, Chan-Woong
    • Macromolecular Research
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    • v.12 no.4
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    • pp.367-373
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    • 2004
  • We have developed a rigorous heat treatment method to improve the biocompatibility of chitosan as a tissue-engineered scaffold. The chitosan scaffold was prepared by the controlled freezing and lyophilizing method using dilute acetic acid and then it was heat-treated at 110$^{\circ}C$ in vacuo for 1-3 days. To explore changes in the physicochemical properties of the heat-treated scaffold, we analyzed the degree of deacetylation by colloid titration with poly(vinyl potassium sulfate) and the structural changes were analyzed by scanning electron microscopy, Fourier transform infrared (FT-IR) spectroscopy, wide-angle X-ray diffractometry (WAXD), and lysozyme susceptibility. The degree of deacetylation of chitosan scaffolds decreased significantly from 85 to 30% as the heat treatment time increased. FT-IR spectroscopic and WAXD data indicated the formation of amide bonds between the amino groups of chitosan and acetic acids carbonyl group, and of interchain hydrogen bonding between the carbonyl groups in the C-6 residues of chitosan and the N-acetyl groups. Our rigorous heat treatment method causes the scaffold to become more susceptible to lysozyme treatment. We performed further examinations of the changes in the biocompatibility of the chitosan scaffold after rigorous heat treatment by measuring the initial cell binding capacity and cell growth rate. Human dermal fibroblasts (HDFs) adhere and spread more effectively to the heat-treated chitosan than to the untreated sample. When the cell growth of the HDFs on the film or the scaffold was analyzed by an MTT assay, we found that rigorous heat treatment stimulated cell growth by 1.5∼1.95-fold relative to that of the untreated chitosan. We conclude that the rigorous dry heat treatment process increases the biocompatibility of the chitosan scaffold by decreasing the degree of deacetylation and by increasing cell attachment and growth.