• Title/Summary/Keyword: gas measurement method

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A Development Of The Portable Spirometry System Of Pressure Method Using Static Pressure In Pitot Tube (개구관에서의 정체압을 이용한 차동 압력 방식의 휴대형 호흡측정 시스템 개발)

  • 이종수;신창민;김영길
    • Journal of Biomedical Engineering Research
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    • v.22 no.6
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    • pp.479-486
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    • 2001
  • Spirometer is a medical equipment which diagnoses respiratory function by measuring 9as volume across Patient's lunes through airway. Because a little overdose of anesthesia medicine can take away Patient's life in the ventilator for a surgical operation. an exact measurement of respiring volume is very important. This Paper Presented an exact flow volume calculation method from factors having an influence on measurement and introduced a spirometry system for an anesthesia ventilato. This system, using differential Pressure sensor measured flow by mutual relation with Pressure. temperature. gas density and linearization from the 2nd order characteristics of differential pressure with flow.

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Determination of Ni, Cr, Mo in Low Alloy Steel Reference Materials by Isotope Dilution Inductively Coupled Plasma Mass Spectrometry (동위원소희석 유도결합플라스마질량분석법에 의한 저 합금강 표준시료중의 Ni, Cr, Mo의 분석)

  • Suh, Jungkee;Woo, Jinchoon;Min, Hyungsik;Yim, Myeongcheul
    • Analytical Science and Technology
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    • v.16 no.1
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    • pp.82-89
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    • 2003
  • Isotope dilution mass spectrometry (IDMS) was applied to the determination of Ni, Cr, Mo in low alloy steel reference materials. The Mo isotope ratio measurement was performed by dynamic reaction cell inductively coupled plasma mass spectrometry (DRC-ICP/MS) using ammonia as a reaction cell gas. In the case of Ni and Cr measurement, all data were obtained at medium resolution mode (m/${\Delta}m=3000$) of double focusing sector field high resolution inductively coupled plasma mass spectrometry (HR-ICP/MS). For the method validation of the technique was assessed using the certified reference materials such as NIST SRM 361, NIST SRM 362, NIST SRM 363, NIST SRM 364, NIST SRM 36b. This method was applied to the determination of Ni, Cr and Mo in low alloy steel sample (CCQM-P25) provided by NMIJ for international comparison study.

Cross-verified Measurement of Sulfide Concentration in Anaerobic Conditions Using Spectroscopic, Electrochemical, and Mass Spectrometric Methods

  • Nakkyu Chae;Samuel Park;Sungyeol Choi
    • Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
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    • v.21 no.1
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    • pp.43-53
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    • 2023
  • Sulfide concentrations critically affect worker safety and the integrities of underground facilities, such as deep geological repositories for spent nuclear fuel. Sulfide is highly sensitive to oxygen, which can oxidize sulfide to sulfate. This can hinder precise measurement of the sulfide concentration. Hence, a literature review was conducted, which revealed that two methods are commonly used: the methylene blue and sulfide ion-selective electrode (ISE) methods. Inductively coupled plasma optical emission spectroscopy (ICP-OES) was used for comparison with the two methods. The sulfide ISE method was found to be superior as it yielded results with a higher degree of accuracy and involved fewer procedures for quantification of the sulfide concentration in solution. ICP-OES results can be distorted significantly when sulfide is present in solution owing to the formation of H2S gas in the ICP-OES nebulizer. Therefore, the ICP-OES must be used with caution when quantifying underground water to prevent any distortion in the measured results. The results also suggest important measures to avoid problems when using ICP-OES for site selection. Furthermore, the sulfide ISE method is useful in determining sulfide concentrations in the field to predict the lifetime of disposal canisters of spent nuclear fuel in deep geological repositories and other industries.

Characterization and Preparation of Polyimide Copolymer Membranes by Non-Solvent Induced Phase Separation Method (비용매 유도 상전이법을 이용한 공중합체 폴리이미드 분리막의 제조 및 특성평가)

  • Lee, Jung Moo;Park, Jeong Ho;Kim, Deuk Ju;Lee, Myung Gun;Nam, Sang Yong
    • Membrane Journal
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    • v.25 no.4
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    • pp.343-351
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    • 2015
  • In this study, we synthesis polyimide with high gas selectivity using 2,2-bis(3,4-carboxylphenyl) hexafluoropropane, 2,4,6-Trimethyl-1,3-phenylenediamine (DAM) and 4,4-Methylenedianiline (p-MDA), and then the asymmetric membrane was fabricated by non-solvent phase separation method. To confirm the property change of the membrane using different solvent, we measured and compared the viscosity of the polymer solution, cloud point and non-solvent phase separation coefficient. The morphology and gas separation property of membrane prepared by phase separation method was confirmed using Field Emission Scanning Electron Microsope and the single gas permeation measurement apparatus. The single gas ($CH_4$, $N_2$, $O_2$, $CO_2$) permeation property and selectivity value of the membrane prepared with NMP was higher than the membrane prepared with DMAc. We confirmed that the gas selectivity of the membrane increased and the permeation property decreased with increasing of the solvent evaporation time.

Wax Appearance Temperature Measurement of Opaque Oil for Flow Assurance in Subsea Petroleum Production System (해저 석유 생산시스템 내 유동안정성 확보를 위한 불투명 오일의 왁스생성온도 측정법)

  • Lim, Jong-Se;Back, Seung-Young;Kang, Pan-Sang;Yul, Seung-Ryul;Kim, Hyo-Sang;Park, Ji-Hong
    • Journal of Advanced Marine Engineering and Technology
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    • v.36 no.1
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    • pp.185-194
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    • 2012
  • Deepwater oil is becoming more attractive because most onshore and shallow water oil is developing or developed. With the on-going trend to deepwater oil developments, flow assurance problems which prevent oil flow from reservoir to processing facilities are becoming an issue because deposited material can be occurred in case oil is exposed to very different environment from reservoir. Wax deposition which is one of flow assurance problems can be a major technical and economic issue because it is very sensitive to temperature. In order to predict and mitigate wax problems, the precise measurement of wax appearance temperature (WAT) which is the starting temperature of wax precipitation is very important. Various methods have been suggested for WAT measurement of opaque oil because there is no standard method for opaque oil. In this study, the WAT of opaque oil samples was measured using viscosity measurement method, differential scanning calorimetry, filter plugging method, and pressurized filter plugging method. Wax deposition test and high temperature gas chromatography analysis were applied to verify measured WAT. As a result of study, the WAT of opaque oils was successfully measured and verified. If WAT measurement methods of opaque oil related to oil characteristics is systematized using the results of this study, it can be a valuable tool for WAT measurement of opaque oil and flow assurance related to wax deposition.

Effect of nozzle diameter on the reduction of smoke emission from naval ship diesel engines (함정용 디젤엔진의 노즐 직경 변화가 매연 발생에 미치는 영향)

  • Son, Min-Soo;Choi, Jae-Sung;Cho, Kwon-Hae
    • Journal of Advanced Marine Engineering and Technology
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    • v.40 no.3
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    • pp.180-184
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    • 2016
  • Legislative and regulatory actions regarding the exhaust gas from ships are being strengthened by both international organizations and national governments, to protect human health and the environment. Exhaust gas traps are excluded from exhaust gas regulation applications, but, recently, the United States, Britain, and other developed countries have examined a variety of ways to improve the system, including the introduction of electric propulsion systems to prevent air pollution generated by naval ships. This study investigates a large number of smoke problems of naval diesel engines to verify the effect of improving the nozzle characteristics. An exhaust gas emission measurement method to determine the quality of pollutant exhaust gas generated during low-load operation is proposed through the research methodology of the smoke problem. It was confirmed that the emissions value is improved by decreasing the nozzle hole diameter and increasing the injection pressure. At the same time, the flow rate decrease equation and setting up a test memo based on the nozzle diameter confirmed that the fuel consumption, to which the nozzle diameter in the flow path is related, is reduced.

Electrical Properties and Microstructures in Ti Films Deposited by TFT dc Sputtering

  • Han, Chang-Suk;Jeon, Seung-Jin
    • Korean Journal of Materials Research
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    • v.26 no.4
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    • pp.207-211
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    • 2016
  • Ti films were deposited on glass substrates under various preparation conditions in a chamber of two-facing-target type dc sputtering; after deposition, the electric resistivity values were measured using a conventional four-probe method. Crystallographic orientations and microstructures, including the texture and columnar structure, were also investigated for the Ti films. The morphological features, including the columnar structures and surface roughness, are well explained on the basis of Thornton's zone model. The electric resistivity and the thermal coefficient of the resistivity vary with the sputtering gas pressure. The minimum value of resistivity was around 0.4 Pa for both the $0.5{\mu}m$ and $3.0{\mu}m$ thick films; the apparent tendencies are almost the same for the two films, with a small difference in resistivity because of the different film thicknesses. The films deposited at high gas pressures show higher resistivities. The maximum of TCR is also around 0.4 Pa, which is the same as that obtained from the relationship between the resistivity and the gas pressure. The lattice spacing also decreases with increasing sputtering gas pressure for both the $0.5{\mu}m$ and $3.0{\mu}m$ thick films. Because they are strongly related to the sputtering gas pressures for Ti films that have a crystallographic anisotropy that is different from cubic symmetry, these changes are well explained on the basis of the film microstructures. It is shown that resistivity measurement can serve as a promising monitor for microstructures in sputtered Ti films.

Measurement of Indoor Air Quality for Ventilation with the Existence of Occupants in Schools

  • Shin Hee-Soo;Lee Jai-Kwon;Ahn Young-Chull;Yeo Chang-Shin;Byun Sang-Hyun;Lee Jae-Keun;Kang Tae-Wook;Lee Kam-Gyu;Park Hyo-Soon
    • Journal of Mechanical Science and Technology
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    • v.19 no.4
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    • pp.1001-1005
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    • 2005
  • This paper evaluates the performance of ventilation for the removal of indoor pollutants as a function of ventilation rate and the number of occupants in a test room and school classroom. An experimental apparatus consists of a test room, a tracer gas supply system, a gas detector, and a fan for ventilation air supply with a controller. The ventilation performance is evaluated in a step-down method based on ASTM Standard E741-83 using $CO_{2}$ gas as a tracer gas in the test room of 35 $m^{3}.$ For the ventilation air flow rate of 1.0 ACH, a recommended ventilation flow rate of Korea school standard for acceptable indoor air quality in the case of one person, CO_{2}$ gas concentration decreases up to $55{\%}$ within 50 minutes without occupancy and increases up to $75{\%}$ in the case of one occupant. Also indoor air quality at the school classroom is investigated experimentally.

Measurement of Volatile Organic Sulfur Compounds in Ambient Air by Canister and Tedlar-bag Sampling Method (캐니스터와 Tedlar-bag 시료채집법을 이용한 대기 중의 휘발성유기황화합물의 측정)

  • 전선주;허귀석
    • Journal of Korean Society for Atmospheric Environment
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    • v.15 no.4
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    • pp.417-428
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    • 1999
  • The measurement of VOSCs(volatile organic sulfur compounds) in the air is nowadays a very important environmental research field. It is, however, very difficult because the concentration of the VOSC in ambient air is usually very low and the high reactivity makes it difficult to keep in container without loss of recovery. In this study, sampling method with cryogenic preconcentration is evaluated for analysis of atmospheric VOSC such as $CH_3SH,\;CH_3CH_2SH,\;CH_3SCH_3,\;CS_2,\;CH_3SSCH_3,\;CH_3SCH_2SCHA_3,\;and\;C_2H_5SSC_2H_5$ analyzed by GC-MS or GC-FID. Repeatabilities of measurement accompanied with preconcentration for 3-successive runs were in the range of 0.2~1.0% as a relative standard deviation. Stabilities up to 13 days were measured in 6 L canister and 10 L tedlar bag filled with VOSCs in ppb level. Higher stability was observed in tedlar bag as compared to canister with glass coated inner walls, and thiol compounds show dramatic losses in canister within 2~3 days. It is found that recovery over 70% was obtained in a week for all tested VOSCs when the compounds from ambient air matrix were stored in tedlar bag. It is also found that the stabilities of VOSCs are depending on humidity and coexisting compounds in matrix gas due to sample adsorption onto inner surface and reactivity. The results indicate the possibility and limitations of VOSC analysis in ambient air using container sampling method with cryogenic preconcentration.

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A Study on the Characteristics of Vehicle Fuel Economy by Increasing Mileage (주행거리 증가에 따른 자동차 연비 특성 연구)

  • LIM, JAE-HYUK;KIM, KI-HO;LEE, MIN-HO;PARK, JIN-SUNG;LEE, JUNG-MIN
    • Journal of Hydrogen and New Energy
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    • v.29 no.3
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    • pp.299-305
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    • 2018
  • The domestic label fuel economy measurement method is the same as the North American measurement method. The results of two test modes (city [FTP-75 mode], highway [HWFET mode]) are calculated to be equivalent to the final fuel economy value calculated as the result of five test modes reflecting various environmental conditions and driving patterns 5-cycle correction formula is used. In this study, we tried to find out that the difference between the domestic label fuel economy of the vehicle and the real road fuel economy felt by the driver compared to the new vehicle condition as the mileage increases. Using domestic label fuel economy measurement method, Four gasoline vehicles and four diesel vehicles were tested for the fuel economy of a new vehicle with a mileage of 150 km or less and domestic fuel economy test $6,500{\pm}1,000km$ durability condition and 15,000 km durability. It is confirmed that the certain portion (6,500 km endurance vehicle) The increase in mileage did not affect the fuel economy or the emission gas significantly, indicating that vehicle durability was limited.