• Journal of Surface Science and Engineering
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• v.49 no.1
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• pp.92-97
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• 2016

The plasma has been used in various industrial fields of semiconductors, displays, transparent electrode and so on. Plasma diagnostics is critical to the uniform process and the product. We use the electron temperature of the various plasma parameters for the diagnosis of plasma. Generally, the range of the electron temperature which is used in a semiconductor process used the range of 1 eV to 10 eV. The difference of electron temperature of 0.5 eV has a influence in plasma process. The electron temperature can be measured by the electrical method and the optical method. Measurement of electron temperature for various gas flow rates was performed in DC-magnetron sputter and Inductively Coupled Plasma. The physical properties of the thin film were also determined by changing electron temperatures. The transmittance was measured using the integrating sphere, and wavelength range was measured at 300 ~ 1100 nm. We obtain the thin film of the mobility, resistivity and carrier concentration using the hall measurement system. As to the electron temperature increase, optical and electrical properties decrease. We determine it was influenced by the oxygen flow ratio and plasma.

• Tunnel and Underground Space
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• v.5 no.3
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• pp.251-265
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• 1995

One of the most important matters in stress measurement by hydraulic fracturing technique is the determination of the breakdown pressure, reopening pressure, and shut-in pressure, since these values are the basic input data for the calculation of the in-situ stress. The control of the fracture propagation is also important when the hydraulic fracturing technique is applied to the development of groundwater system, geothermal energy, oil, and natural gas. In this study, a laboratory scale hydraulic fracturing device was built and a series of model tests were conducted with cube blocks of Machon gabbro. A new method called 'flatjack method' was adopted to determine shut-in pressure. The initial stress calculated from the shut-in pressure measured by flatjack method showed much higher accuracy than the stress determined by the conventional method. The dependency of the direction of fracture propagation on the state of the initial stresses was measured by introducin g artificial slots in the borehole made by water jet system. Numerical modeling by BEM was also performed to simulate the fracture propagation process. Both results form numerical and laboratory tests showed good agreement. From this study which provides the extensive results on the determination of shut-in pressure and the control of fracture propagation which are the critical issue in the recent hydraulic fracturing, it is conclued that in-situ stress measurement and the control of fracture propagation could be achived more accurately.

• Journal of the Korean Institute of Gas
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• v.19 no.1
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• pp.12-17
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• 2015

The core of the CNG fueling station is the compressor and most of CNG compressors in Korea require lubrication. Lubrication oil of CNG compressor that can be transferred into the pressure regulators and the engines of fueling system can cause a negative effect on NGV(Nature Gas Vehicle) performance during refueling due to oil Carry-over. In order to avoid the problem, it is necessary to enhance the quality of the compressed natural gas by measuring quantitatively the amount of the transferred oil. In this research, a sampling device and sampling tube were developed, which can be used with a gravimetric method of detection to measure CNG oil Carry-over. In addition, CNG samples were taken at 6 pre-selected CNG fueling stations and analysed for their trace oil Carry-over. The measured total oil Carry-over ranged from 2.569 to 6.509 ppm. This test measurements were compared with those of previous studies to verify the results.

• Proceedings of the KIEE Conference
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• 2007.11b
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• pp.46-47
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• 2007

SCADA (Supervisory Control and Data Acquisition) system has been used fur remote measurement and control on the critical infrastructures as well as modem industrial facilities. As cyber attacks increase on communication networks. SCADA network has been also exposed to cyber security problems. Especially, SCADA systems of energy industry such as electric power, gas and oil are vulnerable to targeted cyber attack and terrorism. Recently, many research efforts to solve the problems have made progress on SCADA network security. In this paper, we introduce recent security issue of SCADA network and propose the application of encryption method to Korea SCADA network.

• Journal of Environmental Science International
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• v.19 no.12
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• pp.1447-1454
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• 2010

In this study, the detection limits of lower fatty acids in air were investigated by using Dynamic SPME(Solid Phase Micro-Extraction), i.e. improved Head Space - SPME method(HS-SPME). This Dynamic SPME, called SPDE(Solid Phase Dynamic Extraction), is the analytical method for volatile compounds in air with the extraction by using a stainless steel needle of which inner surface is coated with adsorption material and following the gas chromatographic analysis by inserting the needle into a injection port of GC and subsequently, desorption of the volatile compounds into a gas-chromatographic column. Extraction was carried out by passing the sample air through the needle with a suction pump which has been used for a detection tube. The result of measurement for the 6 lower fatty acids showed that the detection limits ranged from 0.10 ppm to 0.44 ppm and the linear correlation coefficients were over 0.99. Relative standard deviations obtained from 5 analytical repetition of a ca. 1.6 ppm standard mixture were in the range of 1.87%~2.47%. This method has been shown to be a adequate for the measuring C2~C5 fatty acids in air in the concentrations of over several hundreds ppb.

• Journal of the Korean Institute of Gas
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• v.14 no.5
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• pp.19-25
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• 2010

The flash points for the systems, o-xylene+n-pentanol and m-xylene+n-hexanol, were measured by using Tag open-cup tester(ASTM D1310-86). The experimental data were compared with the values calculated by the Raoult's law and the optimization method using van Laar and Wilson equations. The calculated values based on the optimization method were found to be better than those based on the Raoult's law. The predictive curve of the flash point prediction model based on the van Laar equation described the experimentally-derived data more effectively than was the case when the prediction model was based upon the Wilson equation.

• Journal of the Korean Chemical Society
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• v.4 no.1
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• pp.7-9
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• 1957

On sparking carbon-arc in water we found that a inflammable gas was generated. The object of this experiment is to prepare sols of metals by applying the gas mentioned to a solution of metallic salts. As the result of this experiment we found that : 1) By this method we can prepare easily some kinds of Ag-sol from $AgNO_3$ solution in about 30 sec. by adjusting the temperature, the quantity of stabilizer and the concentration of metallic salt. 2) The appropriate concentration of $AgNO_3$ is about 0.01% by volume, that of the stabilizer, 0.9104 N-NaOH is 0.03-2 cc/100 cc of 0.01% $AgNO_3$ solution. And the lower the temperature, the more concentrated the Ag-sol. But to check the possibility of applying this method to metals other than Au and Ag, measurement of the particle size and properties of a sol prepared by this method, should be studied. Especially, we must study what kinds of gases are generated by sparking the carbon-arc in water.

• International Journal of Aeronautical and Space Sciences
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• v.9 no.2
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• pp.64-70
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• 2008

The UAV propulsion system that will be operated for long time at more than 40,000ft altitude should have not only fuel flow minimization but also high reliability and durability. If this UAV propulsion system may have faults, it is not easy to recover the system from the abnormal, and hence an accurate diagnostic technology must be needed to keep the operational reliability. For this purpose, the development of the health monitoring system which can monitor remotely the engine condition should be required. In this study, a fuzzy trend monitoring method for detecting the engine faults including mechanical faults was proposed through analyzing performance trends of measurement data. The trend monitoring is an engine conditioning method which can find engine faults by monitoring important measuring parameters such as fuel flow, exhaust gas temperatures, rotational speeds, vibration and etc. Using engine condition database as an input to be generated by linear regression analysis of real engine instrument data, an application of the fuzzy logic in diagnostics estimated the cause of fault in each component. According to study results. it was confirmed that the proposed trend monitoring method can improve reliability and durability of the propulsion system for a long endurance UAV to be operated at medium altitude.

• Proceedings of the Korean Society of Propulsion Engineers Conference
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• 2010.05a
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• pp.85-88
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• 2010

It is essential to understand the spray characteristics of injectors for the development of liquid rocket engine systems. In this study, the image processing methods for the measurement of the spray characteristics such as spray angle, breakup length and drop size of Gas-Centered Swirl Coaxial(GCSC) injectors have been investigated. The charge-coupled device (CCD) camera with a stroboscope was used to capture the spray images. It is to be hoped that this methods could contribute to acquisition of reliable and worthwhile data for the design of injectors. Moreover, this image processing method will be verified by comparison with other experimental results.

• Analytical Science and Technology
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• v.36 no.5
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• pp.205-215
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• 2023

In the present study, an analytical method was proposed for detecting trifluralin in aquatic products at trace concentrations. The method employed QuEChERS (Quick, Easy, Cheap, Effective, Rugged, and Safe) and gas chromatography coupled with tandem mass spectrometry (GC-MS/MS) as the sample preparation and measurement, respectively. The effect of the aqueous phase volume used in the QuEChERS was demonstrated, and the ratio of 10:10 (mL) between water and acetonitrile phase was used for 5 g of sample. Besides, dSPE using C18 and primary-secondary amine (PSA) was applied to remove the potential interferences from the food matrices, indicating no remarkable analyte loss. The linear range was built up from 0.50 ㎍ L^-1 to 3.0 ㎍ L^-1 (R² = 0.9993). Other criteria, i.e., repeatability (RSD_r = 0.86-1.96 %), reproducibility (RSD_R = 1.09-2.01 %), and recovery (over 90 %), were in accordance with Appendix F of AOAC (2016) for method performance. Although no trifluralin was detected for the commercial samples (fish, shrimp, and breaded shrimp), the spiked samples performed favorable recoveries and precision.