• 제목/요약/키워드: film crystallinity

검색결과 642건 처리시간 0.034초

원거리 플라즈마 화학증착을 이용한 규소 박막의 결정성 (The crystallinity of silicon films deposited at low temperatures with Remote Plasma Enhanced Chemical Vapor Deposition(RPECVD))

  • 김동환;이일정;이시우
    • 한국진공학회지
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    • 제4권S1호
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    • pp.1-6
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    • 1995
  • Polycrystalline Si films have been used in many applications such as thin film transistors(TFT), image sensors and LSI applications. In this research deposition of Si films at low temperatures with remote plasma enhanced CVD from Si2H6-SiF4-H2 on SiO2 was studied and their crystallinity was investigated. It was condluded that growth of crystalline Si films was favorable with (1) low Si2H6 flow rates, (2) moderate plasma power, (3) moderate SiF4 flow rates, (4) moderate substrate temperature, and (5) suitable method of surface cleaning.

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졸-겔법을 이용한 Epitaxial Bismuth Titanate 박막의 제조 (Preparation of epitaxial bismuth titanate thin films by the sol-gel process)

  • 김상복;이영환;윤연흠;황규석;오정선;김병훈
    • 한국결정성장학회지
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    • 제13권2호
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    • pp.56-62
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    • 2003
  • 졸-겔법을 이용하고 금속 나프테네이트를 출발원료로 사용하여 $SrTiO_3$(100), $LaA1O_3$(100) 및 MgO(100) 기판 위에 에피탁샬 $Bi_4Ti_3O_{12}$ 박막을 제조하였다. 코팅된 전구막은 $500^{\circ}C$에서 10분간 전열처리 하였고, $750^{\circ}C$에서 30분간 최종 열처리를 행하였다. 박막의 결정화도는 X-선회절 분석법 ($\theta$-2$\theta$ 스캔과 $\beta$ 스캔)으로 조사하였고, 표면 미세구조와 거칠기를 field emission-scanning electron microscope와 atomic force microscope를 이용하여 각각 분석하였다. MgO(100) 기판 위에 제조한 박막은 모든 기판 중에서 가장 낮은 결정화도와 면내 배향성을 보였다. 가장 낮은 결정화도와 배향성을 보인 MgO(100) 기판위의 박막은 침상 형태로 성장한 반면, 결정성과 배향성이 좋은 $LaA1O_3$(100)과 $SrTiO_3$(100) 기판위의 박막들은 원형의 입자 성장 형태를 보이고 있었다.

Interface and Crystallinity of 1,4,5,8,9,11-Hexaazatriphenylene-hexanitrile thin films between an Organic and Transparent Conductive Oxide layers

  • 이현휘;이정환;김장주;김효정
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2016년도 제50회 동계 정기학술대회 초록집
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    • pp.248-248
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    • 2016
  • We have investigated the crystallinity, preferential ordering, and interfacial stability of 1,4,5,8,9,11-hexaazatriphenylene-hexanitrile (HATCN) thin film interconnected with organic/inorganic multilayer. At the region close to the organic-organic interface, HATCN formed low crystalline order with substantial amorphous phase. As film growth continued, HATCN stacked with high crystalline phase. After a sputtering deposition of the indium zinc oxide (IZO) layer on top of HATCN/organic layer, the volume fraction of preferentially ordered HATCN crystals increased without any structural deterioration. In addition, the HATCN surface was kept quite stable by preserving the sharp interface between HATCN and sputtering deposited IZO layers.

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두께에 따른 $V_{1.85}W_{0.15}O_5$ 박막의 전기적 특성 (Electrical Properties of $V_{1.85}W_{0.15}O_5$ Thin Films with Thickness)

  • 이승환;이성갑;배선기;이영희
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2008년도 Techno-Fair 및 추계학술대회 논문집 전기물성,응용부문
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    • pp.121-122
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    • 2008
  • The films of the vanadium tungsten oxide, $V_{1.85}W_{0.15}O_5$, were grown on Pt/Ti/$SiO_2$/Si substrate by RF sputtering method. It was found that film crystallinity, dielectric properties, and TCR properties were strongly dependent upon the thin film thickness. As increasing of $V_{1.85}W_{0.15}O_5$ thickness, the grain size, morphology, and crystallinity increased. The dielectric constants of $V_{1.85}W_{0.15}O_5$ thin films deposited at 150nm were 71.11, with a dielectric loss of 0.015, respectively. Also, The $V_{1.85}W_{0.15}O_5$ thin films showed good TCR values of -3.45%/K.

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반응성 DC 마그네트론 스퍼터법에 의한 SnO$_2$ : F 박막의 전기광학적 특성 (Electrical and Optical Properties of SnO$_2$: F Thin Films by Reactive DC Magnetron Sputtering Method)

  • 정영호;김영진;신재혁;송국현;신성호;박정일;박광자
    • 한국표면공학회지
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    • 제32권2호
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    • pp.125-133
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    • 1999
  • Fluorine-doped $SnO_2$ thin films were deposited on soda-lime glass substrates by reactive DC magnetron sputtering method. Crystallinity as well as electrical and optical properties of $SnO_2$ : F thin film were investigated as the variations of deposition conditions such as substrate temperature, DC Power, $O_2$ gas pressure, $SF_6$ gas pressure. $SnO_2$ : F thin film deposited with 5% $SF_6$ gas pressure showed electrical resistivities of $2.5\times10^{-3}$cm with the average optical transparency (about 80%) These electrical and optical properties were found to be related to the crystallinity of $SnO_2$ : F thin films.

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고상 결정화에 의해 제작된 다결정 실리콘 박막의 특성 연구 (A Study on the characteristics of polycrystalline silicon thin films prepared by solid phase cyrstallization)

  • 김용상
    • E2M - 전기 전자와 첨단 소재
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    • 제10권8호
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    • pp.794-799
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    • 1997
  • Poly-Si films have been prepared by solid phase crystallization of LPCVD(low-pressure CVD) amorphous silicon. The crystallinity of poly-Si films has been derived from UV reflectance spectrum and lies in the range between 70% and 80% . From XRD measurement the peak at 28.2$^{\circ}$from (111) plane is dominantly detected in the SPC poly-Si films, The average grain size of poly-Si film is determined by the image of SEM and varies from 4000 $\AA$ to 8000$\AA$. The electrical conductivity of as-deposited amorphous silicon film is about 2.5$\times$10$^{-7}$ ($\Omega$.cm)$^{-1}$ , and 3~4$\times$10$^{-6}$ ($\Omega$.cm)$^{-1}$ of room temperature conductivity is the SPC poly-Si films. The conductivity activation energies are 0.5~0.6 eV or the 500$\AA$-thick poly-Si films.

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고온 필라멘트 다이아몬드 CVD에서 기체유동변수가 결정성장에 미치는 영향 (Effects of Gas Flow Variables on the Crystal Growth of Diamond in Hot Filament-Assisted CVD)

  • 서문규;이지화
    • 한국세라믹학회지
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    • 제31권1호
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    • pp.88-96
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    • 1994
  • Hot filament-assisted CVD was carried out to deposit diamond films on Si(100) substrate at 90$0^{\circ}C$ using a 1% CH4-H2 mixture gas. Deposition was made at various conditions of mass flow rate of the feed gas (30~1000 sccm), pressure (2.5~300 Torr), and filament-substrate distance (4~15 mm), and the deposited films were characterized by SEM, XRD, and Raman spectroscopy. As the flow rate increases, the growth rate also increased but the crystallinity of the film was degraded. A longer filament-substrate distance simply caused both the growth rate and the crystallinity to become poorer. On the other hand, the pressure variation resulted in a maximum growth rate of 2.6 ${\mu}{\textrm}{m}$/hr at 10 Torr and the best film quality around 50 Torr, exhibiting an optimum condition. The observed trends were interpreted in terms of the flow velocity-dependent pyrolysis reaction efficiency and mass transport through the boundary layer.

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신 기술에 의한 페라이트 막의 저온 제작과 그 응용에 관한 연구 (A Study on the Low Temperature Preparation and the Practical Application of Ferrite Films by New Techniques.)

  • 최동진
    • 한국전기전자재료학회논문지
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    • 제11권8호
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    • pp.658-663
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    • 1998
  • Ferrite plating enables were grown by ferrite by plating method in solution at low temperature(<10$0^{\circ}C$). This faciltates the fabrication of new ferrite thin film devices using non- heat-resistant materials(plastic, GaAs ect) as substrates. Combining the ferrite plating with sonochemistry, application of power ultrasonic waves to stimulate chemical reactions, the crystallinity and qualities of films were improved. Modifying the reactions cell and plating conditions further improved the film quality.

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BS/Channeling을 이용한 Pt(111)/$Al_2O_3$(0001) 적층 생장 연구 (BS/channeling studies on the epitaxially grown Pt(111) films on $Al_2O_3$(0001))

  • 이종철;김신철;김효배;정광호;김긍호;최원국;송종환
    • 한국진공학회지
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    • 제7권4호
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    • pp.300-305
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    • 1998
  • rf magnetron sputtering 증착법으로 Al2O3(0001)기판위에 적층생장시킨 Pt박막의 결정성 및 이의 구조적 특성을 backscattering spectrometry(BS)/channeling, transmission electron microscopy(TEM)등을 이용해 분석하였다. $MeV^4$He ion channeling 결과, 증착시 기판의 온도가 $600^{\circ}C$, 증착된 Pt층의 두께가 3500$\AA$이었을 때 최소산란수율(channeling minimum yield)이 4%인 결정성이 우수한 Pt박막이 생장되었음을 확인하였으며, 동일한 증 착조건하에서 증착된 Pt층은 $Al_2O_3$(0001)기판위에 6중 대칭구조를 지닌(111)면방향으로 적층 생장되었으며, (111)면방향을 중심으로 대칭적인 원자배열 구조를 갖고 있는 쌍정구조를 형 성하고 있었다. 단면 TEM 분석결과에서도 격자부정합에 의한 strain을 감소시키기 위하여 형성된 쌍정을 관찰할 수 있었으며 strain이 집중되는 쌍정경계면에서 표면거칠기의 증가 또는 관찰되었다.

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