• 제목/요약/키워드: electron microscope analysis

검색결과 1,020건 처리시간 0.026초

계면활성제에 의해 손상된 피부의 Geranium essential oil 미용증진 효과 (Effectiveness for Beauty Improvement of Geranium essential oil on Skin Troubles by Surfactant)

  • 최정숙
    • 한국패션뷰티학회지
    • /
    • 제2권2호
    • /
    • pp.101-106
    • /
    • 2004
  • Allergic contact dermatitis is a common skin disease resulting from specific immunologic sensitization to topically applied various allergen. The Purpose of this study was to investigate skin morphologic cahnges by light microscopic and scanning electron Microscope, changes of protein band by SDS-PAGE(SDS-polyacrylamide gel electrophoresis) in the skin effectiveness for beruty improvement of Geranium essential oil on skin troubles by surfactant. The results of the study are as follows, 1. From the observed result of FE-Scanning Electron Microscope, groups treated by Geranium essential oil in group treated Geranium essential oil during 1 week in surfactant treated group during 1 week, the group was repaired in irregularity surface of tissue by alleviate-keratinization of Geranium essential oil. 2. As a result of protein analysis the group treated on surfactant was rised protein upper range of 97,0004a11on by hyper-keratinization and group treated during 1 week by surfactant was decreased protein below range of 43,000dalton.

  • PDF

쌍롤 주조법에 의해 제조한 알루미늄 합금의 미세조직 (Microstructures of Twin Roll Cast Aluminum Alloys)

  • 박종우;김희수;백남익
    • 한국주조공학회지
    • /
    • 제16권2호
    • /
    • pp.149-157
    • /
    • 1996
  • Several aluminum based alloys were fabricated by a twin roll strip casting mill. As-cast microstructures and microsegregations of these aluminum alloys were investigated by means of optical microscope, scanning electron microscope and electron probe micro analysis. Clear distinction on microsegregation among the alloy systems was observed, that is, A1235 and A8011 alloys showed diffused segregation in the middle of the strip, while A3003 and A5086 alloys revealed a centerline segregation consisted of lamellar structure. Above center line segregation was resulted from enrichment of the alloying elements such as Mn, Fe, Cu, Si and eutictic reaction in central region of the alloy strip.

  • PDF

저탄소.저합금 강의 베이나이트 미세 구조 연구 (Study on the bainitic microstructure in low carbon HSLA steels)

  • 강주석;안성수;유장용;박찬경
    • 한국소성가공학회:학술대회논문집
    • /
    • 한국소성가공학회 2007년도 추계학술대회 논문집
    • /
    • pp.154-157
    • /
    • 2007
  • The austenite phase observed in low carbon HSLA steels is well known to be decomposed to various bainitic microstructures, such as granular bainite, acicular ferrite and bainitic ferrite during continuous cooling process. These bainitic microstructures have been usually identified by using either scanning electron microscope (SEM) or transmission electron microscope (TEM). However, SEM and TEM images do no exactly coincide, because of the quite different sample preparation method in SEM and TEM observations. These conventional analysis method is, thus, not suitable for characterization of the complex bainitic microstructure. In this study, focused ion beam (FIB) technique was applied to make site-specific TEM specimens and to identify the 3-dimensional grain morphologies of the bainitic microstructure. The morphological feature and grain boundary characteristics of each bainitic microstructure were exactly identified.

  • PDF

Microstructural and Magnetic Characterization of Fe Nanosized Powder Synthesized by Pulsed Wire Evaporation

  • Kim, Deok Hyeon;Lee, Bo Wha
    • Journal of Magnetics
    • /
    • 제22권1호
    • /
    • pp.100-103
    • /
    • 2017
  • We studied the microstructure and magnetic properties of Fe nanosized powder synthesized by the pulsed wire evaporation method. The x-ray diffraction spectrum confirmed that this powder had a pure ${\alpha}$-Fe phase. Scanning electron microscope and transmission electron microscope measurements indicated that the prepared powder had uniform spherical shape with core-shell structure. The mean powder size was about 35 nm and the thickness of the surface passivation layer was about 5 nm. Energy dispersive X-ray spectroscopy measurement indicated that the surface passivation layer was iron oxide. Magnetic field dependent magnetization measurement at room temperature showed that the maximum magnetization of the prepared powder was 177.1 emu/g at 1 T.

3.5% NaCl에서 Arc Thermal and Plasma Arc Spray 공법이 적용된 Al- Zn 코팅 강재의 내 식 성능 평가에 관한 연구 (Performance of Al-Zn Coating by Arc Thermal and Plasma arc Thermal Spray Processes in 3.5% NaCl Solution)

  • 잔낫;이한승
    • 한국건축시공학회:학술대회논문집
    • /
    • 한국건축시공학회 2021년도 가을 학술논문 발표대회
    • /
    • pp.17-18
    • /
    • 2021
  • In the present study, Al-Zn coating was deposited by Arc thermal (AT) and plasma arc thermal (PAT) spray processes, and their corrosion characteristics were studied in 3.5% NaCl through electrochemical impedance spectroscopy (EIS), scanning electron microscope (SEM) and mechanical tests. The bond adhesion result showed that plasma arc sprayed coating had a higher value attributed to compact, dense, and less porous coating compared to arc thermal spray coating which contains defects/pores and uneven morphology as revealed by scanning electron microscope analysis. Electrochemical results revealed that the plasma arc sprayed coating had a high polarization resistance at early stage of immersion, suggesting its excellent corrosion protection performance.

  • PDF

Empirical relationship between band gap and synthesis parameters of chemical vapor deposition-synthesized multiwalled carbon nanotubes

  • Obasogie, Oyema E.;Abdulkareem, Ambali S.;Mohammed, Is'haq A.;Bankole, Mercy T.;Tijani, Jimoh. O.;Abubakre, Oladiran K.
    • Carbon letters
    • /
    • 제28권
    • /
    • pp.72-80
    • /
    • 2018
  • In this study, an empirical relationship between the energy band gap of multi-walled carbon nanotubes (MWCNTs) and synthesis parameters in a chemical vapor deposition (CVD) reactor using factorial design of experiment was established. A bimetallic (Fe-Ni) catalyst supported on $CaCO_3$ was synthesized via wet impregnation technique and used for MWCNT growth. The effects of synthesis parameters such as temperature, time, acetylene flow rate, and argon carrier gas flow rate on the MWCNTs energy gap, yield, and aspect ratio were investigated. The as-prepared supported bimetallic catalyst and the MWCNTs were characterized for their morphologies, microstructures, elemental composition, thermal profiles and surface areas by high-resolution scanning electron microscope, high resolution transmission electron microscope, energy dispersive X-ray spectroscopy, thermal gravimetry analysis and Brunauer-Emmett-Teller. A regression model was developed to establish the relationship between band gap energy, MWCNTs yield and aspect ratio. The results revealed that the optimum conditions to obtain high yield and quality MWCNTs of 159.9% were: temperature ($700^{\circ}C$), time (55 min), argon flow rate ($230.37mL\;min^{-1}$) and acetylene flow rate ($150mL\;min^{-1}$) respectively. The developed regression models demonstrated that the estimated values for the three response variables; energy gap, yield and aspect ratio, were 0.246 eV, 557.64 and 0.82. The regression models showed that the energy band gap, yield, and aspect ratio of the MWCNTs were largely influenced by the synthesis parameters and can be controlled in a CVD reactor.

A Note on Biogenic Effects of Coralloid Speleothems in Round Mountain Lava Cave, Oregon, U.S.A.

  • Kashima, Naruhiko;Ogawa, Takanori
    • 동굴
    • /
    • 제9권
    • /
    • pp.3-7
    • /
    • 1999
  • Corralloid speleothems from Round Mountain lave cave are are studied by scanning microscope and electron microprobe analyses. Scanning microscopy observation indicates that the diatom Melosira seems to contribute significantly to siliceous coralloid speleothems Electron microprobe confirms the presence of diatom and fragmental minerals(plagioclase and orthopyroxene) in coralloid speleothems. Chemical analysis of 3 diatom cells gives SiO2(74.8%), Al2O3(0.12%), FeO(0.11%), CaO(0.47%) and MgO(0.81%).

  • PDF

전자현미경 In-Situ 관찰방법을 이용한 황동의 절삭성평가 (Estimation of Machinability of Lead Brass Based on In-Situ Observation in Scanning Electron Microscope)

  • 정승부;임옥동;안성욱
    • Applied Microscopy
    • /
    • 제24권3호
    • /
    • pp.87-93
    • /
    • 1994
  • In order to elucidate the machinability of lead brass, orthogonal machining experiment was conducted in SEM(Scanning Electron Microscope) equipped with a micro-machining device at a cutting speed of $7{\mu}m/s$ for brass containing 0.2 to 3wt% Pb. The microfactors (i.e., shear angle, contact length between chip and tool) were determined by in-situ observations. Machinability of brass containing lead is discussed in terms of the microfactors and the cutting resistant force tested by lathe cutting. The dynamic behavior of the chip formation of lead brass during the machining process was examined: The chips of lead brass form as a shear angle type. The shear angle increases with the content of lead in (6:4) brass. The pronounced effect of lead on the contact length between chip and tool was observed above 1% Pb. The cutting resistant force tested by lathe decreases remarkably with the lead content in brass. The observed microfactors are in close relation to the tested resistant force in macromachining.

  • PDF

천연 강황 추출물의 약리, 화학적 특성 및 분석 (A Study on the Pharmaceutical & Chemical Characteristics and Analysis of Natural Curcumin Extract)

  • 성기천
    • 한국응용과학기술학회지
    • /
    • 제28권4호
    • /
    • pp.393-401
    • /
    • 2011
  • Natural Curcumin belongs to Zingiber Officinale Roscoe was known to possess natural odor, natural taste, natural color, and other pharmaceutical & chemical characteristics. Natural Curcumin extract was made to use ethanol as a solvent was to show a yellow color having state of solid powder and an active component. Natural Curcumin extract tested pharmaceutical & chemical experiment to dilute in curcumin 1%-water solution. Curcumin extract tested antimicrobial experiment using microbe, and tested dye experiment using fiber. Some conclusions in the result of characteristics experiment was obtained as follow. The result of antimicrobial experiment showed that the growth of staphylococcus aureus (ATCC-001) and aspergillus niger (ATCC-002) as microbes decreased according to passage of time. This phenomenon could know that Curcumin compoment showed influence to antimicrobial effect. Also, the result of dye experiment showed that cotton and sick with fiber dyeing dyed in direction of dark yellow color. This phenomenon could know that Curcumin extract showed influence to dyeing effect in observation of optical electron microscope(OEM.) The result of instrument analysis ascertained inorganic components of K(53.300ppm), Na(1.150ppm), Ca(0.711ppm), Ti(0.351ppm), Li(0.256ppm), Cu(0.233ppm) etcs from Curcumin component with ICP/OES, and ascertained organic components of propanoic acid(1.859), benzene(10.814), phenol(14.194) etcs from Curcumin component with GC/MSD.

천연 오미자 추출물의 약리, 화학적 특성 및 분석 (A study on the Pharmaceutical & Chemical Characteristics and Analysis of Natural Omija Extract)

  • 성기천
    • 한국응용과학기술학회지
    • /
    • 제28권3호
    • /
    • pp.290-298
    • /
    • 2011
  • Natural Omija belongs to magnoliaceae was known to possess natural odor, taste, color, and various pharmaceutical & chemical characteristics. Omija extraction was extracted using ethanol as a solvent. Omija extract showed a light red-violet color of viscous liquid state. Some conclusions from the result of characteristic experiment were obtained as follows. From the result of antimicrobial experiment, occurrence of staphylococuss aureus and aspergillus niger as microbes was decreased according to the passage of time. This phenomenon could know that Omija component is affected to antimicrobial effect. From the result of dye experiment, fiber dyeing showed with some ivory color after dyed to cotton and silk. This phenomenon could know that Omija component is affected to dyeing effect from observation of scanning electron microscope(SEM). From the result of instrument analysis, inorganic components of K(107.30ppm), Na(2.110ppm), Ca(0.935ppm), Mg(0.891ppm), Li(0.270ppm) etcs from Omija were detected with ICP/OES, and aromatic components of benzene(10.808), a-pinene(13.996), phenol(14.183), ${\beta}$-terpene(15.840), a-terpinolene(17.616) etcs from Omija were also detected with GC/MSD.