• 제목/요약/키워드: electron microscope analysis

검색결과 1,020건 처리시간 0.027초

ABS/AES 블렌드의 물성에 관한 연구 (Studies on the Properties of ABS/AES Blonds)

  • 강동일;하창식;조원제
    • Elastomers and Composites
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    • 제27권1호
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    • pp.13-19
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    • 1992
  • In this work, properties of ABS/AES blends were investigated. Blends were prepared by casting from THF. The thermal stability, light resistance, storage modulus and flame retardancy were measured by thermogravimetric analysis, cole. difference in Fade-o-meter, Rheovibron, and limiting oxygen index(LOI). The thermal stability, light resistance and storage modulus increased with increasing contents of AES. ABS and AES showed similar LOI. The LOI of the ABS/AES blends increased with rising contents of AES but all the blends were found to be flammable. It was observed that ABS and AES was incompatible from the morphology by scanning electron microscope(SEM).

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Synthesis and Thermo-mechanical Property of Multi-walled Carbon Nanotubes/Poly(methyl methacrylate-co-butyl acrylate) Nanocomposites Prepared Using Emulsion Polymerizations in the Presence of Amphiphilic Random Terpolymer

  • Chang, Woo-Hyuck;Ki, Ho-Seong;Cheong, In-Woo
    • 한국고분자학회:학술대회논문집
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    • 한국고분자학회 2006년도 IUPAC International Symposium on Advanced Polymers for Emerging Technologies
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    • pp.289-289
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    • 2006
  • The carboxylated MWNTs were successfully prepared by conventional acid treatment, and their structures were confirmed by FT-IR, Raman and TEM analysis. The water-dispersibility of the surface modified WNTs were good. The COOH-MWNT will show better stability during the emulsion polymerization as compared with Pristine MWNT. In-situ emulsion polymerizations of methyl methacrylate N(MMA) and n-butyl acrylate (BA) were carried out. Aggregate size and dispersion stability of the CNTs in water phase were measured using dynamic light scattering, turbidity, UV-visible spectrophotometer, and electron microscope. In addition, thermo-mechanical properties of MWNT/polymer nanocomposites were investigated.

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리그닌 함유 셀룰로오스 나노섬유로 강화된 폴리락틴산 나노복합재의 제조 및 분석 (Preparation and Characterization of Poly(lactic acid) Nanocomposites Reinforced with Lignin-containing Cellulose Nanofibrils)

  • Sun, Haibo;Wang, Xuan;Zhang, Liping
    • 폴리머
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    • 제38권4호
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    • pp.464-470
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    • 2014
  • A chemo-mechanical method was used to prepare lignin-containing cellulose nanofibrils(L-CNF) from unbleached woodpulps dispersed uniformly in an organic solvent. L-CNF/PLA composites were obtained by solvent casting method. The effects of L-CNF concentration on the composite performances were characterized by tensile test machine, contact angle machine, scanning electron microscope (SEM), and Fourier transform infrared spectroscopy (FTIR). The tensile test results indicated that the tensile strength and elongation-at-break increased by 50.6% and 31.8% compared with pure PLA. The contact angle of PLA composites decreased from $79.3^{\circ}$ to $68.9^{\circ}$. The FTIR analysis successfully showed that L-CNF had formed intermolecular hydrogen bonding with PLA matrix.

전단토에 대(對)한 점토광물학적(粘土鑛物學的) 연구(硏究) (A Study on Clay Mineralogical Characteristics of Jeondanto)

  • 최대웅;엄기태;신용화
    • 한국토양비료학회지
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    • 제6권1호
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    • pp.33-34
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    • 1973
  • Jeondanto which is known a edible earth material in the legend of local people on the Mt. Baegdeog at Yeongweul Gun, Gangweon-Do, is one of pure and well crystalized kaolinite having a thin hexagonal platy structure by X-ray, DTA and electron microscope analysis. Even though its extent is currently unknown, Jeondanto will be one of interesting materials for mineralogical study of its uniquely well crystalized structure.

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Epitaxial Growth of $NdF_3:Er^{3+}/CaF_2(111)$ by MBE

  • Ko, J.M.;Fukuda, T.
    • 한국결정성장학회:학술대회논문집
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    • 한국결정성장학회 1998년도 PROCEEDINGS OF THE 14TH KACG TECHNICAL MEETING AND THE 5TH KOREA-JAPAN EMGS (ELECTRONIC MATERIALS GROWTH SYMPOSIUM)
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    • pp.71-74
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    • 1998
  • $Er^{3+}$ doped $NdF_{3}$ single crystalline thin films with smooth, microcrack-free, and high-crystalline quality were grown on $CaF_{2}(111)$ substrate at $500^{\circ}C$by molecular beem epitaxy(MBE). The relation-ship between subcell and supercell showing the reconstructed $3^{1/2} \times 3^{1/2}$ structure was studied by reflection high-energy electron diffraction(RHEED) investigation. The film surface and the growth mode were examined in studied by RHEED patterns and atomic force microscope(AFM) images ex situ. The crystallinity of film and the lattice mismatch between $NdF_{3}Er}^{3+}(0002)$ film and $CaF_{2}(111)$ substrate depending in the $Er^{3+}$ concentration were investigated by X-ray rocking curve analysis.

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자외선 조사에 따른 실리콘 교무에 존재하는 가동성 저분자량 성분의 거동 (The Behavior of Low Molecular Weight Silicone Fluids in Silicone Rubber)

  • 홍주일;이기택;서유진;황선묵;허창수
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2004년도 추계학술대회 논문집 Vol.17
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    • pp.312-315
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    • 2004
  • In this paper we investigated the behavior of low molecular weight silicone fluids in silicone rubber by W treatment with solvent-extraction and GPC. It was shown that LMW quantity which was extracted by solvent-extraction was decreased in UV treatment time. $200{\sim}450\;g/mol$ distribution of LMW silicone fluid was contributed to recovery. It was similar to result from corona discharge. Morphological analysis was investigated by scanning electron microscope(SEM) and X-ray diffraction (XRD). The behavior of LMW silicone fluids in silicone rubber which was contributed to recovery was discussed.

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스피넬상 ${LiMn_2}{O_4}$의 합성과 수소환원에 의한 활성화 (Synthesis of Spinel Phase ${LiMn_2}{O_4}$ and its Activation by Hydrogen Reduction)

  • 이동석;류대선;임병오;이풍헌
    • 한국세라믹학회지
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    • 제37권6호
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    • pp.564-568
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    • 2000
  • Spinel LiMn2O4 catalyst with submicron and single phase particles was synthesized at 48$0^{\circ}C$ for 12 hr in air by a sol-gel method. The spinel LiMn2O4 was deoxidized by hydrogen at various temperatures. Effects of physiochemical properties of the catalyst reduced by hydrogen were examined with X-ray diffractometer, thermogravimetric analysis and scanning electron microscope. The decomposition rate of carbon dioxide was measrued using the catalyst deosidized at 35$0^{\circ}C$.

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Nature of Surface and Bulk Defects Induced by Epitaxial Growth in Epitaxial Layer Transfer Wafers

  • Kim, Suk-Goo;Park, Jea-Gun;Paik, Un-Gyu
    • Transactions on Electrical and Electronic Materials
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    • 제5권4호
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    • pp.143-147
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    • 2004
  • Surface defects and bulk defects on SOI wafers are studied. Two new metrologies have been proposed to characterize surface and bulk defects in epitaxial layer transfer (ELTRAN) wafers. They included the following: i) laser scattering particle counter and coordinated atomic force microscopy (AFM) and Cu-decoration for defect isolation and ii) cross-sectional transmission electron microscope (TEM) foil preparation using focused ion beam (FIB) and TEM investigation for defect morphology observation. The size of defect is 7.29 urn by AFM analysis, the density of defect is 0.36 /cm$^2$ at as-direct surface oxide defect (DSOD), 2.52 /cm$^2$ at ox-DSOD. A hole was formed locally without either the silicon or the buried oxide layer (Square Defect) in surface defect. Most of surface defects in ELTRAN wafers originate from particle on the porous silicon.

쇄석 골재의 알칼리-실리카 반응에 관한 실험적 연구( 제 2보 : 첨가알칼리량 및 종류가 알칼리-실리카 반응에 미치는 영향) (A Experimental Study on the Alkali-Silica Reaction of Crushed Stones (Part 2 : The Influence of the Alkali Content and the Kind of Added Alkali to the Alkali-Silica Reaction))

  • 이영수;윤재환;정재동;노재호;이양수;조일호
    • 한국콘크리트학회:학술대회논문집
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    • 한국콘크리트학회 1993년도 가을 학술발표회 논문집
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    • pp.108-112
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    • 1993
  • The term Alkali-Silica Reaction (ASR) is used to describe a reaction between certain siliceous aggregates and hydroxyl ions present in the pore fluid of a concrete. The ASR is affected by the content of alkali, the particle size and the content of reactive aggregate, water-cement ratio, humidity, temperature and so on. In this paper, the fluence of alkali content and kind of added alkali to the ASR was studied. As a result, the more the content of alkali was increased, the more the mortar-bar was expand and the expansion of mortar-bar was showed differently with the added alkali kinds, The reaction products by ASR were observed by SEM(Scanning Electron Microscope) and analyzed by EDXA(Energy Dispersive X-ray Analysis) also and showed a gel composed of alkali(Na+, K+), silica and calcium.

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이산화실리콘 층의 예각부식 (Acute Angle Etching of silicon Dioxide Layer)

  • 최연익
    • 대한전자공학회논문지
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    • 제22권4호
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    • pp.84-91
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    • 1985
  • 열적으로 성장된 이산화실리콘 층 위에 실리카 필름 박막을 도포함으로써, 열산화막의 예각부식 공정이 제안되었다. 실리카필름의 밀화온도를 175$^{\circ}C$ 에서 1,150$^{\circ}C$로 변화시킴에 따라, $3^{\circ}$ 에서 $40^{\circ}$사이의 경사각을 얻었다. 또한 예각부식 공정의 해석적인 모형이 제시되었으며, 이산화실리콘 층의 부식단면을 기술하는 방정식이 Fermat의 최단시간 정리를 이용하여 유도되었다. 전자주사 현미경으로 부터 얻어진 부식단면과 이론적으로 계산된 단면을 비교한 결과, 서로 잘 부합되었다.

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