• 한국가스학회지
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• 제2권4호
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• pp.42-46
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• 1998

소형 시험편 기술은 최소량의 재료를 사용하여 그 재료의 물리적인 거동을 특성화할 수 있기 때문에 산업설비로부터 많은 재료를 수집할 수 없는 경우에 유용한 방법이다. 본 연구에서 사용한 재료는 화력발전소 터빈로터 소재로 많이 사용되고 있는 1Cr-1Mo-0.25V강이었으며, $^630{\circ}C$에서 등온열화처리하여 5종류의 가속 열화 모사재를 만들었다. 충격시험에는 표준 시험편과 소형 시험편이 사용되었으며, 일부 소형 시험편에 소성 구속을 증가시키기 위해 측면흠을 만들어 넣었다. 표준 시험편과 소형 시험편의 충격특성을 비교하였으며 크기효과를 고찰하였고, 소형 시험편의 연성취성천이온도와 표준 시험편의 연성취성천이온도와의 상관관계를 만들었다. 따라서 소형 시험편의 충격시험결과로부터 표준 시험편의 충격특성을 추정하는 것이 가능하게 되었다.

• Geomechanics and Engineering
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• 제24권2호
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• pp.157-166
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• 2021

This paper aims at the temperature and slenderness ratio effects on physical and mechanical properties of Beishan granite. A series of uniaxial compression tests with various slenderness ratios and temperatures were carried out, and the acoustic emission signal was also collected. As the temperature increases, the fracture aperture of intercrystalline cracks gradually increases, and obvious transcrystalline cracks occurs when T > 600℃. The failure patterns change from tensile failure mode to ductile failure mode with the increasing temperature. The elastic modulus decreases with the temperature and increases with slenderness ratio, then tends to be a constant value when T = 1000℃. However, the peak strain has the opposite evolution as the elastic modulus under the effects of temperature and slenderness ratio. The uniaxial compression strength (UCS) changes a little for the low-temperature specimens of T < 400℃, but a significant decrease happens when T = 400℃ and 800℃ due to phase transitions of mineral. The evolution denotes that the critical brittle-ductile transition temperature increases with slenderness ratio, and the critical slenderness ratio corresponding to the characteristic mechanical behavior tends to be smaller with the increasing temperature. Additionally, the AE quantity also increases with temperature in an exponential function.

• Journal of Welding and Joining
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• 제10권1호
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• pp.43-51
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• 1992

The plastic zone formed around a notch tip is important in analyzing the fracture toughness of structures and particularly weld cracks existed in the weld HAZ (heat affected zone) which produces local plastic deformation at the crack tip. Therefore, in order to analyze the fracture toughness in weld HAZ, it is necessary to investigate the new fracture toughness parameter $K_{c}$ $^{*}$ and critical plastic strain energy $W_{p}$ $^{c}$ according to the shape and size of the plastic zone. 1) If the temperature corresponding to $K_{c}$ $^{*}$=130kg-m $m^{-3}$ 2/ is determined, transition temperature $T_{tr}$ the magnitude of plastic zone size, and heat input change depending on the fracture toughness. The blunted amounts of the parent and weld HAZ show mild linear variation until .delta.=0.4mm and then increase very steeply there after. 2) The relation between the plastic strain energy( $W^{p}$ ) and transition temperature( $T_{*}$tr) in parent metal is more sensitive than that of weld HAZ. However, the plastic strain energy depends on the transition temperature, and thus the yield stress, .sigma.$_{ys}$ becomes an important parameter for plastic strain energy. 3) The critical plastic strain energy( $W_{p}$ $^{c}$ ) absorbed by the plastic zone at the notch tip indicated in case of parent metal: 60J/mm, in case of heat input(20KJ/cm): 75J/mm, in case of heat input(30KJ/cm); 50J/mmJ/mm.

• 대한기계학회:학술대회논문집
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• 대한기계학회 2001년도 춘계학술대회논문집A
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• pp.132-137
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• 2001

Miniaturized specimen technology is useful to characterize the mechanical behavior using a minimum volume of material, because it is almost impossible to sample the conventional specimen for the fracture toughness test without damage to equipment. Test material was 1Cr-1Mo-0.25V steel which was widely used for turbine rotor material. Two kinds of miniaturized impact specimens were prepared, i.e., miniaturized specimen with side groove and without side groove. The correlation between ductile brittle transition temperature(DBTT) of full size impact specimen and that of miniaturized impact specimen was made. The characteristics of miniaturized impact specimens technique as well as fracture stress were discussed. Finally, we concluded that the characteristics of fracture stress change on aging time were similar to that of DBTT.

• 열처리공학회지
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• 제26권6호
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• pp.306-316
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• 2013

Microstructure and fracture behavior of a multi-phase low-density steel were investigated. After hot-rolling and heat treatment, the microstructure of low-density steel was composed of coarse ferrite grains and elongated bands which include second phases such as austenite, martensite and ${\kappa}$-carbide depending on holding time during isothermal heat treatment. After tensile test, microcracks were observed at martensite or ${\kappa}$-carbide interface in the elongated bands. Coarse ferrite grains showed cleavage fracture behavior regardless of second phase. The cleavage fracture of ferrite could be attributed to their coarse grain size and solute atoms that increase ductile-to-brittle transition temperature of ferrite. Despite of the tendency of cleavage fracture in coarse ferrite grains, a specimen having coarse spheroidized ${\kappa}$-carbide particles in the elongated bands showed high total elongation of 30%. Thus, the easiness of plastic deformation in the elongated band seems to play an important role in retardation of cleavage crack formation in coarse ferrite grains.

• 대한기계학회논문집A
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• 제20권10호
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• pp.3234-3242
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• 1996

This paper describes experimental results of modified small punch( MSP) test conducted to evaluate the fracure characteristics and mechanical properties of plasma sparayed zirconia ($ZrO_2$ stabilized with 8wt. % $Y_20_3$ : YSZ) NiCrAlY composite. The mixing ratios of YSZ/NiCrAlY were 0/100, 25/75, 50/50, 100/0 v.%. Test temperatures ranged from 293K to 1473K. This study is directed at development of thermal barrrier coating(TBC) system with superior heat resistance and mechanical properties. The microstructure and fracture process of the composite were examined by SEM and AE method. The mechanical properties of 100% YSZ were nearly independent of the temperatures tested in this study. In contrast, the NiCrAlY-containing composites showed a significant decrease of the mechanical properties above 1273K, showing a ductile- brittle transition behavior up to the temperature. Furthermore, it can seen that 25% YSZ/75% NiCrAlY composite gave the highest fracure strength and fracture energy among the mixing ratio tested over the temperature range.

• 대한기계학회논문집A
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• 제25권12호
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• pp.2109-2115
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• 2001

Miniaturized specimen technology is useful to characterize the mechanical behavior when it is difficult to sample the material enough for the test. In this study, two kinds of miniaturized Charpy impact specimens(i.e., miniaturized specimen with side groove and without side groove) of aged 1Cr- lMo-0.25V steel were prepared and tested. The relationship between the extent of degradation in terms of ductile brittle transition temperature(DBTT) and the fracture stress of 1Cr-1Mo-0.25V steel was established. The fracture stress obtained from miniaturized specimen without side groove turned out to be linearly related with the DBTT of standard specimen. Therefore the fracture toughness of aged turbine rotor steel might be evaluated by the fracture stress. In addition, the correlation between DBTT of standard specimen and that of miniaturized specimen was investigated. As the results of normalizing DBTT by maximum elastic tensile stress, the normalized DBTT of miniaturized specimen without side groove allows one to estimate that of standard specimen.

• 한국재료학회지
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• 제24권4호
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• pp.180-185
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• 2014

The current concern about these materials ($MoSi_2$ and $NbSi_2$) focuses on their low fracture toughness below the ductile-brittle transition temperature. To improve the mechanical properties of these materials, the fabrication of nanostructured and composite materials has been found to be effective. Nanomaterials frequently possess high strength, high hardness, excellent ductility and toughness, and more attention is being paid to their potential application. In this study, nanopowders of Mo, Nb, and Si were fabricated by high-energy ball milling. A dense nanostructured $MoSi_2-NbSi_2$ composite was simultaneously synthesized and sintered within two minutes by high-frequency induction heating method using mechanically activated powders of Mo, Nb, and Si. The high-density $MoSi_2-NbSi_2$ composite was produced under simultaneous application of 80MPa pressure and an induced current. The sintering behavior, mechanical properties, and microstructure of the composite were investigated. The average hardness and fracture toughness values obtained were $1180kg/mm^2$ and $3MPa{\cdot}m^{1/2}$, respectively. These fracture toughness and hardness values of the nanostructured $MoSi_2-NbSi_2$ composite are higher than those of monolithic $MoSi_2$ or $NbSi_2$.

• Journal of Welding and Joining
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• 제20권6호
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• pp.99-99
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• 2002

In order to evaluate the proper fracture strength of microstructures in a steel weldment, smaller size loading ball than used for a conventional small punch(CSP) testing is required due to regional limitation on constitutive structures. In this study, the minimized loading ball(φ 1.5mm) and bore diameter of lower die(φ 3mm) were designed for an advanced small punch(ASP) test. The results obtained from the ASP test were compared with those from a CSP testing for a X20CrMoV121 steel weldment. It was found that the ASP test clearly showed the microstructural dependance on fracture strength and ductile-brittle transition behavior of the weldment. In the ASP test, especially, the cracks tend to initiate for various directions within hemispherical indentation region of an objective structure in SP test. This indicates that the evaluation of more proper fracture strength for F.L+CGHAZ, FGHAZ and ICHAZ can be performed by means of the ASP test in a steel weldment.

• Journal of Welding and Joining
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• 제20권6호
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• pp.823-829
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• 2002

In order to evaluate the proper fracture strength of microstructures in a steel weldment, smaller size loading ball than used for a conventional small punch(CSP) testing is required due to regional limitation on constitutive structures. In this study, the minimized loading ball(${\varphi}1.5mm$) and bore diameter of lower die(${\varphi}3mm$) were designed for an advanced small punch(ASP) test. The results obtained from the ASP test were compared with those from a CSP testing for a X20CrMoV121 steel weldment. It was found that the ASP test clearly showed the microstructural dependance on fracture strength and ductile-brittle transition behavior of the weldment. In the ASP test, especially, the cracks tend to initiate for various directions within hemispherical indentation region of an objective structure in SP test. This indicates that the evaluation of more proper fracture strength for F.L+CGHAZ, FGHAZ and ICHAZ can be performed by means of the ASP test in a steel weldment.