• 제목/요약/키워드: direct determination

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DIRECT DETERMINATION OF THE DERIVATIVES OF CONDUCTIVITY AT THE BOUNDARY FROM THE LOCALIZED DIRICHLET TO NEUMANN MAP

  • Gen-Nakamura;Kazumi-Tanuma
    • Communications of the Korean Mathematical Society
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    • v.16 no.3
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    • pp.415-425
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    • 2001
  • We consider the problem of determining conductivity of the medium from the measurements of the electric potential on the boundary and the corresponding current flux across the boundary. We give a formula for reconstructing the conductivity and its normal derivative at the point of the boundary simultaneously from the localized Diichlet to Neumann map around that point.

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Chiral Separation of Aromatic Acids by Capillary Electrophoresis Using HP $\beta$-Cyclodextrin as the Chiral Selector

  • La, Soo-Kie;Kim, Ji-Young;Kim, Jung-Han;Kim, Kyoung-Rae
    • Proceedings of the PSK Conference
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    • 2002.10a
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    • pp.399.2-399.2
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    • 2002
  • Capillary electrophoretic direct chiral separation method is described for the determination of the absolute configuration of chiral aromatic acids, The enantiomeric separation was achieved by capillary electrophoresis using HP $\beta$-cyclodextrin (CD) as the chiral selector. The effect of CD concentration was investigated to optimize the chiral separation and resolution. When applied to microbial culture fluid. the present method allowed positive identification of chiral aromatic acids and their chirality as well.

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Determination of meloxicam in human plasma by semi-micro high-performance liqiud chromatography.

  • Park, Chang-Hun;Kim, Ho-Hyun;Lee, Hee-Joo;Beom, Han-Sang
    • Proceedings of the PSK Conference
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    • 2003.04a
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    • pp.276.1-276.1
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    • 2003
  • This study describes a simple and sensitive semi-micro HPLC method with UV detection and direct deproteinization. The plasma protein was precipitated using perchloric acid (60%) and the supernatant was directly injected onto the semi-micro HPLC system. The separation was achieved on a C18 (25 mm ${\times}$ 2.0 mm I.D) analytical column with a mobile phase of sodium acetate buffer (pH 3.5, 50 mmol) - acetonitrile (60:40, V/V). (omitted)

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Determination of nucleosides in human urine by high-performance liquid chromatography with electrospray ionization mass spectrometry(LC/ESI-MS)

  • Lee, Sang-Hee;Jung, Byung-Hwa;Kim, Sun-Yeou;Kim, Ho-Cheol;Chung, Bong-Chul
    • Proceedings of the PSK Conference
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    • 2003.04a
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    • pp.290.1-290.1
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    • 2003
  • Oxidative DNA damage has been associated with many disease. Quantation of DNA adducts is considered to be a useful biomarker of oxidative DNA damage because its formation can also be induced by oxidative stress. Extensive efforts have been taken to identify the analytical methods for minimizing the artifactual formation of oxidative DNA damage. We have done direct analysis of DNA adducts using LC/ESI-MS without urine sample extraction. (omitted)

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A Rapid Quantitative Assay of Intact Ambroxol Tablets by FT-NIR Spectroscopy

  • Kim, Do-Hyung;Ah, Woo-Young;Kim, Hyo-Jin
    • Proceedings of the PSK Conference
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    • 2003.10b
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    • pp.213.2-213.2
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    • 2003
  • A simple analytical procedure using FT-NIR for the rapid determination of individual ingredients was evaluated. Direct measurements were made by reflection using a reflectance accessory, by transmittance using tablet accessory and turn table. FT-NIR spectral data were transformed to the first derivative. Partial Least Square Regression(PLSR) was applied to quantify near-infrared (NIR) spectra of 2 ingredients. These calibration models were cross-validated (leave-one-out approach). The prediction ability of the models was evaluated on ambroxol tablets and compared with the real values in manufacturing procedure. (omitted)

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A Review on the Analytical Techniques for the Determination of Fluorine Contents in Soil and Solid Phase Samples (토양 및 고체시료 중 불소함량 측정기법)

  • An, Jinsung;Kim, Joo-Ae;Yoon, Hye-On
    • Journal of Soil and Groundwater Environment
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    • v.18 no.1
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    • pp.112-122
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    • 2013
  • Current status of soil contamination with fluorine and its source were investigated. The basic principles and procedures of various techniques for the analysis of fluorine contents in soil and solid phase samples were summarized in this review. Analysis of fluorine in solid matrices can be achieved by two types of techniques: (i) UV/Vis spectrophotometer or ion selective electrode (ISE) analysis after performing appropriate extraction steps and (ii) direct solid analysis. As the former cases, the standard method of Korean ministry of environment, alkali fusion-ISE method, pyrohydrolysis, oxygen bomb combustion, aqua regia digestion-automatic analysis, and sequential extraction-ISE method were introduced. In addition, direct analysis methods (i.e., X-ray fluorescence spectrometry and proton induced gamma-ray emission spectrometry) and atomic spectrometry combining with the equipment for introducing solid phase sample were also reviewed. Fluorine analysis techniques can be reasonably selected through site-specific information such as matrix condition, contamination level, the amount of samples and the principles of various methods for the analysis of fluorine presented in this review.

Fuel-Optimal Altitude Maintenance of Low-Earth-Orbit Spacecrafts by Combined Direct/Indirect Optimization

  • Kim, Kyung-Ha;Park, Chandeok;Park, Sang-Young
    • Journal of Astronomy and Space Sciences
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    • v.32 no.4
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    • pp.379-386
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    • 2015
  • This work presents fuel-optimal altitude maintenance of Low-Earth-Orbit (LEO) spacecrafts experiencing non-negligible air drag and J2 perturbation. A pseudospectral (direct) method is first applied to roughly estimate an optimal fuel consumption strategy, which is employed as an initial guess to precisely determine itself. Based on the physical specifications of KOrea Multi-Purpose SATellite-2 (KOMPSAT-2), a Korean artificial satellite, numerical simulations show that a satellite ascends with full thrust at the early stage of the maneuver period and then descends with null thrust. While the thrust profile is presumably bang-off, it is difficult to precisely determine the switching time by using a pseudospectral method only. This is expected, since the optimal switching epoch does not coincide with one of the collocation points prescribed by the pseudospectral method, in general. As an attempt to precisely determine the switching time and the associated optimal thrust history, a shooting (indirect) method is then employed with the initial guess being obtained through the pseudospectral method. This hybrid process allows the determination of the optimal fuel consumption for LEO spacecrafts and their thrust profiles efficiently and precisely.

Atmospheric Correction and Velocity Aberration for Physical Sensor Modeling of High-Resolution Satellite Images (고해상도 위성영상의 센서모델링을 위한 대기 및 속도 보정)

  • Oh, Jae-Hong;Lee, Chang-No
    • Journal of the Korean Society of Surveying, Geodesy, Photogrammetry and Cartography
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    • v.29 no.5
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    • pp.519-525
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    • 2011
  • High-resolution earth-observing satellites acquire substantial amount of geospatial images. In addition to high image quality, high-resolution satellite images (HRSI) provide unprecedented direct georegistration accuracy, which have been enabled by accurate orbit determination technology. Direct georegistration is carried out by relating the determined position and attitude of camera to the ground target, i.e., projecting an image point to the earth ellipsoid using the collinearity equation. However, the apparent position of ground target is displaced due to the atmosphere and satellite velocity causing significant georegistration bias. In other words, optic ray from the earth surface to satellite cameras at 400~900km altitude refracts due to the thick atmosphere which is called atmospheric refraction. Velocity aberration is caused by high traveling speed of earth-observing satellites, approximately 7.7 km/s, relative to the earth surface. These effects should be compensated for accurate direct georegistration of HRSI. Therefore, this study presents the equation and the compensation procedure of atmospheric refraction and velocity aberration. Then, the effects are simulated at different image acquisition geometry to present how much bias is introduced. Finally, these effects are evaluated for Quickbird and WorldView-1 based on the physical sensor model.

Direct Position Determination of Coherently Distributed Sources based on Compressed Sensing with a Moving Nested Array

  • Yankui, Zhang;Haiyun, Xu;Bin, Ba;Rong, Zong;Daming, Wang;Xiangzhi, Li
    • KSII Transactions on Internet and Information Systems (TIIS)
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    • v.13 no.5
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    • pp.2454-2468
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    • 2019
  • The existing direct position determinations(DPD) for coherently distributed(CD) sources are mostly applicable for uniform linear array(ULA), which result in a low degree of freedom(DOF), and it is difficult for them to realize the effective positioning in underdetermined condition. In this paper, a novel DPD algorithm for coherently distributed sources based on compressed sensing with a moving nested array is present. In this algorithm, the nested array is introduced to DPD firstly, and a positioning model of signal moving station based on nested array is constructed. Owing to the features of coherently distributed sources, the cost function of compressed sensing is established based on vectorization. For the sake of convenience, unconstrained transformation and convex transformation of cost functions are carried out. Finally, the position coordinates of the distribution source signals are obtained according to the theory of optimization. At the same time, the complexity is analyzed, and the simulation results show that, in comparison with two-step positioning algorithms and subspace-based algorithms, the proposed algorithm effectively solves the positioning problem in underdetermined condition with the same physical element number.

Exercise Adherence Model of Middle-Aged based on Theory of Self-determination

  • Lee, Miok
    • Journal of the Korea Society of Computer and Information
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    • v.23 no.10
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    • pp.143-149
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    • 2018
  • The purpose of this study was to construct and validate a middle - aged exercise adherence model. The model was designed based on self - determination theory. Participants were 215 middle-aged men and women aged 40-60 who had been exercising for more than six months. Data was collected from four big cities of Seoul, Busan, Gwangju and Daejeon in Korea, using a questionnaire consisting of basic psychological needs, intrinsic motivation, social support, and exercise adherence. Data were analyzed with SPSS 19.0 and AMOS 20.0. Social support and exercise adherence of the questionnaire were partially revised and verified by confirmatory factor analysis. The results of the study were as follows. The model's fit indices: GFI = .938, AGFI) = .915, NFI = .912, CFI = .941, and RMSEA = 0.041. The model satisfied the model fit of the structural model equation. This study model based on self - determination theory was confirmed that basic psychological needs, intrinsic motivation, and social support were important factors for the middle - aged's exercise adherence. Basic psychological need and intrinsic motivation had a direct influence on the adherence of exercise, and social support indirectly influenced the exercise adherence through intrinsic motivation. Both basic psychological needs and social support directly affected internal motivation. The most influential factor in the middle - aged's exercise adherence was intrinsic motivation. In conclusion, it was found that intrinsic motivation such as interest and fun is important for the middle - aged to continue the exercise. Also, the basic psychological needs were important for middle aged's exercise adherence. The results of this study will provide basic data for restoring or maintaining health by continuing exercise. Strategies that enhance intrinsic motivation are needed when a chronic ill person needs to continue long-term exercising.