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Development of µ-PIM standard mold with exchangable insert core in order to manufacture micro pattern (마이크로 패턴 성형을 위한 인서트 코어 적용 µ-PIM 표준금형 개발에 관한 연구)

  • Park, Chi Yoel;Seo, Chan-Yoel;Kim, Yongdae
    • Design & Manufacturing
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    • v.11 no.3
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    • pp.29-34
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    • 2017
  • Increased demand for parts with micro-pattern structure made of metals, ceramics, and composites in various fields such as medical ultrasonic sensors, CT collimators, and ultra-small actuator parts. Micro powder injection molding (PIM) is a technology for manufacturing micro size, high volume, complex, precision, net-shape components from either metal or ceramic powder. In the present study, a standard mold with a variable insert core capable of producing various micro patterns was investigated. An injection molding test was performed on a standard mold using a line type micro-pattern core having an aspect ratio of 2, a slenderness ratio of 70, a pattern size of $200{\mu}m$, and a pattern spacing of $150{\mu}m$. During the filling process, the deformation of the mold with large aspect ratio and slenderness ratio was analyzed by the experiment and the numerical simulation according to the position of the gate. We proposed a mold structure that minimizes mold deformation by gate modification and enables uniform pattern filling behavior.

Se-loss-induced CIS Thin Films in RTA Process after Co-sputtering Using CuSe2 and InSe2 Targets

  • Kim, Nam-Hoon;Jun, Young-Kil;Cho, Geum-Bae
    • Journal of Electrical Engineering and Technology
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    • v.9 no.3
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    • pp.1009-1015
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    • 2014
  • Chalcopyrite $CuInSe_2$ (CIS) thin films were prepared without Se- / S-containing gas by co-sputtering using $CuSe_2$ and $InSe_2$ selenide-targets and rapid thermal annealing. The grain size increased to a maximum of 54.68 nm with a predominant (112) plane. The tetragonal distortion parameter ${\eta}$ decreased and the inter-planar spacing $d_{(112)}$ increased in the RTA-treated CIS thin films annealed at a $400^{\circ}C$, which indicates better crystal quality. The increased carrier concentration of RTA-treated p-type CIS thin films led to a decrease in resistivity due to an increase in Cu composition at annealing temperatures ${\geq}350^{\circ}C$. The optical band gap energy ($E_g$) of CIS thin films decreased to 1.127 eV in RTA-treated CIS thin films annealed at $400^{\circ}C$ due to the improved crystallinity, elevated carrier concentration and decreased In composition.

Preparation and Properties of SEBS (Styrene Ethylene Butadiene Styrene Copolymer)-Clay Hybrid Gas Barrier Membranes (Gas Barrier성 SEBS (Styrene Ethylene Butadiene Styrene Copolymer)-Clay 하이브리드 막의 제조 및 물성)

  • Nam Sang Yong;Yeom Bong Yeol;Min Byoung Ryul;Kim Young Jin
    • Membrane Journal
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    • v.15 no.1
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    • pp.62-69
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    • 2005
  • SEBS-clay hybrid membranes were prepared by melt intercalation method with internal mixer. In the hybrid, the amount of clay content was fixed to 5 phr. MMT was intercalated or exfoliated by the ionomer and it was confirmed by X-ray diffraction method. D-spacing of the characteristic peak from MMT plate in SAXD was moved and diminished. Gas permeability, mechanical properties and thermal properties of the SEBS-clay hybrid membranes were investigated. Gas permeability through the SEBS-clay hybrid membranes decreased due to increased tortuosity made by intercalation of clay in SEBS.

Microstructural Feature of Discontinuous Precipitates Formed by Furnace Cooling in AZ91 Magnesium Alloy (AZ91 마그네슘 합금에서 노냉으로 생성된 불연속 석출물의 미세조직 특징)

  • Jun, Joong-Hwan
    • Journal of the Korean Society for Heat Treatment
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    • v.31 no.5
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    • pp.231-236
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    • 2018
  • The purpose of this study was to investigate the microstructural characteristics and hardness distribution of AZ91 magnesium alloy furnace-cooled to room temperature after solution treatment, and to compare the results with those of as-cast condition. The as-cast alloy showed a partially divorced eutectic ${\beta}(Mg_{17}Al_{12})$ phase and discontinuous precipitates (DPs) with a lamellar morphology, while only DPs were observed in the furnace-cooled alloy. The DPs in the furnace-cooled AZ91 alloy had various apparent interlamellar spacings, which would be ascribed to the different transformation temperatures during the furnace cooling. The average hardness for the furnace-cooled alloy is similar to that for the as-cast alloy. It is interesting to note that the hardness values of the furnace-cooled alloy were distributed over a narrower range than those of the as-cast alloy. This is likely to be caused by the relatively more homogeneous microstructure of the furnace-cooled alloy in comparison with the ascast one.

Highly Porous Pillared Clay with Multistacked $SiO_2/TiO_2$ Nanosols

  • 조진호;박주형;윤주병
    • Bulletin of the Korean Chemical Society
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    • v.19 no.11
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    • pp.1185-1188
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    • 1998
  • Layered nanocomposite, SiO2/TiO2 sol pillared clay, has been prepared by the ion exchange reaction of Na' ion in montmorillonite with positively charged mixed SiO2/TiO2 sol. The nanosized sol particles were synthesized by mixing SiO2 sol solution with TiO2 one, which is obtained by acidic hydrolysis of TEOS and TiCl4, respectively. From powder XRD, the basal spacing (d001) of the sample calcined at 400 ℃ was found to be ca. 60 Å, due to the multistacking of nanosized SiO2 and TiO2 sol particles, which was confirmed by the pore size analysis from 129Xe NMR and micropore analysis calculated from nitrogen adsorption. The BET specific surface area shows the value of 684 m2g-1 (Langmuir 1115 m2g-1), which is the highest among various pillared clays ever reported previously, and the total porosity is found to be 0.51 mlg-1, and the pores are mainly composed of micropore with a size of ca. 11.8 Å. This result agrees with the adsorption capacity obtained from water adsorption. According to diffuse reflectance ultraviolet-visible spectroscopy, it is found that the TiO2 particles stabilized in the interlayer space of montmorillonite are quantum-sized of ca. 20 Å.

Experimental investigation on shear capacity of RC beams with GFRP rebar & stirrups

  • Vora, Tarak P.;Shah, Bharat J.
    • Steel and Composite Structures
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    • v.21 no.6
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    • pp.1265-1285
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    • 2016
  • This paper presents experimental results of advanced investigation carried out on the beams reinforced with Glass Fiber Reinforced Polymer (GFRP) rebar and stirrups. Twelve beams reinforced with GFRP and one beam with steel reinforcement of size $230{\times}300{\times}2000mm$ were investigated. Longitudinal reinforcement, shear span and spacing of stirrups were the main variables to form the set. In advanced testing three types of strain gauges for steel, composite and concrete surface were applied to observe strain/stress development against the applied load. Live data were recorded from four strain gauges applied on stirrups, one at center on longitudinal reinforcement, two on the concrete surface and central deflection during the test. Although the focus of the paper was mainly on the behavior of GFRP shear reinforcement, other parallel data were observed for the completeness of the test. Design recommendations of ISIS Canada Design Manual (2007), Japan Society of Civil Engineers (1997) and American Concrete Institute (ACI-440.1R-06) were reviewed. Shear design predictions were compared with experimental results in which it was observed that all the three standards provided conservative predictions. However, ACI found most efficient compare to other two there is room to improve the efficiency of the recommendations.

Stress Analysis of Orthogonally Stiffened Rectangular Plates by the Laplace Transformation (직교보강재(直交補强材)가 붙은 구형평판(矩形平板)에 있어서의 응력해석(應力解析))

  • S.J.,Yim;J.D.,Kim
    • Bulletin of the Society of Naval Architects of Korea
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    • v.13 no.3
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    • pp.11-19
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    • 1976
  • Grillages are abundant in ship structures and in many other types of structures such as bridges and building floors. Clarkson has shown that plated grillages can be satisfactorily analyzed as gridworks if an appropriate effective breadth is taken into account. Also, it has previously been pointed out, by Nielsen, that grillage calculations could be simplified by use of the Laplace transformation. In this paper, it is assumed that the torsional rigidity of the members and axial load are negligible, also that girders have the same scantling and spacing each other and so stiffeners do. Then the grillages composed of both-end-fixed girders and both-end-hinged stiffeners, which are subjected only to uniform normal loads are investigated. The calculus of variation is used to set up the differential equations and the Laplace transformation is applied to solve the differential equations. The program has been tested by FACOM 28 and the results show good agreements with those by the STRESS, which was developed in M.I.T.. The amount of the data input and computing time are much less than those of the STRESS. But this program has so much restrictions that it is urgent to extend the program to the grillage problems of arbitrary loading and boundary conditions.

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Forces and flow around three side-by-side square cylinders

  • Zheng, Qinmin;Alam, Md. Mahbub;Rehman, S.;Maiti, D.K.
    • Wind and Structures
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    • v.29 no.1
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    • pp.1-13
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    • 2019
  • A numerical investigation on forces and flow around three square cylinders in side-by-side arrangement is conducted at a Reynolds number Re = 150 with the cylinder center-to-center spacing ratio L/W = 1.1 ~ 9.0, where W is the cylinder side width. The flowat this Re is assumed to be two-dimensional, incompressible, and Newtonian. The flow simulation is conducted by using ANSYS-Fluent. The flow around the three side-by-side cylinders entails some novel flow physics, involving the interaction between the gap and free-stream side flows as well as that between the two gap flows. An increase in L/W from 1.1 to 9.0 leads to five distinct flow regimes, viz., base-bleed flow (L/W < 1.4), flip-flopping flow (1.4 < L/W < 2.1), symmetrically biased beat flow (2.1 < L/W < 2.6), non-biased beat flow (2.6 < L/W < 7.25) and weak interaction flow (7.25 < L/W < 9.0). The gap flow behaviors, time-averaged and fluctuating fluid forces, time-averaged pressure, recirculation bubble, formation length, and wake width in each flow regime are discussed in detail.

Effects of Al Content on Microstructure and Hardness of Discontinuous Precipitates Formed by Continuous Cooling After Solution Treatment in Mg-Al Alloys (Mg-Al 합금에서 용체화처리 후 연속 냉각으로 생성된 불연속 석출물 의 미세조직과 경도에 미치는 Al 함량의 영향)

  • Joong-Hwan, Jun
    • Journal of the Korean Society for Heat Treatment
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    • v.35 no.6
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    • pp.295-302
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    • 2022
  • The present study aims to investigate the effect of Al content on microstructure and hardness of discontinuous precipitates (DPs) formed by continuous cooling (CC) in Mg-8%Al and Mg-9.5%Al alloys. The DPs had a wide range of (α+β) interlamellar spacings, which may well be attributed to the different transformation temperatures during CC. The higher Al content gave rise to the higher level of interlamellar spacings of the DPs, and thicker and larger amount of β phase layer in the DPs. It is noticeable that the Mg-9.5%Al alloy exhibited higher hardness of the DPs than the Mg-8%Al alloy, but the ratio of increase in hardness of the DPs compared to that of the as-cast state was similar regardless of the Al content. The reason was discussed based on the differences in microstructures of the DPs for the Mg-8%Al and Mg-9.5%Al alloys.

Comparison of Hardness and Damping Capacities of Mg-Al Alloy Subjected to T6 Heat Treatment and Low Temperature Long Term Isothermal Aging (T6 열처리 및 저온 장시간 등온 시효한 Mg-Al 합금의 경도 및 진동감쇠능 비교)

  • Joong-Hwan Jun
    • Journal of the Korean Society for Heat Treatment
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    • v.36 no.5
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    • pp.277-284
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    • 2023
  • Hardness and damping characteristics of fine discontinuous precipitates (DPs) microstructure generated by low temperature long term isothermal aging were investigated in comparison with those of T6 heat-treated microstructure composed of DPs and continuous precipitates (CPs) in Mg-9%Al alloy. In this study, T6 and fine DPs microstructures were obtained by isothermal aging at 453 K for 24 h and at 413 K for 336 h, respectively, after solution treatment at 693 K for 24 h. The DPs microstructure exhibited higher hardness than the T6 microstructure, which is related to the lower (α + β) interlamellar spacing of the DPs. The DPs microstructure possessed better damping capacity than the T6 microstructure in the strain-amplitude independent region, whereas in the strain-amplitude dependent region, the reverse behavior was observed. The damping tendencies depending on strain-amplitude were discussed based on the microstructural features of the T6 and DPs microstructures.